The use of optical methods for measuring irregular reflection of weak acoustic shock pulses from a solid surface in air

2017 ◽  
Vol 141 (5) ◽  
pp. 3730-3730
Author(s):  
Maria M. Karzova ◽  
Petr V. Yuldashev ◽  
Didier Dragna ◽  
Sébastien Ollivier ◽  
Vera Khokhlova ◽  
...  
2019 ◽  
Vol 145 (1) ◽  
pp. 26-35 ◽  
Author(s):  
Maria M. Karzova ◽  
Thomas Lechat ◽  
Sébastien Ollivier ◽  
Didier Dragna ◽  
Petr V. Yuldashev ◽  
...  

2016 ◽  
Vol 139 (4) ◽  
pp. 2207-2207
Author(s):  
Desjouy Cyril ◽  
Sébastien Ollivier ◽  
Olivier Marsden ◽  
Didier Dragna ◽  
Maria Karzova ◽  
...  

2016 ◽  
Vol 28 (2) ◽  
pp. 027102 ◽  
Author(s):  
Cyril Desjouy ◽  
Sébastien Ollivier ◽  
Olivier Marsden ◽  
Maria Karzova ◽  
Philippe Blanc-Benon

Author(s):  
A. Legrouri

The industrial importance of metal catalysts supported on reducible oxides has stimulated considerable interest during the last few years. This presentation reports on the study of the physicochemical properties of metallic rhodium supported on vanadium pentoxide (Rh/V2O5). Electron optical methods, in conjunction with other techniques, were used to characterise the catalyst before its use in the hydrogenolysis of butane; a reaction for which Rh metal is known to be among the most active catalysts.V2O5 powder was prepared by thermal decomposition of high purity ammonium metavanadate in air at 400 °C for 2 hours. Previous studies of the microstructure of this compound, by HREM, SEM and gas adsorption, showed it to be non— porous with a very low surface area of 6m2/g3. The metal loading of the catalyst used was lwt%Rh on V2Q5. It was prepared by wet impregnating the support with an aqueous solution of RhCI3.3H2O.


Author(s):  
H. Seiler ◽  
U. Haas ◽  
K.H. Körtje

The physical properties of small metal particles reveal an intermediate position between atomic and bulk material. Especially Ag has shown pronounced size effects. We compared silver layers evaporated in high vacuum with cluster layers of small silver particles, evaporated in N2 at a pressure of about 102 Pa. The investigations were performed by electron optical methods (TEM, SEM, EELS) and by Photoacoustic (PA) Spectroscopy (gas-microphone detection).The observation of cluster layers with TEM and high resolution SEM show small silver particles with diameters of about 50 nm (Fig. 1 and Figure 2, respectively). The electron diffraction patterns of homogeneous Ag layers and of cluster layers are similar, whereas the low loss EELS spectra due to plasmon excitation are quite different. Fig. 3 and Figure 4 show first results of EELS spectra of a cluster layer of small silver particles on carbon foil and of a homogeneous Ag layer, respectively.


2020 ◽  
pp. 49-56
Author(s):  
Vitaly V. Volkov ◽  
Michael A. Suslin ◽  
Jamil U. Dumbolov

One of the conditions for ensuring the safety of air transport operation is the quality of aviation fuel refueled in aircraft. Fuel quality control is a multi-parameter task that includes monitoring the free moisture content. Regulatory documents establish the content of free water no more than 0.0015% by weight. It is developed a direct electrometric microwave resonance method for controlling free moisture in aviation fuels, which consists in changing the shape of the water drops by pressing them on a solid surface inside a cylindrical cavity resonator. This can dramatically increase dielectric losses. Analytical and experimental analysis of the proposed method is carried out. The control range from 0,5 to 30 μl of absolute volume of moisture in aviation fuels with a maximum error of not morethan 25 % is justified. The sensitivity of the proposed method for monitoring microwave losses in free moisture drops transformed into a thin layer by pressing is an order of magnitude greater than the sensitivity of the method for monitoring microwave losses in moisture drops on a solid surface in a resonator. The proposed method can be used as a basis for the development of devices for monitoring the free moisture of aviation fuels in the conditions of the airfield and laboratory. The direction of development of the method is shown.


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