Ceramic Additive Manufacturing Using VAT Photopolymerization

2018 ◽  
Author(s):  
Diptanshu ◽  
Erik Young ◽  
Chao Ma ◽  
Suleiman Obeidat ◽  
Bo Pang ◽  
...  
Keyword(s):  
Surface Roughness ◽  
Additive Manufacturing ◽  
Thermal Processing ◽  
Biomedical Applications ◽  
Ceramic Materials ◽  
Ceramic Suspension ◽  
Alumina Particles ◽  
Compressive Testing ◽  
The Difference ◽  
Porosity Percentage

The popularity of additive manufacturing for producing porous bio-ceramics using vat photopolymerization in the recent years has gained a lot of impetus due to its high resolution and low surface roughness. In this study, a commercial vat polymerization printer (Nobel Superfine, XYZprinting) was used to create green bodies using a ceramic suspension consisting of 10 vol.% of alumina particles in a photopolymerizable resin. Four different sizes of cubical green bodies were printed out. They were subjected to thermal processing which included de-binding to get rid of the polymer and thereafter sintering for joining of the ceramic particles. The porosity percentage of the four different sizes were measured and compared. The lowest porosity was observed in the smallest cubes (5 mm). It was found to be 43.3%. There was an increase in the porosity of the sintered parts for the larger cubes (10, 15 and 20 mm). However, the difference in the porosity among these sizes was not significant and ranged from 61.5% to 65.2%. The compressive testing of the samples showed that the strength of the 5-mm cube was the maximum among all samples and the compressive strength decreased as the size of the samples increased. These ceramic materials of various densities are of great interest for biomedical applications.

scholarly journals Effect of Process Parameters on the Generated Surface Roughness of Down-Facing Surfaces in Selective Laser Melting

2019 ◽  
Vol 9 (6) ◽  
pp. 1256 ◽  
Author(s):  
Amal Charles ◽  
Ahmed Elkaseer ◽  
Lore Thijs ◽  
Veit Hagenmeyer ◽  
Steffen Scholz
Keyword(s):  
Surface Roughness ◽  
Additive Manufacturing ◽  
Selective Laser Melting ◽  
Process Parameters ◽  
Process Models ◽  
Average Error ◽  
Lead Times ◽  
Laser Melting ◽  
Optimization Of Process Parameters ◽  
The Difference

Additive manufacturing provides a number of benefits in terms of infinite freedom to design complex parts and reduced lead-times while globally reducing the size of supply chains as it brings all production processes under one roof. However, additive manufacturing (AM) lags far behind conventional manufacturing in terms of surface quality. This proves a hindrance for many companies considering investment in AM. The aim of this work is to investigate the effect of varying process parameters on the resultant roughness of the down-facing surfaces in selective laser melting (SLM). A systematic experimental study was carried out and the effects of the interaction of the different parameters and their effect on the surface roughness (Sa) were analyzed. It was found that the interaction and interdependency between parameters were of greatest significance to the obtainable surface roughness, though their effects vary greatly depending on the applied levels. This behavior was mainly attributed to the difference in energy absorbed by the powder. Predictive process models for optimization of process parameters for minimizing the obtained Sa in 45° and 35° down-facing surface, individually, were achieved with average error percentages of 5% and 6.3%, respectively, however further investigation is still warranted.

scholarly journals Physical Properties of Modern Reciprocal Endodontic Systems and Fatigue Failure Testing in Simulated Clinical Conditions

2021 ◽  
Vol 11 (23) ◽  
pp. 11160
Author(s):  
Alexandr Jusku ◽  
Jan Tomáštík ◽  
Lukáš Václavek ◽  
Petr Jirásek ◽  
Ľuboš Harvan ◽  
...  
Keyword(s):  
Surface Roughness ◽  
Physical Properties ◽  
Cross Section ◽  
Thermal Processing ◽  
Fatigue Testing ◽  
Cyclic Fatigue ◽  
Factors Affecting ◽  
3D Microscopy ◽  
The Difference ◽  
Clinical Conditions

