Intragranular three-dimensional stress tensor fields in plastically deformed polycrystals

Science ◽  
2019 ◽  
Vol 366 (6472) ◽  
pp. 1492-1496 ◽  
Author(s):  
Yujiro Hayashi ◽  
Daigo Setoyama ◽  
Yoshiharu Hirose ◽  
Tomoyuki Yoshida ◽  
Hidehiko Kimura

The failure of polycrystalline materials used in infrastructure and transportation can be catastrophic. Multiscale modeling, which requires multiscale measurements of internal stress fields, is the key to predicting the deformation and failure of alloys. We determined the three-dimensional intragranular stress tensor fields in plastically deformed bulk steel using a high-energy x-ray microbeam. We observed intragranular local stresses that deviated greatly from the grain-averaged stresses and exceeded the macroscopic tensile strength. Even under deformation smaller than the uniform elongation, the intragranular stress fields were in highly triaxial stress states, which cannot be determined from the grain-averaged stresses. The ability to determine intragranular stress tensor fields can facilitate the understanding and prediction of the deformation and failure of materials through multiscale modeling.

2021 ◽  
Author(s):  
Yusuke Shimada ◽  
Shinnosuke Tokuta ◽  
Akinori Yamanaka ◽  
Akiyasu Yamamoto ◽  
Toyohiko. J Konno

Abstract In iron-based superconductors, randomly oriented grain boundaries have a strong influence on the transport properties via intrinsic weak-link and flux pinning mechanisms. Herein we report the critical current density (Jc) and the three-dimensional microstructure of polycrystalline bulk Co-doped Ba122 superconductors, with highly dense grain boundaries (grain size smaller than 50 nm), produced by high-energy milling. Three-dimensional electron microscopy revealed that the anomalous growth of secondary particles (aggregation) and the inter-aggregation structures were significantly different in the samples with finer grains, which may have extrinsically limited Jc. These important microstructural features were quantified as two parameters—local thickness and total pore length—by reconstructing the three-dimensional structure of the superconducting phase using the adaptive thresholding method. The results obtained in this study suggest that understanding and controlling the microstructural formation process by sintering are instrumental for improving the Jc properties of 122 polycrystalline materials consisting of ultrafine grains.


MRS Bulletin ◽  
2004 ◽  
Vol 29 (3) ◽  
pp. 166-169 ◽  
Author(s):  
Henning F. Poulsen ◽  
Dorte Juul Jensen ◽  
Gavin B.M. Vaughan

AbstractThree-dimensional x-ray diffraction (3DXRD) microscopy is a tool for fast and nondestructive characterization of the individual grains, subgrains, and domains inside bulk materials. The method is based on diffraction with very penetrating hard x-rays (E ≥ 50 keV), enabling 3D studies of millimeter-to-centimeter-thick specimens.The position, volume, orientation, and elastic and plastic strain can be derived for hundreds of grains simultaneously. Furthermore, by applying novel reconstruction methods, 3D maps of the grain boundaries can be generated. The 3DXRD microscope in use at the European Synchrotron Radiation Facility in Grenoble, France, has a spatial resolution of ∼5 μm and can detect grains as small as 150 nm. The technique enables, for the first time, dynamic studies of the individual grains within polycrystalline materials. In this article, some fundamental materials science applications of 3DXRD are reviewed: studies of nucleation and growth kinetics during recrystallization, recovery, and phase transformations, as well as studies of polycrystal deformation.


Author(s):  
Joel V. Bernier ◽  
Matthew P. Miller ◽  
Jun-Sang Park ◽  
Ulrich Lienert

Quantitative strain analysis (QSA) provides a means for assessing the orientation-dependent micromechanical stress states in bulk polycrystalline materials. When combined with quantitative texture analysis, it facilitates tracking the evolution of micromechanical states associated with selected texture components for specimens deformed in situ. To demonstrate this ability, a sheet specimen of rolled and recrystallized oxygen-free high conductivity Cu was subject to tensile deformation at APS 1-ID-C. Strain pole figures (SPFs) were measured at a series of applied loads, both below and above the onset of macroscopic yielding. From these data, a lattice strain distribution function (LSDF) was calculated for each applied load. Due to the tensorial nature of the LSDF, the full orientation-dependent stress tensor fields can be calculated unambiguously from the single-crystal elastic moduli. The orientation distribution function (ODF) is used to calculate volume-weighted average stress states over tubular volumes centered on the ⟨100⟩∥[100], ⟨311⟩∥[100], and ⟨111⟩∥[100] fibers—accounting for ≈50% of the total volume—are shown as functions of the applied load along [100]. Corresponding weighted standard deviations are calculated as well. Different multiaxial stress states are observed to develop in the crystal subpopulations despite the uniaxial nature of the applied stress. The evolution of the orientation-dependent elastic strain energy density is also examined. The effects of applying stress bound constraints on the SPF inversion are discussed, as are extensions of QSA to examine defect nucleation and propagation.


