Microstructural Evaluation of 9Cr-3W-3Co-Nd-B Heat-Resistant Steel (SAVE12AD) After Long-Term Creep Deformation

2017 ◽  
Author(s):  
Tomoaki Hamaguchi ◽  
Hirokazu Okada ◽  
Shinnosuke Kurihara ◽  
Hiroyuki Hirata ◽  
Mitsuru Yoshizawa ◽  
...  
Keyword(s):  
Base Metal ◽  
Heat Affected Zone ◽  
Welded Joints ◽  
Rupture Strength ◽  
Large Diameter ◽  
Creep Rupture ◽  
Martensite Lath ◽  
Creep Rupture Strength ◽  
Term Creep

The new ferritic heat-resistant steel composed of 9Cr-3W-3Co-Nd-B, registered as ASME Code Case 2839, has been developed for large diameter and heavy wall thickness pipes and forgings of fossil-fired power boilers. The steel, which contains 0.01 mass% boron, a small amount of neodymium, and optimized amounts of nitrogen, is characterized by the superior long-term creep strengths of both the base metal and welded joint. P92 had equiaxed subgrain structures changed from martensite lath structures and coarsened M23C6 type carbides after long-term creep. In contrast, the developed steel, SAVE12AD, maintained martensite lath structures with fine M23C6 along the boundaries even after the long-term creep stage. The addition of high amounts of boron suppressed the coarsening of M23C6 along the boundaries, thereby stabilizing the martensite lath structure in the base metal of the steel. Consequently, SAVE12AD had higher creep rupture strength than other high chromium ferritic steels. To investigate the creep rupture strength of welded joints, two welded joints with Ni-based alloy and Grade 92 welding filler wires were prepared by automatic gas tungsten arc welding. The creep rupture strength of each welded joint showed small degradation compared with the base metal in the long-term creep stage over 10,000 hours. These were ruptured 1.5 mm away from the fusion line, which was the same area as Type IV cracking. Microstructural observations were carried out by electron back scatter diffraction analysis using simulated heat-affected zone samples at different peak temperatures from 750 °C to 1350 °C in order to clarify the microstructure in the heat-affected zone. No fine grain area was observed in the microstructure after the simulated heat-affected zone at 910 °C just above AC3 transformation temperature, although there were fine grains along prior austenite grain boundaries, which seemed to form with the diffusion transformation. The creep cracks seemed to have initiated from the fine grain structures, resulting in the rupture at the same area as Type IV cracking. However, the creep rupture strength degradation of the welded joints against the base metal was significantly smaller than that of conventional steel welded joints owing to the suppression of fine grains found in the heat-affected zone heated around AC3 temperature. The developed 9Cr-3W-3Co-Nd-B steel (SAVE12AD) will be used for large diameter and heavy wall thickness pipes and forgings in 600 °C ultra super critical power plants.

Evaluation of Long-Term Creep Strength of Welded Joints of ASME Grades 91, 92 and 122 Type Steels

2012 ◽  
Author(s):  
Masatsugu Yaguchi ◽  
Takuaki Matsumura ◽  
Katsuaki Hoshino
Keyword(s):  
Creep Strength ◽  
Welded Joints ◽  
Rupture Strength ◽  
Reduction Factor ◽  
Creep Rupture ◽  
Creep Rupture Strength ◽  
Strength Reduction Factor ◽  
Rupture Data ◽  
Term Creep

Creep rupture data of welded joints of ASME Grades 91, 92 and 122 type steels have been collected and long-term creep rupture strength of the materials has been evaluated. Similar study was conducted by the SHC Committee in 2004 and 2005, therefore, the evaluation of the creep rupture strength was conducted with emphasis on the long-term creep rupture data obtained after the previous study, in addition to discussion of the effects of product form, welding procedure and test temperature etc. on the creep strength. Almost the same results were obtained on the welded joint of Grade 92 as the previous study, however, the master creep life equations for the welded joints of Grades 91 and 122 were lower than the previous results, especially in the case of Grade 122. Furthermore, the creep strength reduction factor obtained from 100,000 hours creep strength of welded joints and base metal was given as a function of temperature.

Evaluation of Long-Term Creep Strength of ASME Grades 91, 92, and 122 Type Steels

2012 ◽  
Author(s):  
Kazuhiro Kimura ◽  
Yukio Takahashi
Keyword(s):  
Base Metal ◽  
Creep Strength ◽  
Rupture Strength ◽  
Nickel Content ◽  
Creep Rupture ◽  
Tube Steel ◽  
Creep Rupture Strength ◽  
Rupture Data ◽  
Term Creep

Creep rupture data of ASME Grades 91, 92 and 122 type steels have been collected and long-term creep rupture strength of the steels has been evaluated. Similar study was conducted by the SHC committee in 2004 and 2005, therefore, the evaluation of long-term creep rupture strength was conducted with emphasis on the long-term creep rupture data obtained after the previous study. Creep rupture strength was analyzed by means of region splitting analysis method in consideration of 50% of 0.2% offset yield strength, in the same way as the previous study. Almost the same results were obtained on base metal of Grade 92 as the previous study, however, evaluated 100,000 hours creep rupture strength of base metal of Grades 91 and 122 were lower than the previous results. For Grades 91 and 122 type steels, moreover, creep rupture strength of the plate steel were lower than those of pipe and forging steels. Tendency to decrease with increase in nickel content was observed on long-term creep rupture strength of tube steel of Grade 91 at 600°C. According to the evaluation of long-term creep strength of the steels, allowable tensile stress was reviewed and proposed revision was concluded.