Instrument fracture ranks among the most crucial complications during the endodontic treatment of a tooth. In order to better understand the practical limits of the instrument, the relation between the cyclic fatigue resistance and physical properties such as hardness, modulus of elasticity, creep and surface roughness were explored. Cyclic fatigue testing in an artificial root canal at intracanal temperature, nanoindentation and 3D microscopy were used for evaluation of four commonly used thermomechanically treated NiTi endodontic instruments (Unicone Plus 6/025, Unicone 6/025, Reciproc Blue R25 and WaveOne Gold Primary). Cyclic fatigue results were analyzed using the Kruskal–Wallis, Mann–Whitney and Bonferroni corrections. The wear resistance of Unicone 6/025 instruments was significantly lower compared to all other instruments (p < 0.05). WaveOne Gold Primary was significantly less resistant than Unicone Plus 6/025 and Reciproc Blue R25, while the difference between Reciproc Blue R25 and Unicone Plus 6/025 was insignificant (p > 0.05). These results are in correlation with measurements of local mechanical properties (hardness, elastic modulus and their ratios H/E and H3/E2). Even though surface roughness, area of cross-section and shape of instruments are important factors affecting instruments behavior, thermal processing appears to be the most important.

scholarly journals Effect of tillage, slope, and rainfall on soil surface microtopography quantified by geostatistical and fractal indices during sheet erosion

2020 ◽  
Vol 12 (1) ◽  
pp. 232-241
Author(s):  
Na Ta ◽  
Chutian Zhang ◽  
Hongru Ding ◽  
Qingfeng Zhang
Keyword(s):  
Surface Roughness ◽  
Fractal Dimension ◽  
Soil Surface ◽  
Rainfall Events ◽  
Tillage Practices ◽  
Surface Microtopography ◽  
Artificial Rainfall ◽  
Soil Surface Roughness ◽  
The Difference ◽  
Sheet Erosion

AbstractTillage and slope will influence soil surface roughness that changes during rainfall events. This study tests this effect under controlled conditions quantified by geostatistical and fractal indices. When four commonly adopted tillage practices, namely, artificial backhoe (AB), artificial digging (AD), contour tillage (CT), and linear slope (CK), were prepared on soil surfaces at 2 × 1 × 0.5 m soil pans at 5°, 10°, or 20° slope gradients, artificial rainfall with an intensity of 60 or 90 mm h−1 was applied to it. Measurements of the difference in elevation points of the surface profiles were taken before rainfall and after rainfall events for sheet erosion. Tillage practices had a relationship with fractal indices that the surface treated with CT exhibited the biggest fractal dimension D value, followed by the surfaces AD, AB, and CK. Surfaces under a stronger rainfall tended to have a greater D value. Tillage treatments affected anisotropy differently and the surface CT had the strongest effect on anisotropy, followed by the surfaces AD, AB, and CK. A steeper surface would have less effect on anisotropy. Since the surface CT had the strongest effect on spatial variability or the weakest spatial autocorrelation, it had the smallest effect on runoff and sediment yield. Therefore, tillage CT could make a better tillage practice of conserving water and soil. Simultaneously, changes in semivariogram and fractal parameters for surface roughness were examined and evaluated. Fractal parameter – crossover length l – is more sensitive than fractal dimension D to rainfall action to describe vertical differences in soil surface roughness evolution.

scholarly journals Improving surface quality in selective laser melting based tool making

2021 ◽  
Author(s):  
Filippo Simoni ◽  
Andrea Huxol ◽  
Franz-Josef Villmer
Keyword(s):  
Surface Roughness ◽  
Additive Manufacturing ◽  
Surface Quality ◽  
Selective Laser Melting ◽  
Melting Process ◽  
Laser Remelting ◽  
Laser Melting ◽  
Great Cost ◽  
Starting Point ◽  
Processing Techniques

AbstractIn the last years, Additive Manufacturing, thanks to its capability of continuous improvements in performance and cost-efficiency, was able to partly replace and redefine well-established manufacturing processes. This research is based on the idea to achieve great cost and operational benefits especially in the field of tool making for injection molding by combining traditional and additive manufacturing in one process chain. Special attention is given to the surface quality in terms of surface roughness and its optimization directly in the Selective Laser Melting process. This article presents the possibility for a remelting process of the SLM parts as a way to optimize the surfaces of the produced parts. The influence of laser remelting on the surface roughness of the parts is analyzed while varying machine parameters like laser power and scan settings. Laser remelting with optimized parameter settings considerably improves the surface quality of SLM parts and is a great starting point for further post-processing techniques, which require a low initial value of surface roughness.

