ELECTRON BEAM FLUORESCENCE PROBE FOR MEASURING THE LOCAL GAS DENSITY IN A WIDE FIELD OF OBSERVATION

1958 ◽  
Vol 36 (6) ◽  
pp. 659-671 ◽  
Author(s):  
B. W. Schumacher ◽  
E. O. Gadamer
Keyword(s):  
Electron Beam ◽  
Fluorescence Probe ◽  
Local Density ◽  
Unit Length ◽  
Three Dimensional ◽  
Light Output ◽  
Photometric Observation ◽  
Spectral Lines ◽  
Wide Field ◽  
Total Light

An electron beam was fired across the field of observation of the UTIA low-density wind tunnel. Along its path gaseous fluorescence was excited and visible light emitted. The total light output per unit length of the electron beam can be assumed to be proportional to the density of the gas if suitable spectral lines are selected. A three-dimensional scan of the field would give the local density for each spot. Visual, photographic, and photometric observation is possible. Some photographs are presented along with approximate data for the light output in air. The spatial resolution of the fluorescence probe is also discussed.

Voids in Quenched Nickel

1968 ◽  
Vol 26 ◽  
pp. 266-267
Author(s):  
J. J. Laidler
Keyword(s):  
Electron Beam ◽  
Ambient Temperature ◽  
Cooling Rate ◽  
Three Dimensional ◽  
Cooling Curve ◽  
Polycrystalline Nickel ◽  
Quenching Temperature ◽  
Long Tail ◽  
Diffusion Pump

The presence of three-dimensional voids in quenched metals has long been suspected, and voids have indeed been observed directly in a number of metals. These include aluminum, platinum, and copper, silver and gold. Attempts at the production of observable quenched-in defects in nickel have been generally unsuccessful, so the present work was initiated in order to establish the conditions under which such defects may be formed.Electron beam zone-melted polycrystalline nickel foils, 99.997% pure, were quenched from 1420°C in an evacuated chamber into a bath containing a silicone diffusion pump fluid . The pressure in the chamber at the quenching temperature was less than 10-5 Torr . With an oil quench such as this, the cooling rate is approximately 5,000°C/second above 400°C; below 400°C, the cooling curve has a long tail. Therefore, the quenched specimens are aged in place for several seconds at a temperature which continuously approaches the ambient temperature of the system.

Nanoscale Self-Assembly Using Ion and Electron Beam Techniques: A Rapid Review

MRS Advances ◽  
2020 ◽  
Vol 5 (64) ◽  
pp. 3507-3520
Author(s):  
Chunhui Dai ◽  
Kriti Agarwal ◽  
Jeong-Hyun Cho
Keyword(s):  
Electron Beam ◽  
Self Assembly ◽  
Ion Beam ◽  
Three Dimensional ◽  
The Self ◽  
Stress Generation ◽  
Rapid Review ◽  
High Yield ◽  
3D Nanostructures ◽  
Self Assembled

AbstractNanoscale self-assembly, as a technique to transform two-dimensional (2D) planar patterns into three-dimensional (3D) nanoscale architectures, has achieved tremendous success in the past decade. However, an assembly process at nanoscale is easily affected by small unavoidable variations in sample conditions and reaction environment, resulting in a low yield. Recently, in-situ monitored self-assembly based on ion and electron irradiation has stood out as a promising candidate to overcome this limitation. The usage of ion and electron beam allows stress generation and real-time observation simultaneously, which significantly enhances the controllability of self-assembly. This enables the realization of various complex 3D nanostructures with a high yield. The additional dimension of the self-assembled 3D nanostructures opens the possibility to explore novel properties that cannot be demonstrated in 2D planar patterns. Here, we present a rapid review on the recent achievements and challenges in nanoscale self-assembly using electron and ion beam techniques, followed by a discussion of the novel optical properties achieved in the self-assembled 3D nanostructures.

A Three-Dimensional Tetraphenylethylene-Based Fluorescence Covalent Organic Framework for Molecular Recognition

2020 ◽  
Author(s):  
Junxia Ren ◽  
Yaozu Liu ◽  
Xin Zhu ◽  
Yangyang Pan ◽  
Yujie Wang ◽  
...  
Keyword(s):  
Molecular Recognition ◽  
Fluorescence Probe ◽  
Three Dimensional ◽  
Hazardous Substances ◽  
Covalent Organic Framework ◽  
Highly Sensitive ◽  
Volatile Organic ◽  
Polycyclic Aromatic ◽  
Better Than ◽  
Organic Framework