A Postassessment Test of 100,000 h Creep Rupture Strength of Grade 91 Steel at 600 °C

2017 ◽  
Vol 139 (5) ◽  
Author(s):  
K. Maruyama ◽  
N. Sekido ◽  
K. Yoshimi
Keyword(s):  
Rupture Strength ◽  
Creep Rupture ◽  
Creep Rupture Strength ◽  
Data Points ◽  
Predicted Values ◽  
Grade 91 ◽  
Term Creep ◽  
Term Data ◽  
Grade 91 Steel

Predictions as to 105 h creep rupture strength of grade 91 steel have been made recently. The predicted values are examined with long-term creep rupture data of the steel. Three creep rupture databases were used in the predictions: data of tube products of grade 91 steel reported in National Institute for Materials Science (NIMS) Creep Data Sheet (NIMS T91 database), data of T91 steel collected in Japan, and data of grade 91 steel collected by an American Society of Mechanical Engineers (ASME) code committee. Short-term creep rupture data points were discarded by the following criteria for minimizing overestimation of the strength: selecting long-term data points with low activation energy (multiregion analysis), selecting data points crept at stresses lower than a half of proof stress (σ0.2/2 criterion), and selecting data points longer than 1000 h (cutoff time of 1000 h). In the case of NIMS T91 database, a time–temperature parameter (TTP) analysis of a dataset selected by multiregion analysis can properly describe the long-term data points and gives the creep rupture strength of 68 MPa at 600 °C. However, TTP analyses of datasets selected by σ0.2/2 criterion and cutoff time of 1000 h from the same database overestimate the data points and predict the strength over 80 MPa. Datasets selected by the same criterion from the three databases provide similar values of the strength. The different criteria for data selection have more substantial effects on predicted values of the strength of the steel than difference of the databases.

scholarly journals Effect of Cobalt and Boron on Long-term Creep Rupture Strength of 12Cr Cast Steels

2010 ◽  
Vol 96 (10) ◽  
pp. 620-628 ◽  
Author(s):  
Masahiko Arai ◽  
Kentaro Asakura ◽  
Hiroyuki Doi ◽  
Hirotsugu Kawanaka ◽  
Toshihiko Koseki ◽  
...  
Keyword(s):  
Rupture Strength ◽  
Creep Rupture ◽  
Creep Rupture Strength ◽  
Cast Steels ◽  
Term Creep

Prediction of Breakdown Transition of Creep Strength in Advanced High Cr Ferritic Steels by Hardness Measurement of Aged Structures at High Temperature

2007 ◽  
Vol 345-346 ◽  
pp. 553-556 ◽  
Author(s):  
Hassan Ghassemi Armaki ◽  
Kouichi Maruyama ◽  
Mitsuru Yoshizawa ◽  
Masaaki Igarashi
Keyword(s):  
Power Plants ◽  
Rupture Strength ◽  
Hardness Measurement ◽  
Creep Rupture ◽  
Ferritic Steels ◽  
Creep Rupture Strength ◽  
Cr Concentration ◽  
Reduction Of Area ◽  
Term Creep

Recent researches have shown the premature breakdown of creep rupture strength in long term creep region of advanced high Cr ferritic steels. As safe operation of power plants becomes a serious problem we should be able to detect and predict the breakdown transition of creep rupture strength. Some methods for detecting the breakdown transition have been presented till now like the measurement of reduction of area after creep rupture and particle size of laves phase. However it will be more economic if we make use of non-destructive tests, for example, hardness testing. In this paper 3 types of ferritic steels with different Cr concentration have been studied. The results suggest that the hardness of aged structures is constant independently of exposure time in short term region, whereas the hardness breaks down in long term region. The boundary of breakdown in hardness coincides with that of breakdown in creep rupture strength.