scholarly journals Directionally-Dependent Mechanical Properties of Ti6Al4V Manufactured by Electron Beam Melting (EBM) and Selective Laser Melting (SLM)

Materials ◽  
2021 ◽  
Vol 14 (13) ◽  
pp. 3603
Author(s):  
Tim Pasang ◽  
Benny Tavlovich ◽  
Omry Yannay ◽  
Ben Jakson ◽  
Mike Fry ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Surface Roughness ◽  
Tensile Strength ◽  
Electron Beam ◽  
Additive Manufacturing ◽  
Selective Laser Melting ◽  
Electron Beam Melting ◽  
Rolling Direction ◽  
Laser Melting ◽  
Plate Rolling

An investigation of mechanical properties of Ti6Al4V produced by additive manufacturing (AM) in the as-printed condition have been conducted and compared with wrought alloys. The AM samples were built by Selective Laser Melting (SLM) and Electron Beam Melting (EBM) in 0°, 45° and 90°—relative to horizontal direction. Similarly, the wrought samples were also cut and tested in the same directions relative to the plate rolling direction. The microstructures of the samples were significantly different on all samples. α′ martensite was observed on the SLM, acicular α on EBM and combination of both on the wrought alloy. EBM samples had higher surface roughness (Ra) compared with both SLM and wrought alloy. SLM samples were comparatively harder than wrought alloy and EBM. Tensile strength of the wrought alloy was higher in all directions except for 45°, where SLM samples showed higher strength than both EBM and wrought alloy on that direction. The ductility of the wrought alloy was consistently higher than both SLM and EBM indicated by clear necking feature on the wrought alloy samples. Dimples were observed on all fracture surfaces.

scholarly journals SURFACE ROUGHNESS CONSIDERATIONS IN DESIGN FOR ADDITIVE MANUFACTURING - A LITERATURE REVIEW

2021 ◽  
Vol 1 ◽  
pp. 2841-2850
Author(s):  
Didunoluwa Obilanade ◽  
Christo Dordlofva ◽  
Peter Törlind
Keyword(s):  
Surface Roughness ◽  
Additive Manufacturing ◽  
Literature Review ◽  
Future Research ◽  
Reduction Potentials ◽  
Research Fields ◽  
Post Process ◽  
Accessibility Issues ◽  
End Use ◽  
And Performance

AbstractOne often-cited benefit of using metal additive manufacturing (AM) is the possibility to design and produce complex geometries that suit the required function and performance of end-use parts. In this context, laser powder bed fusion (LPBF) is one suitable AM process. Due to accessibility issues and cost-reduction potentials, such ‘complex’ LPBF parts should utilise net-shape manufacturing with minimal use of post-process machining. The inherent surface roughness of LPBF could, however, impede part performance, especially from a structural perspective and in particular regarding fatigue. Engineers must therefore understand the influence of surface roughness on part performance and how to consider it during design. This paper presents a systematic literature review of research related to LPBF surface roughness. In general, research focuses on the relationship between surface roughness and LPBF build parameters, material properties, or post-processing. Research on design support on how to consider surface roughness during design for AM is however scarce. Future research on such supports is therefore important given the effects of surface roughness highlighted in other research fields.

scholarly journals 3D Printed Masks for Powders and Viruses Safety Protection Using Food Grade Polymers: Empirical Tests

Polymers ◽  
2021 ◽  
Vol 13 (4) ◽  
pp. 617
Author(s):  
Ruben Foresti ◽  
Benedetta Ghezzi ◽  
Matteo Vettori ◽  
Lorenzo Bergonzi ◽  
Silvia Attolino ◽  
...  
Keyword(s):  
Surface Roughness ◽  
Additive Manufacturing ◽  
Material Selection ◽  
Mechanical Resistance ◽  
Biological Safety ◽  
Fused Deposition ◽  
Industrial Grade ◽  
Safety Protection ◽  
3D Printed ◽  
Manufacturing Technologies

