Field ion microscopy images of multilayered graphene and graphene oxide

Author(s):  
Yahachi Saito
1982 ◽  
Vol 14 ◽  
Author(s):  
Christopher Grovenor ◽  
George Smith

ABSTRACTThe use of a Time-of-Flight Atom Probe in the analysis of silicon surfaces, and the interfaces between metals and silicon, promises to provide very accurate chemical analysis allied with structural information from Field Ion Microscopy images. This paper presents results on the analysis of silicon surfaces by this technique,showing that good spectra can be obtained without difficulty. Some preliminary experiments on the structure of such specimens after the deposition of thin layers of Pd and Ni will be described,concentrating on the analysis of the stoichiometry of the reacted layers.


2014 ◽  
Vol 90 (24) ◽  
Author(s):  
Sören Zint ◽  
Daniel Ebeling ◽  
Dirk Dietzel ◽  
Jens Falter ◽  
André Schirmeisen

2001 ◽  
Vol 89 (1-3) ◽  
pp. 137-144 ◽  
Author(s):  
F. Vurpillot ◽  
A. Bostel ◽  
D. Blavette

2012 ◽  
Vol 112 (1) ◽  
pp. 1-9 ◽  
Author(s):  
Daniel NiewieczerzaŁ ◽  
CzesŁaw Oleksy ◽  
Andrzej Szczepkowicz

Author(s):  
O. T. Inal ◽  
L. E. Murr

When sharp metal filaments of W, Fe, Nb or Ta are observed in the field-ion microscope (FIM), their appearance is differentiated primarily by variations in regional brightness. This regional brightness, particularly prominent at liquid nitrogen temperature has been attributed in the main to chemical specificity which manifests itself in a paricular array of surface-atom electron-orbital configurations.Recently, anomalous image brightness and streaks in both fcc and bee materials observed in the FIM have been shown to be the result of surface asperities and related topographic features which arise by the unsystematic etching of the emission-tip end forms.


Author(s):  
Gert Ehrlich

The field ion microscope, devised by Erwin Muller in the 1950's, was the first instrument to depict the structure of surfaces in atomic detail. An FIM image of a (111) plane of tungsten (Fig.l) is typical of what can be done by this microscope: for this small plane, every atom, at a separation of 4.48Å from its neighbors in the plane, is revealed. The image of the plane is highly enlarged, as it is projected on a phosphor screen with a radius of curvature more than a million times that of the sample. Müller achieved the resolution necessary to reveal individual atoms by imaging with ions, accommodated to the object at a low temperature. The ions are created at the sample surface by ionization of an inert image gas (usually helium), present at a low pressure (< 1 mTorr). at fields on the order of 4V/Å.


Author(s):  
H.C. Eaton ◽  
B.N. Ranganathan ◽  
T.W. Burwinkle ◽  
R. J. Bayuzick ◽  
J.J. Hren

The shape of the emitter is of cardinal importance to field-ion microscopy. First, the field evaporation process itself is closely related to the initial tip shape. Secondly, the imaging stress, which is near the theoretical strength of the material and intrinsic to the imaging process, cannot be characterized without knowledge of the emitter shape. Finally, the problem of obtaining quantitative geometric information from the micrograph cannot be solved without knowing the shape. Previously published grain-boundary topographies were obtained employing an assumption of a spherical shape (1). The present investigation shows that the true shape deviates as much as 100 Å from sphericity and boundary reconstructions contain considerable error as a result.Our present procedures for obtaining tip shape may be summarized as follows. An empirical projection, D=f(θ), is obtained by digitizing the positions of poles on a field-ion micrograph.


Author(s):  
R. Levi-Setti ◽  
J.M. Chabala ◽  
Y.L. Wang

Finely focused beams extracted from liquid metal ion sources (LMIS) provide a wealth of secondary signals which can be exploited to create high resolution images by the scanning method. The images of scanning ion microscopy (SIM) encompass a variety of contrast mechanisms which we classify into two broad categories: a) Emission contrast and b) Analytical contrast.Emission contrast refers to those mechanisms inherent to the emission of secondaries by solids under ion bombardment. The contrast-carrying signals consist of ion-induced secondary electrons (ISE) and secondary ions (ISI). Both signals exhibit i) topographic emission contrast due to the existence of differential geometric emission and collection effects, ii) crystallographic emission contrast, due to primary ion channeling phenomena and differential oxidation of crystalline surfaces, iii) chemical emission or Z-contrast, related to the dependence of the secondary emission yields on the Z and surface chemical state of the target.


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