Evaluation of Stress Rupture Factors for Grade 91 Weldments

2018 ◽  
Author(s):  
Kazuhiro Kimura
Keyword(s):  
Base Metal ◽  
Rupture Strength ◽  
Stress Rupture ◽  
Creep Rupture ◽  
Weld Strength ◽  
Creep Rupture Strength ◽  
Premature Failure ◽  
Type Iv ◽  
Grade 91

Stress rupture factors and weld strength reduction factors for Grade 91 weldments in the codes and literatures have been reviewed. Stress rupture factors for weld metals proposed for Code Case N-47 in the mid 1980’s was defined as the average rupture strength of the deposited filler metal to the average rupture strength of the base metal. Remarkable drop in creep rupture strength of weldments is significant issue of Grade 91, especially in the low-stress and long-term regime. A premature failure of Grade 91 weldments in the long-term, however, is caused by Type IV failure which takes place in the fine grained heat affected zone (FG-HAZ), rather than fracture in the deposited weld metal. The stress rupture factor of the Grade 91 steel, therefore, was based on the creep rupture strength of cross weld test specimens. Time and temperature dependent stress rupture factors for Grade 91 have been estimated based on the average creep rupture strength of cross weld test specimen to the average creep rupture strength of base metal.

Assessment of Creep Rupture Strength for New Martensitic 9% Cr Steels

2007 ◽  
Author(s):  
Walter Bendick ◽  
Jean Gabrel ◽  
Bruno Vandenberghe
Keyword(s):  
Power Plants ◽  
Rupture Strength ◽  
Strength Properties ◽  
Creep Rupture ◽  
Assessment Procedure ◽  
Creep Rupture Strength ◽  
Raw Data ◽  
Cr Steels ◽  
Term Creep

The application of new heat resistant steels in power plants requires reliable long term creep rupture strength values as basis for design. Modern martensitic 9% Cr-steels have complex microstructures that change with service exposure. That is why extrapolations of long term strength properties will be most difficult. Due to new long term test results, re-assessments became necessary for grades 911 and 92. Different methods have been used. Good agreement was obtained between a graphical and the numerical ISO 6303 method. In both cases a two-step assessment procedure was used. First the raw data was prepared in a suitable way, which was followed by mathematical averaging procedures. For comparison a Larson-Miller analysis on the raw data was performed, too. The results turned out to be too optimistic at temperatures higher than 575°C (1050°F). It is shown that a suitable preparation of data can improve the Larson-Miller assessment. As a result of the new assessments the design values had to be reduced for both grades. With respect to previous assessments the new values are up to almost 10% lower. In the case of grade 92 the difference from the former ASME values are even higher. Consequences concerning design and service operation are discussed.

Re-Evaluation of Long-Term Creep Strength of Welded Joint of ASME Grade 91 Type Steel

2016 ◽  
Author(s):  
Masatsugu Yaguchi ◽  
Kaoru Nakamura ◽  
Sosuke Nakahashi
Keyword(s):  
Creep Strength ◽  
Welded Joints ◽  
Rupture Strength ◽  
Creep Rupture ◽  
Base Metals ◽  
Rupture Data ◽  
Grade 91 ◽  
Term Creep ◽  
Grade 91 Steel

Creep rupture data of welded joints of ASME Grade 91 type steel have been collected from Japanese plants, milling companies and institutes, and the long-term creep rupture strength of the material has been evaluated. This evaluation of welded joints of Grade 91 steel is the third one in Japan as similar studies were conducted in 2004 and 2010. The re-evaluation of the creep rupture strength was conducted with emphasis on the long-term creep rupture data obtained since the previous study, with durations of the new data of up to about 60000h. The new long-term data exhibited lower creep strength than that obtained from the master creep life equation for welded joints of Grade 91 steel determined in 2010, then the master creep life equation was again reviewed on the basis of the new data using the same regression method as that used in 2010. Furthermore, the weld strength reduction factors obtained from 100000h creep strength of welded joints and the base metals are given as a function of temperature, where the master creep equations of the base metals are also redetermined in this study.

Evaluation of Creep Strength Reduction Factors for Welded Joints of Modified 9Cr-1Mo Steel (P91)

2006 ◽  
Author(s):  
Masaaki Tabuchi ◽  
Yukio Takahashi
Keyword(s):  
Base Metal ◽  
Creep Strength ◽  
Welded Joints ◽  
Welded Joint ◽  
Rupture Strength ◽  
Reduction Factor ◽  
Creep Rupture ◽  
Type Iv ◽  
Rupture Data ◽  
Term Creep

In order to review the allowable creep strength of high Cr ferritic steels, creep rupture data of base metal and welded joints have been collected and long-term creep strength have been analyzed in the SHC committee in Japan since 2004. In the present paper, the creep rupture data of 370 points for welded joint specimens of modified 9Cr-1Mo steel (ASME Grade 91) offered from seven Japanese companies and institutes were analyzed. These data clearly indicated that the creep strength of welded joints was lower than that of base metal due to Type IV fracture in HAZ at or above 600°C. From the activities of this committee, the master curve for life evaluation of welded joints of Gr.91 steel could be represented as follows: LMP==34154+3494(logσ)−2574(logσ)2,C=31.4 The reduction factor of 100,000 hours creep rupture strength of welded joint to base metal was concluded to be 0.75 at 600°C and 0.70 at 650°C for the Gr.91 steel.

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