The production of 3D printed safety protection devices (SPD) requires particular attention to the material selection and to the evaluation of mechanical resistance, biological safety and surface roughness related to the accumulation of bacteria and viruses. We explored the possibility to adopt additive manufacturing technologies for the production of respirator masks, responding to the sudden demand of SPDs caused by the emergency scenario of the pandemic spread of SARS-COV-2. In this study, we developed different prototypes of masks, exclusively applying basic additive manufacturing technologies like fused deposition modeling (FDM) and droplet-based precision extrusion deposition (db-PED) to common food packaging materials. We analyzed the resulting mechanical characteristics, biological safety (cell adhesion and viability), surface roughness and resistance to dissolution, before and after the cleaning and disinfection phases. We showed that masks 3D printed with home-grade printing equipment have similar performances compared to the industrial-grade ones, and furthermore we obtained a perfect face fit by customizing their shape. Finally, we developed novel approaches to the additive manufacturing post-processing phases essential to assure human safety in the production of 3D printed custom medical devices.

scholarly journals Assessing the Functional Properties of TiZr Nanotubular Structures for Biomedical Applications, through Nano-Scratch Tests and Adhesion Force Maps

Molecules ◽  
2021 ◽  
Vol 26 (4) ◽  
pp. 900
Author(s):  
Maria Vardaki ◽  
Aida Pantazi ◽  
Ioana Demetrescu ◽  
Marius Enachescu
Keyword(s):  
Surface Roughness ◽  
Functional Properties ◽  
Bacterial Adhesion ◽  
Biomedical Applications ◽  
Adhesion Force ◽  
Roughness Parameters ◽  
Force Microscopy ◽  
Atomic Force ◽  
The Mean ◽  
Scratch Tests

In this work we present the results of a functional properties assessment via Atomic Force Microscopy (AFM)-based surface morphology, surface roughness, nano-scratch tests and adhesion force maps of TiZr-based nanotubular structures. The nanostructures have been electrochemically prepared in a glycerin + 15 vol.% H2O + 0.2 M NH4F electrolyte. The AFM topography images confirmed the successful preparation of the nanotubular coatings. The Root Mean Square (RMS) and average (Ra) roughness parameters increased after anodizing, while the mean adhesion force value decreased. The prepared nanocoatings exhibited a smaller mean scratch hardness value compared to the un-coated TiZr. However, the mean hardness (H) values of the coatings highlight their potential in having reliable mechanical resistances, which along with the significant increase of the surface roughness parameters, which could help in improving the osseointegration, and also with the important decrease of the mean adhesion force, which could lead to a reduction in bacterial adhesion, are providing the nanostructures with a great potential to be used as a better alternative for Ti implants in dentistry.

Slip Casting Used as a Forming Technique for Hydroxyapatite Processing

2016 ◽  
Vol 720 ◽  
pp. 219-222 ◽  
Author(s):  
Rubens Lincoln Santana Blazutti Marçal ◽  
Daniel Navarro da Rocha ◽  
Marcelo Henrique Prado da Silva
Keyword(s):  
Slip Casting ◽  
Ceramic Materials ◽  
Processing Route ◽  
Ceramic Suspension ◽  
Polyethylene Glycol 400 ◽  
Density Measurements ◽  
Hydroxyapatite Powder ◽  
Heat Treated ◽  
Thermal Phase ◽  
Before And After

Ceramic materials have particular properties when compared to other classes of materials, exhibiting poor ductility as an example. Slip casting is a widely used ceramic forming technique, and already established in the literature and in the ceramic industry. This study aims to present slip casting as a processing route for producing hydroxyapatite (HA) struts, and show the thermal phase stability. The ceramic suspension was produced and stabilized with hydroxyapatite powder, deionized water and polyethylene glycol 400. The slip was poured into gypsum mold. The green bodies were heat treated at 900 and 1100°C. Hydroxyapatite was the only phase present in all samples, before and after heat treatments. Density measurements showed that the densification was higher for the ceramic bodies sintered at 1100°C, when compared to the ones calcined at 900°C.

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