The reactions of arenesulphonyl azides with tetrahydropyrido[1,2-a]indoles and the X-ray crystallographic structure determination of a resultant novel zwitterion, 1,2,3,4-tetrahydro-10-methyl-4a-p-tolylsulphonylaminopyrido[1,2-a] indole

1979 ◽  
Vol 57 (5) ◽  
pp. 558-564 ◽  
Author(s):  
T. Stanley Cameron ◽  
Ruth E. Cordes ◽  
Aris Terzis ◽  
A. Sydney Bailey ◽  
Peter W. Scott

The reactions of arenesulphonyl azides with tetrahydropyrido[1,2-a]indoles have been examined. Compounds formed by elimination and by ring enlargement are obtained, including a compound with a novel zwitterion structure. The structure of this compound has been determined by X-ray crystallography.

2013 ◽  
Vol 88 ◽  
pp. 107-109 ◽  
Author(s):  
J.J. Nair ◽  
O.Q. Munro ◽  
M. Pošta ◽  
H.B. Papenfus ◽  
P. Beier ◽  
...  

Chemistry ◽  
2020 ◽  
Vol 2 (4) ◽  
pp. 796-804
Author(s):  
David John Watkin ◽  
Richard Ian Cooper

The Flack Parameter is now almost universally reported for all chiral materials characterized by X-ray crystallography. Its elegant simplicity was an inspired development by Howard Flack, and although the original algorithm for its computation has been strengthened by other workers, it remains an essential outcome for any crystallographic structure determination. As with any one-parameter metric, it needs to be interpreted in the context of its standard uncertainty.


1986 ◽  
Vol 51 (21) ◽  
pp. 3973-3978 ◽  
Author(s):  
Russell Rodrigo ◽  
Susan M. Knabe ◽  
Nicholas J. Taylor ◽  
Dayananda Rajapaksa ◽  
Michael J. Chernishenko

ChemInform ◽  
2010 ◽  
Vol 28 (24) ◽  
pp. no-no
Author(s):  
H. KAKUDA ◽  
T. SUZUKI ◽  
Y. TAKEUCHI ◽  
M. SHIRO

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