A comparative study of x-ray phase micro-tomography: grating based technique vs. high-energy propagation based technique

2017 ◽  
Author(s):  
Huiqiang Liu ◽  
Xizeng Wu ◽  
Tiqiao Xiao
Keyword(s):  
Comparative Study ◽  
High Energy ◽  
Energy Propagation ◽  
X Ray ◽  
Micro Tomography

scholarly journals The comparative study of measurements of high energy x-ray beams, using solid phantoms.

1996 ◽  
Vol 52 (10) ◽  
pp. 1451
Author(s):  
Koji Yamashita ◽  
Ikuo Ikeda ◽  
Hiromi Ikezaki ◽  
Norikazu Shimizu ◽  
Shinji Kiuchi
Keyword(s):  
Comparative Study ◽  
High Energy ◽  
X Ray ◽  
The Comparative Study

The New GKSS Materials Science Beamlines at DESY: Recent Results and Future Options

2010 ◽  
Vol 638-642 ◽  
pp. 2470-2475 ◽  
Author(s):  
Peter Staron ◽  
Norbert Schell ◽  
Astrid Haibel ◽  
Felix Beckmann ◽  
Thomas Lippmann ◽  
...  
Keyword(s):  
Residual Stress ◽  
High Resolution ◽  
Materials Science ◽  
High Energy ◽  
Energy Materials ◽  
X Ray ◽  
High Energy Materials ◽  
X Ray Scattering ◽  
Residual Stress Analysis ◽  
Micro Tomography

GKSS is currently investing heavily into new beamlines at DESY in Hamburg, Germany. After the completed installation of the wiggler beamline HARWI II at DORIS III GKSS is now building two new undulator beamlines at the new PETRA III storage ring. The High Energy Materials Science Beamline (HEMS) will allow high resolution diffraction experiments using samples and sample environments with masses up to 1 t, 3DXRD measurements, and high-energy micro-tomography experiments. The Imaging Beamline (IBL) will provide a nano-tomography as well as a micro-tomography station for X-ray energies up to 50 keV. Examples of typical experiments in the field of residual stress analysis, micro-tomography, and high-energy small-angle X-ray scattering will be given.

scholarly journals High Energy X-ray Micro-tomography for the characterization of thermally fatigued GlidCop specimen

2013 ◽  
Vol 425 (21) ◽  
pp. 212015 ◽  
Author(s):  
A Khounsary ◽  
P Kenesei ◽  
J Collins ◽  
G Navrotski ◽  
J Nudell
Keyword(s):  
High Energy ◽  
X Ray ◽  
Micro Tomography

X-ray micro tomography in the scanning electron microscope

1978 ◽  
Vol 36 (1) ◽  
pp. 106-107 ◽  
Author(s):  
W. Brünger
Keyword(s):  
Electron Beam ◽  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Target Surface ◽  
The Body ◽  
X Rays ◽  
Cross Sectional ◽  
X Ray ◽  
Micro Tomography ◽  
Scanning Electron

Reconstructive tomography is a new technique in diagnostic radiology for imaging cross-sectional planes of the human body /1/. A collimated beam of X-rays is scanned through a thin slice of the body and the transmitted intensity is recorded by a detector giving a linear shadow graph or projection (see fig. 1). Many of these projections at different angles are used to reconstruct the body-layer, usually with the aid of a computer. The picture element size of present tomographic scanners is approximately 1.1 mm2.Micro tomography can be realized using the very fine X-ray source generated by the focused electron beam of a scanning electron microscope (see fig. 2). The translation of the X-ray source is done by a line scan of the electron beam on a polished target surface /2/. Projections at different angles are produced by rotating the object.During the registration of a single scan the electron beam is deflected in one direction only, while both deflections are operating in the display tube.

High-purity Ge x-ray detectors: Sensitivity factors and usefulness

1990 ◽  
Vol 48 (2) ◽  
pp. 548-548
Author(s):  
E. B. Steel
Keyword(s):  
High Purity ◽  
High Energy ◽  
Quantitative Chemical Analysis ◽  
Detector Performance ◽  
X Ray ◽  
Detector Sensitivity ◽  
Specimen Holder ◽  
Many Instruments ◽  
Charge Resolution ◽  
Sensitivity Factors

High Purity Germanium (HPGe) x-ray detectors are now commercially available for the analytical electron microscope (AEM). The detectors have superior efficiency at high x-ray energies and superior resolution compared to traditional lithium-drifted silicon [Si(Li)] detectors. However, just as for the Si(Li), the use of the HPGe detectors requires the determination of sensitivity factors for the quantitative chemical analysis of specimens in the AEM. Detector performance, including incomplete charge, resolution, and durability has been compared to a first generation detector. Sensitivity factors for many elements with atomic numbers 10 through 92 have been determined at 100, 200, and 300 keV. This data is compared to Si(Li) detector sensitivity factors.The overall sensitivity and utility of high energy K-lines are reviewed and discussed. Many instruments have one or more high energy K-line backgrounds that will affect specific analytes. One detector-instrument-specimen holder combination had a consistent Pb K-line background while another had a W K-line background.

