Studies on mixing. XX. Pumping effect of high-speed rotary mixers

1968 ◽  
Vol 33 (3) ◽  
pp. 836-849 ◽  
Author(s):  
I. Fořt ◽  
V. Sedláková
Keyword(s):  
1989 ◽  
Vol 54 (9) ◽  
pp. 2345-2356 ◽  
Author(s):  
Ivan Fořt ◽  
Jiří Hájek ◽  
Václav Machoň

The paper deals with the experimental study of the indicating particle circulation and the impeller power input in a liquid mechanically agitated with two high-speed impellers (combination of the standard turbine impeller and the six inclined (at 45°) plane blades impeller) on the same shaft in a slender vessel (its height is equal double of the vessel diameter) equipped with four radial baffles at its walls under the turbulent regime of agitated charge flow. By the visual method of the indicating particle it is examined its circulation in the lower part of the system pumping effect of the lower impeller), its circulation in the upper part of the system (pumping effect of the upper impeller), and the exchangeable circulation between the upper and lower part of the system and vice versa. The impeller power input is ascertained from the measured current electricity in the anchor of the direct current driving motor. It follows from the calculated energetic efficiency (the ratio of the cube of the sum of the impeller flow rate numbers and the sum of the impeller power numbers) of the investigated combinations of impellers that the highest value of this quantity is exhibited for two standard turbine impellers on the same shaft and for a combination of the lower standard turbine impeller and the upper impeller with inclined plane blades pumping upwards; slightly less value of the impeller energetic efficiency appears for the combination of two impellers with six inclined plane blades, the upper one pumps liquid upwards and the lower one downwards. For all the configurations the vertical distance of impellers on the same shaft has to be longer than the vessel diameter.


1987 ◽  
Vol 52 (11) ◽  
pp. 2640-2653 ◽  
Author(s):  
Ivan Fořt ◽  
Václav Machoň ◽  
Jiří Hájek ◽  
Eva Fialová

The paper deals with the experimental study of the indicating particle circulation in a liquid mechanically agitated with two high-speed impellers (two standard turbine impellers or a lower standard turbine and upper six inclined (at 45°) plane blade impeller) on the same shaft in a slender vessel (its height equals double of the vessel diameter) equipped with four radial baffles at its walls under the turbulent flow regime of agitated charge. The visual method of observation of the indicating particle is used to investigate the model system. Four types of the particle circulation are examined: its circulation in the lower part of the system (pumping effect of the lower impeller), its circulation in the upper part of the system (pumping effect of the upper impeller), and the exchangeable circulation between the upper and lower part of the system and vice versa. It follows from the obtained average data of the above-mentioned circulations that the homogeneous circulation of charge in the whole system is reached providing the vertical distance of the high-speed impellers is equal to at least double of their diameter, their pumping capacities being approximately double compared to those reached in the system with one impeller where the off-bottom liquid level height is equal to the vessel diameter. It follows from the comparison of two arrangements, when the upper high-speed impeller pumps liquid either upwards or downwards, that the homogeneous circulation of all the charge agitated is attained in the first of both the cases compared.


Author(s):  
E.D. Wolf

Most microelectronics devices and circuits operate faster, consume less power, execute more functions and cost less per circuit function when the feature-sizes internal to the devices and circuits are made smaller. This is part of the stimulus for the Very High-Speed Integrated Circuits (VHSIC) program. There is also a need for smaller, more sensitive sensors in a wide range of disciplines that includes electrochemistry, neurophysiology and ultra-high pressure solid state research. There is often fundamental new science (and sometimes new technology) to be revealed (and used) when a basic parameter such as size is extended to new dimensions, as is evident at the two extremes of smallness and largeness, high energy particle physics and cosmology, respectively. However, there is also a very important intermediate domain of size that spans from the diameter of a small cluster of atoms up to near one micrometer which may also have just as profound effects on society as “big” physics.


Author(s):  
N. Yoshimura ◽  
K. Shirota ◽  
T. Etoh

One of the most important requirements for a high-performance EM, especially an analytical EM using a fine beam probe, is to prevent specimen contamination by providing a clean high vacuum in the vicinity of the specimen. However, in almost all commercial EMs, the pressure in the vicinity of the specimen under observation is usually more than ten times higher than the pressure measured at the punping line. The EM column inevitably requires the use of greased Viton O-rings for fine movement, and specimens and films need to be exchanged frequently and several attachments may also be exchanged. For these reasons, a high speed pumping system, as well as a clean vacuum system, is now required. A newly developed electron microscope, the JEM-100CX features clean high vacuum in the vicinity of the specimen, realized by the use of a CASCADE type diffusion pump system which has been essentially improved over its predeces- sorD employed on the JEM-100C.