<p><a></a><a></a><a></a><a></a><a></a><a></a><a></a><a>The development of highly-sensitive recognition of </a><a></a><a></a><a></a><a></a><a>hazardous </a>chemicals, such as volatile organic compounds (VOCs) and polycyclic aromatic hydrocarbons (PAHs), is of significant importance because of their widespread social concerns related to environment and human health. Here, we report a three-dimensional (3D) covalent organic framework (COF, termed JUC-555) bearing tetraphenylethylene (TPE) side chains as an aggregation-induced emission (AIE) fluorescence probe for sensitive molecular recognition.<a></a><a> </a>Due to the rotational restriction of TPE rotors in highly interpenetrated framework after inclusion of dimethylformamide (DMF), JUC-555 shows impressive AIE-based strong fluorescence. Meanwhile, owing to the large pore size (11.4 Å) and suitable intermolecular distance of aligned TPE (7.2 Å) in JUC-555, the obtained material demonstrates an excellent performance in the molecular recognition of hazardous chemicals, e.g., nitroaromatic explosives, PAHs, and even thiophene compounds, via a fluorescent quenching mechanism. The quenching constant (<i>K</i><sub>SV</sub>) is two orders of magnitude better than those of other fluorescence-based porous materials reported to date. This research thus opens 3D functionalized COFs as a promising identification tool for environmentally hazardous substances.</p>

scholarly journals Online Measurement of Deposit Surface in Electron Beam Freeform Fabrication

Sensors ◽  
2019 ◽  
Vol 19 (18) ◽  
pp. 4001 ◽  
Author(s):  
Shuhe Chang ◽  
Haoyu Zhang ◽  
Haiying Xu ◽  
Xinghua Sang ◽  
Li Wang ◽  
...  
Keyword(s):  
Electron Beam ◽  
3D Reconstruction ◽  
Three Dimensional ◽  
Thermal Conditions ◽  
Online Measurement ◽  
Three Dimensional Reconstruction ◽  
Continuous Change ◽  
Position Information ◽  
Freeform Fabrication ◽  
Dimensional Reconstruction

In the process of electron beam freeform fabrication (EBF3), due to the continuous change of thermal conditions and variability in wire feeding in the deposition process, geometric deviations are generated in the deposition of each layer. In order to prevent the layer-by-layer accumulation of the deviation, it is necessary to perform online geometry measurement for each deposition layer, based on which the error compensation can be done for the previous deposition layer in the next deposition layer. However, the traditional three-dimensional reconstruction method that employs structured laser cannot meet the requirements of long-term stable operation in the manufacturing process of EBF3. Therefore, this paper proposes a method to measure the deposit surfaces based on the position information of electron beam speckle, in which an electron beam is used to bombard the surface of the deposit to generate the speckle. Based on the structured information of the electron beam in the vacuum chamber, the three-dimensional reconstruction of the surface of the deposited parts is realized without need of additional structured laser sensor. In order to improve the detection accuracy, the detection error is theoretically analyzed and compensated. The absolute error after compensation is smaller than 0.1 mm, and the precision can reach 0.1%, which satisfies the requirements of 3D reconstruction of the deposited parts. An online measurement system is built for the surface of deposited parts in the process of electron beam freeform fabrication, which realizes the online 3D reconstruction of the surface of the deposited layer. In addition, in order to improve the detection stability of the whole system, the image processing algorithm suitable for this scene is designed. The reliability and speed of the algorithm are improved by ROI extraction, threshold segmentation, and expansion corrosion. In addition, the speckle size information can also reflect the thermal conditions of the surface of the deposited parts. Hence, it can be used for online detection of defects such as infusion and voids.

Gold Nanoparticle-Enhanced Laser-Induced Breakdown Spectroscopy and Three-Dimensional Contour Imaging of an Aluminum Alloy

2020 ◽  
pp. 000370282097304
Author(s):  
Amal A. Khedr ◽  
Mahmoud A. Sliem ◽  
Mohamed Abdel-Harith
Keyword(s):  
Gold Nanoparticles ◽  
Aluminum Alloy ◽  
Three Dimensional ◽  
Plasma Temperature ◽  
Spectral Lines ◽  
Laser Induced Breakdown Spectroscopy ◽  
Al Alloy ◽  
Boltzmann Plot ◽  
Breakdown Spectroscopy ◽  
Laser Induced Breakdown

In the present work, nanoparticle-enhanced laser-induced breakdown spectroscopy was used to analyze an aluminum alloy. Although LIBS has numerous advantages, it suffers from low sensitivity and low detection limits compared to other spectrochemical analytical methods. However, using gold nanoparticles helps to overcome such drawbacks and enhances the LIBS sensitivity in analyzing aluminum alloy in the current work. Aluminum was the major element in the analyzed samples (99.9%), while magnesium (Mg) was the minor element (0.1%). The spread of gold nanoparticles onto the Al alloy and using a laser with different pulse energies were exploited to enhance the Al alloy spectral lines. The results showed that Au NPs successfully improved the alloy spectral lines intensity by eight times, which could be useful for detecting many trace elements in higher matrix alloys. Under the assumption of local thermodynamic equilibrium, the Boltzmann plot was used to calculate the plasma temperature. Besides, the electron density was calculated using Mg and H lines at Mg(I) at 285.2 nm and Hα(I) at 656.2 nm, respectively. Three-dimensional contour mapping and color fill images contributed to understanding the behavior of the involved effects.