Designing high-resolution slow scan CCD-based TEM camera systems

1992 ◽  
Vol 50 (2) ◽  
pp. 946-947
Author(s):  
James F. Mancuso ◽  
William B. Maxwell ◽  
Russell E. Camp ◽  
Mark H. Ellisman
Keyword(s):  
Fiber Optics ◽  
Ccd Camera ◽  
High Energy ◽  
Phosphor Layer ◽  
X Ray ◽  
Light Production ◽  
Camera Systems ◽  
X Ray Imaging ◽  
Electron Image ◽  
Scintillating Fiber

The imaging requirements for 1000 line CCD camera systems include resolution, sensitivity, and field of view. In electronic camera systems these characteristics are determined primarily by the performance of the electro-optic interface. This component converts the electron image into a light image which is ultimately received by a camera sensor.Light production in the interface occurs when high energy electrons strike a phosphor or scintillator. Resolution is limited by electron scattering and absorption. For a constant resolution, more energy deposition occurs in denser phosphors (Figure 1). In this respect, high density x-ray phosphors such as Gd2O2S are better than ZnS based cathode ray tube phosphors. Scintillating fiber optics can be used instead of a discrete phosphor layer. The resolution of scintillating fiber optics that are used in x-ray imaging exceed 20 1p/mm and can be made very large. An example of a digital TEM image using a scintillating fiber optic plate is shown in Figure 2.

The Basic Physical Principles of Ion, Electron, and X-Ray Detectors and Their Application to Microanalysis

1985 ◽  
Vol 43 ◽  
pp. 154-157
Author(s):  
A.J. Tousimis
Keyword(s):  
Ion Beam ◽  
Depth Resolution ◽  
Sample Surface ◽  
High Energy ◽  
X Rays ◽  
X Ray ◽  
Electrons And Ions ◽  
Spatial Depth ◽  
Minimum Surface Area ◽  
Physical Principles

An integral and of prime importance of any microtopography and microanalysis instrument system is its electron, x-ray and ion detector(s). The resolution and sensitivity of the electron microscope (TEM, SEM, STEM) and microanalyzers (SIMS and electron probe x-ray microanalyzers) are closely related to those of the sensing and recording devices incorporated with them.Table I lists characteristic sensitivities, minimum surface area and depth analyzed by various methods. Smaller ion, electron and x-ray beam diameters than those listed, are possible with currently available electromagnetic or electrostatic columns. Therefore, improvements in sensitivity and spatial/depth resolution of microanalysis will follow that of the detectors. In most of these methods, the sample surface is subjected to a stationary, line or raster scanning photon, electron or ion beam. The resultant radiation: photons (low energy) or high energy (x-rays), electrons and ions are detected and analyzed.

Utilisation of High-Energy Heat Sources in Magnesium Alloy Surface Layer Treatment

2013 ◽  
Vol 58 (2) ◽  
pp. 619-624 ◽  
Author(s):  
M. Szafarska ◽  
J. Iwaszko ◽  
K. Kudła ◽  
I. Łegowik
Keyword(s):  
Surface Layer ◽  
Magnesium Alloy ◽  
Physicochemical Properties ◽  
Treatment Effectiveness ◽  
High Energy ◽  
Alloy Surface ◽  
Heat Sources ◽  
X Ray ◽  
Additional Equipment ◽  
Alloy Surface Layer

The main aim of the study was the evaluation of magnesium alloy surface treatment effectiveness using high-energy heat sources, i.e. a Yb-YAG Disk Laser and the GTAW method. The AZ91 and AM60 commercial magnesium alloys were subject to surface layer modification. Because of the physicochemical properties of the materials studied in case of the GTAW method, it was necessary to provide the welding stand with additional equipment. A novel two-torch set with torches operating in tandem was developed within the experiment. The effectiveness of specimen remelting using a laser and the GTAW method was verified based on macro- and microscopic examinations as well as in X-ray phase analysis and hardness measurements. In addition, the remelting parameters were optimised. The proposed treatment methodology enabled the achieving of the intended result and effective modification of a magnesium alloy surface layer.

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