A Thermodynamic and Kinetic Study of Electrochemical Lithium Intercalation in Na0.33 V 2 O 5 Bronze Prepared by a Sol‐Gel Process

1990 ◽  
Vol 137 (4) ◽  
pp. 1042-1048 ◽  
Author(s):  
S. Bach ◽  
J. P. Pereira‐Ramos ◽  
N. Baffier ◽  
R. Messina
Keyword(s):  
Kinetic Study ◽  
Sol Gel ◽  
Lithium Intercalation ◽  
Sol Gel Process

ChemInform Abstract: A Kinetic Study of Lithium Transport in a New Li Intercalation Material Al0.11V2O5.15 Synthesized via a Sol-Gel Process.

ChemInform ◽  
2010 ◽  
Vol 27 (46) ◽  
pp. no-no
Author(s):  
R. BADDOUR-HADJEAN ◽  
J. FARCY ◽  
J. P. PEREIRA-RAMOS ◽  
N. BAFFIER
Keyword(s):  
Kinetic Study ◽  
Sol Gel ◽  
Lithium Transport ◽  
Sol Gel Process

A Kinetic Study of Lithium Transport in a New Li Intercalation Material Al0.11 V 2 O 5.15 Synthesized via a Sol‐Gel Process

1996 ◽  
Vol 143 (7) ◽  
pp. 2083-2088 ◽  
Author(s):  
R. Baddour‐Hadjean ◽  
J. Farcy ◽  
J. P. Pereira‐Ramos ◽  
N. Baffier
Keyword(s):  
Kinetic Study ◽  
Sol Gel ◽  
Lithium Transport ◽  
Sol Gel Process

The crystallization of thin-film ceramics

1992 ◽  
Vol 50 (1) ◽  
pp. 338-339
Author(s):  
J.M. Schwartz ◽  
L.F. Francis ◽  
L.D. Schmidt ◽  
P.S. Schabes-Retchkiman
Keyword(s):  
Thin Films ◽  
Grain Size ◽  
Sol Gel ◽  
Processing Route ◽  
Small Areas ◽  
Ceramic Thin Films ◽  
Complex Shapes ◽  
Sol Gel Process ◽  
Ceramic Precursors ◽  
Crystalline Ceramic

Ceramic thin films and coatings are of interest for electrical, optical, magnetic and thermal barrier applications. Critical for improved properties in thin films is the development of specific microstructures during processing. To this end, the sol-gel method is advantageous as a versatile processing route. The sol-gel process involves depositing a solution containing metalorganic or colloidal ceramic precursors onto a substrate and heating the deposited layer to form a crystalline or non-crystalline ceramic coating. This route has several advantages, including the ability to create tailored microstructures and properties, to coat large or small areas, simple or complex shapes, and to more easily prepare multicomponent ceramics. Sol-gel derived coatings are amorphous in the as-deposited state and develop their crystalline structure and microstructure during heat-treatment. We are particularly interested in studying the amorphous to crystalline transformation, because many key features of the microstructure such as grain size and grain size distribution may be linked to this transformation.

Epitaxial Growth of Sr0.3Ba0.7Nb2O6 Thin Films Prepared by Sol-Gel Process

1999 ◽  
Vol 606 ◽  
Author(s):  
Keishi Nishio ◽  
Jirawat Thongrueng ◽  
Yuichi Watanabe ◽  
Toshio Tsuchiya
Keyword(s):  
Thin Film ◽  
Thin Films ◽  
Epitaxial Growth ◽  
Raw Materials ◽  
Substrate Surface ◽  
Sol Gel ◽  
Tungsten Bronze ◽  
Monomethyl Ether ◽  
Tetragonal Tungsten Bronze ◽  
Sol Gel Process

AbstructWe succeeded in the preparation of strontium-barium niobate (Sr0.3Ba0.7Nb2O6 : SBN30)that have a tetragonal tungsten bronze type structure thin films on SrTiO3 (100), STO, or La doped SrTiO3 (100), LSTO, single crystal substrates by a spin coating process. LSTO substrate can be used for electrode. A homogeneous coating solution was prepared with Sr and Ba acetates and Nb(OEt)5 as raw materials, and acetic acid and diethylene glycol monomethyl ether as solvents. The coating thin films were sintered at temperature from 700 to 1000°C for 10 min in air. It was confirmed that the thin films on STO substrate sintered above 700°C were in the epitaxial growth because the 16 diffraction spots were observed on the pole figure using (121) reflection. The <130> and <310> direction of the thin film on STO were oriented with the c-axis in parallel to the substrate surface. However, the diffraction spots of thin film on LSTO substrate sintered at 700°C were corresponds to the expected pattern for (110).

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