Structure of a product obtained on treatment of 1-thioacetoacetanilide with sulfuryl chloride

1970 ◽  
Vol 48 (16) ◽  
pp. 2632-2634 ◽  
Author(s):  
M. Curcumelli-Rodostamo ◽  
W. A. Harrison
Keyword(s):  
Infrared Spectrum ◽  
Thionyl Chloride ◽  
Sulfuryl Chloride ◽  
Resonance Structure ◽  
Crystalline Compound ◽  
Carbonyl Absorption

Treatment of 1-thioacetoacetanilide with sulfuryl chloride or thionyl chloride produced a crystalline compound identified as 3,5-diacetonylidene-4-phenyl-1,2,4-dithiazolidine. The absence of carbonyl absorption in the infrared spectrum of the compound indicated that it should be represented by a resonance structure (2) involving non-carbonyl components.

ChemInform Abstract: Sulfenylation Reactions Activated by Thionyl Chloride and Sulfuryl Chloride.

ChemInform ◽  
2010 ◽  
Vol 30 (15) ◽  
pp. no-no
Author(s):  
N. V. Zyk ◽  
E. K. Beloglazkina ◽  
I. D. Titanyuk
Keyword(s):  
Thionyl Chloride ◽  
Sulfuryl Chloride

Photoabsorption spectra of gaseous methyl bromide, ethylene dibromide, nitrosyl bromide, thionyl chloride, and sulfuryl chloride

1978 ◽  
Vol 82 (20) ◽  
pp. 2252-2257 ◽  
Author(s):  
A. P. Uthman ◽  
P. J. Demlein ◽  
T. D. Allston ◽  
M. C. Withiam ◽  
M. J. McClements ◽  
...  
Keyword(s):  
Thionyl Chloride ◽  
Methyl Bromide ◽  
Sulfuryl Chloride ◽  
Ethylene Dibromide

Infrared Spectra of Thionyl Chloride and Sulfuryl Chloride

1954 ◽  
Vol 22 (7) ◽  
pp. 1193-1195 ◽  
Author(s):  
Dowell E. Martz ◽  
Robert T. Lagemann
Keyword(s):  
Infrared Spectra ◽  
Thionyl Chloride ◽  
Sulfuryl Chloride
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