Author(s):  
R. Craig McClung ◽  
Michael P. Enright ◽  
Yi-Der Lee ◽  
Luc J. Huyse ◽  
Simeon H. K. Fitch

Many high-energy turbine engine components are fracture critical. However, the complex three-dimensional (3d) geometries and stress fields associated with these components can make accurate fracture analysis impractical. This paper describes a new computational approach to efficient fracture design for complex turbine engine components. The approach employs a powerful 3D graphical user interface (GUI) for manipulation of geometry models and calculated component stresses to formulate simpler 2D fracture models. New weight function stress intensity factor solutions are derived to address stress gradients that vary in all directions on the fracture plane.


2017 ◽  
Vol 905 ◽  
pp. 157-164 ◽  
Author(s):  
Yujiro Hayashi ◽  
Daigo Setoyama ◽  
Yoshiki Seno

The grain-resolved residual stress (type II) in commercial-quality low carbon steel was observed using scanning three-dimensional X-ray diffraction (3DXRD) microscopy. In this method, grain orientations and lattice parameters are mapped using a monochromatic high-energy X-ray microbeam and 3DXRD-based polycrystalline indexing. Defining the reference lattice parameter a0 as the average value in the entire field of view, grain orientations and lattice parameters are converted into stress tensors, yielding a grain-resolved stress tensor map. The effectiveness of the scanning 3DXRD method was demonstrated by evaluating the residual stress in a cold-rolled low carbon steel sheet using a 50 keV microbeam at SPring-8. The area of the cross-sectional sample was 1×1 mm2, which was sufficiently larger than the grain size of about 20 μm. To produce a two-dimensional map of a circular region with a diameter of 160 μm at a pixel size of 1×1 μm2, the measurement time was about 1 h. From the stress tensor map, differences in residual stress of about 150–200 MPa between some neighboring grains were observed.


1989 ◽  
Vol 111 (2) ◽  
pp. 136-150 ◽  
Author(s):  
J. T. Pindera

The paper presents a theoretical framework of a more comprehensive methodology of analysis of behavior of homogeneous and composite materials and structures. The behavior of bolted flanged connections is taken as an illustrative example. Particular attention is given to the local effects. The term “local effects” denotes the actual, pronounced local three-dimensional stress states which exist in particular regions of the actual, weakly three-dimensional, stress fields occurring in plates and shells. Presented examples show that the local effects can be one of the major causes of failures of homogeneous or composite laminated structures. Within the chosen theoretical framework, an outline of new analytical/experimental methods is presented, called isodyne methods. It is demonstrated that the isodyne methods allow the determination of the normal and shear components of the stress states in plates and beams, including the three-dimensional stress states at the crack tips, tips of local disbounds or defects, or in the lamination planes.


1984 ◽  
Vol 106 (1) ◽  
pp. 48-54 ◽  
Author(s):  
R. J. Stango ◽  
S. S. Wang

A study of process-induced stresses in advanced fiber-reinforced composite laminates is presented. An analysis of the residual thermal stresses is conducted on the basis of laminate thermoelasticity theory in conjunction with a quasi-three-dimensional finite element method. Formulation of the numerical method is briefly outlined in the paper. To illustrate the fundamental nature of the problem, numerical examples for a quasi-isotropic [0 deg/90 deg/ ± 45 deg]s graphite-epoxy composite system are presented. Complex three-dimensional stress states of significant magnitude are reported. Emphasis is placed on the interlaminar stress distributions along ply interfaces. Effects of laminate stacking sequence on the residual thermal stresses are examined in detail. Implications of the results on deformation and failure of composite laminates are discussed.


2000 ◽  
Vol 15 (15) ◽  
pp. 2269-2288
Author(s):  
SANATAN DIGAL ◽  
RAJARSHI RAY ◽  
SUPRATIM SENGUPTA ◽  
AJIT M. SRIVASTAVA

We demonstrate the possibility of forming a single, large domain of disoriented chiral condensate (DCC) in a heavy-ion collision. In our scenario, rapid initial heating of the parton system provides a driving force for the chiral field, moving it away from the true vacuum and forcing it to go to the opposite point on the vacuum manifold. This converts the entire hot region into a single DCC domain. Subsequent rolling down of the chiral field to its true vacuum will then lead to emission of a large number of (approximately) coherent pions. The requirement of suppression of thermal fluctuations to maintain the (approximate) coherence of such a large DCC domain, favors three-dimensional expansion of the plasma over the longitudinal expansion even at very early stages of evolution. This also constrains the maximum temperature of the system to lie within a window. We roughly estimate this window to be about 200–400 MeV. These results lead us to predict that extremely high energy collisions of very small nuclei (possibly hadrons) are better suited for observing signatures of a large DCC. Another possibility is to focus on peripheral collisions of heavy nuclei.


2020 ◽  
Vol 15 (S359) ◽  
pp. 178-179
Author(s):  
Saqib Hussain ◽  
Rafael Alves Batista ◽  
Elisabete Maria de Gouveia Dal Pino ◽  
Klaus Dolag

AbstractWe present results of the propagation of high-energy cosmic rays (CRs) and their secondaries in the intracluster medium (ICM). To this end, we employ three-dimensional cosmological magnetohydrodynamical simulations of the turbulent intergalactic medium to explore the propagation of CRs with energies between 1014 and 1019 eV. We study the interaction of test particles with this environment considering all relevant electromagnetic, photohadronic, photonuclear, and hadronuclear processes. Finally, we discuss the consequences of the confinement of high-energy CRs in clusters for the production of gamma rays and neutrinos.


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