scholarly journals Observation of electron-induced characteristic x-ray and bremsstrahlung radiation from a waveguide cavity

2021 ◽  
Vol 7 (4) ◽  
pp. eabd5677
Author(s):  
Malte Vassholz ◽  
Tim Salditt

We demonstrate x-ray generation based on direct emission of spontaneous x-rays into waveguide modes. Photons are generated by electron impact onto a structured anode target, which is formed as an x-ray waveguide or waveguide array. Both emission of characteristic radiation and bremsstrahlung are affected by the changes in mode density induced by the waveguide structure. We investigate how the excited modal pattern depends on the positions of the metal atoms and the distance of the focused electron beam with respect to the waveguide exit side. We compare the results to synchrotron-excited fluorescence. We then discuss how x-ray generation in waveguides can be used to increase the brilliance and directional emission of tabletop x-ray sources, with a corresponding increase in the spatial coherence. On the basis of the Purcell effect, we lastly show that the gain of emission into waveguide modes is governed by the quality factor of the waveguide.

Author(s):  
Werner P. Rehbach ◽  
Peter Karduck

In the EPMA of soft x rays anomalies in the background are found for several elements. In the literature extremely high backgrounds in the region of the OKα line are reported for C, Al, Si, Mo, and Zr. We found the same effect also for Boron (Fig. 1). For small glancing angles θ, the background measured using a LdSte crystal is significantly higher for B compared with BN and C, although the latter are of higher atomic number. It would be expected, that , characteristic radiation missing, the background IB (bremsstrahlung) is proportional Zn by variation of the atomic number of the target material. According to Kramers n has the value of unity, whereas Rao-Sahib and Wittry proposed values between 1.12 and 1.38 , depending on Z, E and Eo. In all cases IB should increase with increasing atomic number Z. The measured values are in discrepancy with the expected ones.


2019 ◽  
Vol 26 (3) ◽  
pp. 756-761
Author(s):  
Yoko Takeo ◽  
Hiroto Motoyama ◽  
Yasunori Senba ◽  
Hikaru Kishimoto ◽  
Haruhiko Ohashi ◽  
...  

Probing the spatial coherence of X-rays has become increasingly important when designing advanced optical systems for beamlines at synchrotron radiation sources and free-electron lasers. Double-slit experiments at various slit widths are a typical method of quantitatively measuring the spatial coherence over a wide wavelength range including the X-ray region. However, this method cannot be used for the analysis of spatial coherence when the two evaluation points are separated by a large distance of the order of millimetres owing to the extremely narrow spacing between the interference fringes. A Fresnel-mirror-based optical system can produce interference patterns by crossing two beams from two small mirrors separated in the transverse direction to the X-ray beam. The fringe spacing can be controlled via the incidence angles on the mirrors. In this study, a Fresnel-mirror-based optical system was constructed at the soft X-ray beamline (BL25SU) of SPring-8. The relationship between the coherence and size of the virtual source was quantitatively measured at 300 eV in both the vertical and horizontal directions using the beam. The results obtained indicate that this is a valuable method for the optimization of optical systems along beamlines.


2015 ◽  
Vol 22 (3) ◽  
pp. 796-800 ◽  
Author(s):  
Alexander Goikhman ◽  
Ivan Lyatun ◽  
Petr Ershov ◽  
Irina Snigireva ◽  
Pawel Wojda ◽  
...  

This paper reports a special device called a `speckle suppressor', which contains a highly porous nanoberyllium plate squeezed between two beryllium windows. The insertion of the speckle suppressor in an X-ray beam allows manipulation of the spatial coherence length, thus changing the effective source size and removing the undesirable speckle structure in X-ray imaging experiments almost without beam attenuation. The absorption of the nanoberyllium plate is below 1% for 1 mm thickness at 12 keV. The speckle suppressor was tested on the ID06 ESRF beamline with X-rays in the energy range from 9 to 15 keV. It was applied for the transformation of the phase–amplitude contrast to the pure amplitude contrast in full-field microscopy.