Author(s):  
William Krakow

In the past few years on-line digital television frame store devices coupled to computers have been employed to attempt to measure the microscope parameters of defocus and astigmatism. The ultimate goal of such tasks is to fully adjust the operating parameters of the microscope and obtain an optimum image for viewing in terms of its information content. The initial approach to this problem, for high resolution TEM imaging, was to obtain the power spectrum from the Fourier transform of an image, find the contrast transfer function oscillation maxima, and subsequently correct the image. This technique requires a fast computer, a direct memory access device and even an array processor to accomplish these tasks on limited size arrays in a few seconds per image. It is not clear that the power spectrum could be used for more than defocus correction since the correction of astigmatism is a formidable problem of pattern recognition.


Author(s):  
C. O. Jung ◽  
S. J. Krause ◽  
S.R. Wilson

Silicon-on-insulator (SOI) structures have excellent potential for future use in radiation hardened and high speed integrated circuits. For device fabrication in SOI material a high quality superficial Si layer above a buried oxide layer is required. Recently, Celler et al. reported that post-implantation annealing of oxygen implanted SOI at very high temperatures would eliminate virtually all defects and precipiates in the superficial Si layer. In this work we are reporting on the effect of three different post implantation annealing cycles on the structure of oxygen implanted SOI samples which were implanted under the same conditions.


Author(s):  
Z. Liliental-Weber ◽  
C. Nelson ◽  
R. Ludeke ◽  
R. Gronsky ◽  
J. Washburn

The properties of metal/semiconductor interfaces have received considerable attention over the past few years, and the Al/GaAs system is of special interest because of its potential use in high-speed logic integrated optics, and microwave applications. For such materials a detailed knowledge of the geometric and electronic structure of the interface is fundamental to an understanding of the electrical properties of the contact. It is well known that the properties of Schottky contacts are established within a few atomic layers of the deposited metal. Therefore surface contamination can play a significant role. A method for fabricating contamination-free interfaces is absolutely necessary for reproducible properties, and molecularbeam epitaxy (MBE) offers such advantages for in-situ metal deposition under UHV conditions


Author(s):  
Brian Cross

A relatively new entry, in the field of microscopy, is the Scanning X-Ray Fluorescence Microscope (SXRFM). Using this type of instrument (e.g. Kevex Omicron X-ray Microprobe), one can obtain multiple elemental x-ray images, from the analysis of materials which show heterogeneity. The SXRFM obtains images by collimating an x-ray beam (e.g. 100 μm diameter), and then scanning the sample with a high-speed x-y stage. To speed up the image acquisition, data is acquired "on-the-fly" by slew-scanning the stage along the x-axis, like a TV or SEM scan. To reduce the overhead from "fly-back," the images can be acquired by bi-directional scanning of the x-axis. This results in very little overhead with the re-positioning of the sample stage. The image acquisition rate is dominated by the x-ray acquisition rate. Therefore, the total x-ray image acquisition rate, using the SXRFM, is very comparable to an SEM. Although the x-ray spatial resolution of the SXRFM is worse than an SEM (say 100 vs. 2 μm), there are several other advantages.


Author(s):  
J. E. Johnson

In the early years of biological electron microscopy, scientists had their hands full attempting to describe the cellular microcosm that was suddenly before them on the fluorescent screen. Mitochondria, Golgi, endoplasmic reticulum, and other myriad organelles were being examined, micrographed, and documented in the literature. A major problem of that early period was the development of methods to cut sections thin enough to study under the electron beam. A microtome designed in 1943 moved the specimen toward a rotary “Cyclone” knife revolving at 12,500 RPM, or 1000 times as fast as an ordinary microtome. It was claimed that no embedding medium was necessary or that soft embedding media could be used. Collecting the sections thus cut sounded a little precarious: “The 0.1 micron sections cut with the high speed knife fly out at a tangent and are dispersed in the air. They may be collected... on... screens held near the knife“.


Author(s):  
N. David Theodore ◽  
Donald Y.C Lie ◽  
J. H. Song ◽  
Peter Crozier

SiGe is being extensively investigated for use in heterojunction bipolar-transistors (HBT) and high-speed integrated circuits. The material offers adjustable bandgaps, improved carrier mobilities over Si homostructures, and compatibility with Si-based integrated-circuit manufacturing. SiGe HBT performance can be improved by increasing the base-doping or by widening the base link-region by ion implantation. A problem that arises however is that implantation can enhance strain-relaxation of SiGe/Si.Furthermore, once misfit or threading dislocations result, the defects can give rise to recombination-generation in depletion regions of semiconductor devices. It is of relevance therefore to study the damage and anneal behavior of implanted SiGe layers. The present study investigates the microstructural behavior of phosphorus implanted pseudomorphic metastable Si0.88Ge0.12 films on silicon, exposed to various anneals.Metastable pseudomorphic Si0.88Ge0.12 films were grown ~265 nm thick on a silicon wafer by molecular-beam epitaxy. Pieces of this wafer were then implanted at room temperature with 100 keV phosphorus ions to a dose of 1.5×1015 cm-2.


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