scholarly journals The relationship between photometric and spectroscopic oscillation amplitudes from 3D stellar atmosphere simulations

2021 ◽  
Author(s):  
Yixiao Zhou ◽  
Thomas Nordlander ◽  
Luca Casagrande ◽  
Meridith Joyce ◽  
Yaguang Li ◽  
...  
Keyword(s):  
Radial Velocity ◽  
Three Dimensional ◽  
Quantitative Relationship ◽  
Stellar Atmospheres ◽  
Spectral Lines ◽  
Wavelength Shift ◽  
The Sun ◽  
Theoretical Derivation ◽  
Velocity Amplitude ◽  
Good Agreement

Abstract We establish a quantitative relationship between photometric and spectroscopic detections of solar-like oscillations using ab initio, three-dimensional (3D), hydrodynamical numerical simulations of stellar atmospheres. We present a theoretical derivation as proof of concept for our method. We perform realistic spectral line formation calculations to quantify the ratio between luminosity and radial velocity amplitude for two case studies: the Sun and the red giant ε Tau. Luminosity amplitudes are computed based on the bolometric flux predicted by 3D simulations with granulation background modelled the same way as asteroseismic observations. Radial velocity amplitudes are determined from the wavelength shift of synthesized spectral lines with methods closely resembling those used in BiSON and SONG observations. Consequently, the theoretical luminosity to radial velocity amplitude ratios are directly comparable with corresponding observations. For the Sun, we predict theoretical ratios of 21.0 and 23.7 ppm/[m s−1] from BiSON and SONG respectively, in good agreement with observations 19.1 and 21.6 ppm/[m s−1]. For ε Tau, we predict K2 and SONG ratios of 48.4 ppm/[m s−1], again in good agreement with observations 42.2 ppm/[m s−1], and much improved over the result from conventional empirical scaling relations which gives 23.2 ppm/[m s−1]. This study thus opens the path towards a quantitative understanding of solar-like oscillations, via detailed modelling of 3D stellar atmospheres.

scholarly journals Performance of GaN-Based LEDs with Nanopatterned Indium Tin Oxide Electrode

2016 ◽  
Vol 2016 ◽  
pp. 1-7
Author(s):  
Zhanxu Chen ◽  
Wenjie Liu ◽  
Wei Wan ◽  
Gengyan Chen ◽  
Yongzhu Chen ◽  
...  
Keyword(s):  
Tin Oxide ◽  
Indium Tin Oxide ◽  
Ohmic Contacts ◽  
Three Dimensional ◽  
Light Output ◽  
Light Extraction Efficiency ◽  
Experimental Result ◽  
Indium Tin Oxide Electrode ◽  
Light Emitting ◽  
Ito Electrode

The indium tin oxide (ITO) has been widely applied in light emitting diodes (LEDs) as the transparent current spreading layer. In this work, the performance of GaN-based blue light LEDs with nanopatterned ITO electrode is investigated. Periodic nanopillar ITO arrays are fabricated by inductive coupled plasma etching with the mask of polystyrene nanosphere. The light extraction efficiency (LEE) of LEDs can be improved by nanopatterned ITO ohmic contacts. The light output intensity of the fabricated LEDs with nanopatterned ITO electrode is 17% higher than that of the conventional LEDs at an injection current of 100 mA. Three-dimensional finite difference time domain simulation matches well with the experimental result. This method may serve as a practical approach to improving the LEE of the LEDs.

scholarly journals A three-dimensional steady state thermal fluid model of jumbo ingot casting during electron beam re-melting of Ti–6Al–4V

2014 ◽  
Vol 38 (14) ◽  
pp. 3607-3623 ◽  
Author(s):  
X. Zhao ◽  
C. Reilly ◽  
L. Yao ◽  
D.M. Maijer ◽  
S.L. Cockcroft ◽  
...  
Keyword(s):  
Electron Beam ◽  
Steady State ◽  
Fluid Model ◽  
Three Dimensional ◽  
Ingot Casting

Local Density of States of a Three-Dimensional Conductor in the Extreme Quantum Limit

2001 ◽  
Vol 86 (8) ◽  
pp. 1582-1585 ◽  
Author(s):  
D. Haude ◽  
M. Morgenstern ◽  
I. Meinel ◽  
R. Wiesendanger
Keyword(s):  
Density Of States ◽  
Local Density ◽  
Three Dimensional ◽  
Quantum Limit ◽  
Local Density Of States
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