1995 ◽  
Vol 39 ◽  
pp. 81-86
Author(s):  
N. Gao ◽  
I. Ponomarev ◽  
Q. F. Xiao ◽  
W. M. Gibson ◽  
D. A. Carpenter

Simulation and experimental work that compare the performance of straight and tapered monocapillaries when used with laboratory x-ray sources are reported. Detailed simulations for various taper profiles give several important conclusions for optimizing the design of a tapered monocapillary. Several tapered monocapillaries were prepared. With a 16W x-ray source, beam intensities of 4×105 photon/sec/μm2 and 3×105photon/sec/μm2 of Cu Kα x rays were obtained from the tapered monocapillaries for output diameters of 8μm and 3.5μm, respectively. These intensities are 1.4 and 1.5 times that obtained from straight capillaries with the same output beam sizes at the experimental set-up optimized for a straight capillary. In addition to the gain in x-ray flux, the tapered monocapillaries produce output beams with significantly reduced high energy bremsstrahlung radiation and increased flux stability with respect to shifts of the x-ray source spot.


A considerable amount of work has been done by various experimenters showing that, when an element of higher atomic weight than calcium is subjected to a suitable primary beam of X-rays, the rays which leave the radiator consist of two types: firstly, the purely scattered radiation, which is almost exactly similar to the incident beam, and, secondly, a characteristic homogeneous radiation. The scattered radiation which in the case of a primary beam from an X-ray bulb is heterogeneous, is, with elements of low atomic weight, quite small in intensity when compared with the intensity of the homogeneous radiation which is emitted simultaneously. Owing to this fact, it is comparatively easy to prove that the elements with atomic weights between that of calcium and cerium give off when stimulated with X-rays homogeneous beams, and the hardness of the characteristic radiation from each of these elements has been measured by determining the absorption in aluminium. The radiations are usually defined by the value ok their absorption coefficients, that is, by λ/ρ where I = I 0 e -λx ; ρ = density of aluminium. Using the values obtained, it is possible to plot a curve showing the relation between atomic weight and λ/ρ for the elements which emit a characteristic radiation, taking atomic weight as abscissa and λ/ρ for ordinates. If this is done, it will be found that the elements with atomic weights between that of calcium and cerium lie on an approximately smooth curve (Group K). When, however, the elements with higher atomic weight than silver are examined under suitable conditions, it is found that, with these elements, there are two distinct types of radiations: one, a hard characteristic radiations such as belongs to Group K, and superposed on this a very soft radiation. Prof. Barkla and Mr. Nicol have investigated the soft radiations from the elements silver, antimony, iodine, and barium, and have shown that these elements, in addition to the usual characteristic radiation, emit another very soft radiation, which is also characteristic of the element. The values of the λ/ρ for these elements have been determined, and it has been shown, as far as it is possible with such soft rays, that they are homogeneous. If these values are plotted on the same diagram as that mentioned above, a second short curve is obtained, which can be continued to the X axis; when this is done, if this second curve resembles in shape the curve for Group K, it will pass before it reaches the X axis through the region of atomic weights between 184 and 238. which contains tubgsteb, gold, platinum, lead, bismuth, thorium, and uranium. This second series of elements has been designated Group L. Up to the present it has been impossible to draw this curve with any accuracy, as none of the elements between tungsten and uranium have been investigated as regards their X-ray properties.


