Preparation and Properties of Single-Crystal Lead Telluride Films

1969 ◽  
Vol 6 (4) ◽  
pp. 493-497 ◽  
Author(s):  
G. Gardner Sumner ◽  
Lenford L. Reynolds
2014 ◽  
Vol 541 ◽  
pp. 012017 ◽  
Author(s):  
G A Dubov ◽  
S P Zimin ◽  
E S Gorlachev ◽  
I I Amirov ◽  
V V Naumov ◽  
...  

2007 ◽  
Vol 111 (30) ◽  
pp. 11397-11402 ◽  
Author(s):  
Feng Xiao ◽  
Bongyoung Yoo ◽  
Krassimir N. Bozhilov ◽  
Kyu Hwan Lee ◽  
Nosang V. Myung

1990 ◽  
Vol 2 (51) ◽  
pp. 10391-10400 ◽  
Author(s):  
Yu S Gromovoj ◽  
S V Plyatsko ◽  
F F Sizov ◽  
L A Korovina

2008 ◽  
Vol 20 (15) ◽  
pp. 4791-4793 ◽  
Author(s):  
Arup Purkayastha ◽  
Qingyu Yan ◽  
Darshan D. Gandhi ◽  
Huafang Li ◽  
Gyana Pattanaik ◽  
...  

1999 ◽  
Vol 581 ◽  
Author(s):  
Q. Wei ◽  
C.M. Lieber

ABSTRACTDimensionality can play an important role in determining the properties of materials. In the case of thermoelectric materials, it has been proposed that one-dimensional quantum wires, or nanowires, and two-dimensional superlattices could exhibit substantially higher efficiencies compared to the corresponding bulk, three-dimensional solids. To explore such predictions we have initiated a program directed towards the controlled growth of nanowires, and herein, we report the synthesis of single crystal Bi2Te3 and PbTe nanowires by a pulsed laser ablation method. Scanning electron microscopy (SEM) and transmission electron microscopy (TEM) show that Bi2Te3 wires 80 nm to 200 nm in diameter and lengths exceeding 10 microns, and PbTe wires 25 nm to 60 nm in diameter and lengths to 2 microns can be readily produced by the laser ablation method. High-resolution TEM and electron diffraction show that Bi2Te3 nanowires are single crystals with wire axes along the <110> crystal direction. TEM and electron diffraction measurements also show that the PbTe nanowires are single crystals with a <100> growth axis. The transport properties of these new nanowire materials will be discussed.


Author(s):  
Akira Tanaka ◽  
David F. Harling

In the previous paper, the author reported on a technique for preparing vapor-deposited single crystal films as high resolution standards for electron microscopy. The present paper is intended to describe the preparation of several high resolution standards for dark field microscopy and also to mention some results obtained from these studies. Three preparations were used initially: 1.) Graphitized carbon black, 2.) Epitaxially grown particles of different metals prepared by vapor deposition, and 3.) Particles grown epitaxially on the edge of micro-holes formed in a gold single crystal film.The authors successfully obtained dark field micrographs demonstrating the 3.4Å lattice spacing of graphitized carbon black and the Au single crystal (111) lattice of 2.35Å. The latter spacing is especially suitable for dark field imaging because of its preparation, as in 3.), above. After the deposited film of Au (001) orientation is prepared at 400°C the substrate temperature is raised, resulting in the formation of many square micro-holes caused by partial evaporation of the Au film.


Author(s):  
L. E. Murr ◽  
G. Wong

Palladium single-crystal films have been prepared by Matthews in ultra-high vacuum by evaporation onto (001) NaCl substrates cleaved in-situ, and maintained at ∼ 350° C. Murr has also produced large-grained and single-crystal Pd films by high-rate evaporation onto (001) NaCl air-cleaved substrates at 350°C. In the present work, very large (∼ 3cm2), continuous single-crystal films of Pd have been prepared by flash evaporation onto air-cleaved (001) NaCl substrates at temperatures at or below 250°C. Evaporation rates estimated to be ≧ 2000 Å/sec, were obtained by effectively short-circuiting 1 mil tungsten evaporation boats in a self-regulating system which maintained an optimum load current of approximately 90 amperes; corresponding to a current density through the boat of ∼ 4 × 104 amperes/cm2.


Author(s):  
D. J. Barber ◽  
R. G. Evans

Manganese (II) oxide, MnO, in common with CoO, NiO and FeO, possesses the NaCl structure and shows antiferromagnetism below its Neel point, Tn∼ 122 K. However, the defect chemistry of the four oxides is different and the magnetic structures are not identical. The non-stoichiometry in MnO2 small (∼2%) and below the Tn the spins lie in (111) planes. Previous work reported observations of magnetic features in CoO and NiO. The aim of our work was to find explanations for certain resonance results on antiferromagnetic MnO.Foils of single crystal MnO were prepared from shaped discs by dissolution in a mixture of HCl and HNO3. Optical microscopy revealed that the etch-pitted foils contained cruciform-shaped precipitates, often thick and proud of the surface but red-colored when optically transparent (MnO is green). Electron diffraction and probe microanalysis indicated that the precipitates were Mn2O3, in contrast with recent findings of Co3O4 in CoO.


Author(s):  
J. M. Galbraith ◽  
L. E. Murr ◽  
A. L. Stevens

Uniaxial compression tests and hydrostatic tests at pressures up to 27 kbars have been performed to determine operating slip systems in single crystal and polycrystal1ine beryllium. A recent study has been made of wave propagation in single crystal beryllium by shock loading to selectively activate various slip systems, and this has been followed by a study of wave propagation and spallation in textured, polycrystal1ine beryllium. An alteration in the X-ray diffraction pattern has been noted after shock loading, but this alteration has not yet been correlated with any structural change occurring during shock loading of polycrystal1ine beryllium.This study is being conducted in an effort to characterize the effects of shock loading on textured, polycrystal1ine beryllium. Samples were fabricated from a billet of Kawecki-Berylco hot pressed HP-10 beryllium.


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