1996 ◽  
Vol 74 (1-2) ◽  
pp. 10-16 ◽  
Author(s):  
D. V. Rao ◽  
R. Cesareo ◽  
G. E. Gigante ◽  
D. V. Rao ◽  
G. E. Gigante

Coherent- and incoherent-scattering cross sections for the elements Al, Cu, Y, In, Au, and Pb were measured using nearly monoenergetic unpolarized 35.86 and 39.96 keV X-ray beams with high-resolution Si (Li) detectors. Bremsstrahlung radiation from an X-ray tube was used to excite nearly monoenergetic X-rays in secondary targets. To improve the efficiency of the detection system the excitation source, detector, and the target assembly were placed in a vacuum chamber and a pressure of 10−2 mbar was maintained throughout the measurements. This system considerably reduced the background and scattering effects and improved the monochromacy. Experimental coherent-scattering cross sections are compared with the normalized integrated coherent-scattering cross sections calculated using the relativistic, nonrelativistic, and relativistic-modified form factors. Experimental incoherent-scattering cross sections are compared with the theoretical values, calculated using the nonrelativistic incoherent-scattering function. Good correspondence is observed between experimental and theoretical values in the given energy region.


Author(s):  
E. A. Kenik ◽  
J. Bentley

The spatial resolution and accuracy of X-ray microanalysis in an analytical electron microscope (AEM) are limited by a variety of factors, two of which are the hole count and secondary fluorescence. The hole count arises from uncollimated radiation, either electrons or X rays, which excites areas of the specimen other than that excited by the primary electron beam. This can result in X-ray generation even when the probe does not hit the specimen; hence the name hole count. Secondary fluorescence deals with X-ray generation resulting from radiation produced by the interaction of the incident probe with the specimen. This radiation may be either backscattered electrons spiraling in the magnetic field of the objective lens or high energy X rays, particularly forward-peaked bremsstrahlung radiation. As the interaction of both the uncollimated radiation and the secondary radiation with the specimen can be influenced by the tilt angle of the specimen, the variation of the hole count and secondary fluorescence with specimen tilt was investigated.


1999 ◽  
Vol 17 (1) ◽  
pp. 45-58 ◽  
Author(s):  
YUTAKA UESHIMA ◽  
YASUAKI KISHIMOTO ◽  
AKIRA SASAKI ◽  
TOSHIKI TAJIMA

A relativistically intense short laser pulse can produce a large flux of X rays through the interaction with electrons that are driven by its intense electromagnetic fields. Apart from X rays from the high-Z matter irradiation by an intense laser, two main processes, Larmor and Bremsstrahlung radiation, are among the most significant mechanisms for X-ray emission from short-pulse laser irradiation on low-Z matter in the regime of relativistic intensities. We evaluate the power, energy spectrum, brilliance, polarization, and time structure of these X rays. We suggest a few methods that significantly enhance the power of Larmor X rays. Because of the peakedness in the energy spectrum of Larmor X rays, Larmor X rays have important applications.


1984 ◽  
Vol 28 ◽  
pp. 69-74 ◽  
Author(s):  
Peter Wobrauschek ◽  
Hannes Aiginger

AbstractPolarized x-rays are used to excite samples of any kind and shape to emit characteristic radiation. In the appropriate geometry, where source-sample-ED detector are in any orthogonal position to each other, the exciting poLarized x-rays will be practically not scattered from sample and substrate into the detector. This reduces the background considerably and hence improves the lower limits of detection. The production of intensive polarized x-rays is done by using a single crystal-where Bragg reflection occurs at an angle 2 θ = 90° instead of amorphous low Z scatterers. The result is a linear polarized and monochromatic beam. The use of curved crystals instead of plane single crystals further increases the intensity of the exciting radiation. The lower limits of detection attainable with the recently constructed compact polarizer device are in the sub ppm range or in absolute amounts around 150 pg for medium Z elements.


2018 ◽  
Vol 282 ◽  
pp. 309-313
Author(s):  
Rikiichi Ohno ◽  
Koichiro Saga

We have found that to the detection sensitivity of Total reflection X-ray fluorescent spectrometry (TXRF), the total volume of trace particles generated by vapor phase treatment (VPT) must be increased and metal atoms need to be included in the particles. The detection sensitivity for Cu is enhanced by assisting Cu ionization in the liquid drops condensed form the vapor. We consider that since incident and reflected X-rays resonate 30nm from the surface, the total reflection intensity of metals included in the particles is enhanced.


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