Surface Micro-Scale Patterning for Biomedical Implant Material of Pure Titanium via High Energy Pulse Laser Peening

2014 ◽  
Author(s):  
Ninggang Shen ◽  
Chelsey N. Pence ◽  
Robert Bowers ◽  
Yin Yu ◽  
Hongtao Ding ◽  
...  
Keyword(s):  
Shock Wave ◽  
Dental Implant ◽  
Pulse Laser ◽  
Pure Titanium ◽  
Strong Shock ◽  
High Energy ◽  
Laser Peening ◽  
Implant Surface ◽  
Implant Material ◽  
Energy Pulse

Pure titanium (commercial pure cpTi) is an ideal dental implant material without the leeching of toxic alloy elements. Evidence has shown that unsmooth implant surface topologies may contribute to the osteoblast differentiation in human mesenchymal pre-osteoblastic cells, which is helpful to avoid long-term peri-abutment inflammation issues for the dental implant therapy with transcutaneous devices. Studies have been conducted on the grit blasted, acid etched, or uni-directional grooved Ti surface. However, for these existing approaches, the surface quality is difficult to control or may even damage the implant. A novel idea has been studied in which more complex two-dimensional (2D) patterns can be imprinted into the dental implant material of cpTi by high energy pulse laser peening (HEPLP). The strong shock wave generated by HEPLP press a stainless steel grid, used as a stamp, on Ti foils to imprint a 2D pattern. In this study, the multiple grid patterns and grid sizes were applied to test the cell’s favor. The HEPLP induced shock wave pressure profile and history were simulated by a 2D multi-physics hydrodynamic numerical analysis for a better understanding of this technique. Then, the cell culture tests were conducted with the patterned surface to investigate the contribution of these 2D patterns, with the control tests of the other existing implant surface topography forming approaches.

Surface Micropatterning of Pure Titanium for Biomedical Applications Via High Energy Pulse Laser Peening

2015 ◽  
Vol 3 (1) ◽  
Author(s):  
Ninggang Shen ◽  
Hongtao Ding ◽  
Robert Bowers ◽  
Yin Yu ◽  
Chelsey N. Pence ◽  
...  
Keyword(s):  
Shock Wave ◽  
Mechanical Strength ◽  
Pulse Laser ◽  
Biomedical Applications ◽  
Pure Titanium ◽  
Strong Shock ◽  
High Energy ◽  
Laser Peening ◽  
Biomedical Implant ◽  
Energy Pulse

Pure titanium is an ideal material for biomedical implant applications for its superior biocompatibility, but it lacks of the mechanical strength required in these applications compared with titanium alloys. This research is concerned with an innovative laser peening-based material process to improve the mechanical strength and cell attachment property of pure titanium in biomedical applications. Evidence has shown that engineered surface with unsmooth topologies will contribute to the osteoblast differentiation in human mesenchymal pre-osteoblastic cells, which is helpful to avoid long-term peri-abutment inflammation issues for the dental implant therapy with transcutaneous devices. However, surface quality is difficult to control or mechanical strength is not enhanced using conventional approaches. In this paper, a novel high energy pulse laser peening (HEPLP) process is proposed to both improve the mechanical strength and introduce a micropattern into the biomedical implant material of a commercially pure Titanium (cpTi). The strong shock wave generated by HEPLP presses a stainless steel grid, used as a stamp, on cpTi foils to imprint a micropattern. To understand the basic science during the process, the HEPLP induced shock wave pressure profile and history are modeled by a multiphysics hydrodynamic numerical analysis. The micropatterns and strength enhancement are then simulated using a dislocation density-based finite element (FE) framework. Finally, cell culture tests are conducted to investigate the biomedical performance of the patterned surface.

scholarly journals Studying Biomimetic Coated Niobium as an Alternative Dental Implant Material to Titanium (in vitro and in vivo study)

2018 ◽  
Vol 15 (3) ◽  
pp. 253-261
Author(s):  
Baghdad Science Journal
Keyword(s):  
Dental Implant ◽  
Body Fluid ◽  
Pure Titanium ◽  
Commercially Pure Titanium ◽  
Removal Torque ◽  
X Ray ◽  
Commercially Pure ◽  
Implant Material

Commercially pure titanium (cpTi) is widely used as dental implant material although it was found that titanium exhibited high modulus of elasticity and the lower corrosion tendency in oral environment. Niobium(Nb) was chosen for this study as an alternative to cpTi implant material due to its bioinert behavior and good elastic modulus and moderate cost in addition to corrosion resistance. This study was done to evaluate the effect of biomimetic coating on the surface properties of the commercially pure titanium and niobium implants by in vitro and in vivo experiments. The in vitro study was involved etching the samples of each material in HCl then soaking in 10M NaOH aqueous solution. These samples were then immersed in a 5 times concentrated simulated body fluid for 14 days. Scanning Electron Microscope, Energy Dispersive X-ray, and X-Ray Diffraction tests were done to analyze surface changes. The in vivo study was done by the implantation of screw-shaped implants (two from each material, uncoated and the other was biomimetically coated) in the tibias of New Zealand rabbits. After 2 and 4 weeks of healing period, 20 rabbits were sacrificed for each period. A removal torque was done for ten animals in each group, whereas the other ten were used for histological testing and histomorphometric analysis with optical microscope.The in vitro experiments showed that the use of 14 days immersion in a concentrated simulated body fluid produced a layer of calcium phosphate on metal surfaces. The removal torque values and new bone formation were increased significantly in Nb than Ti, in coated than uncoated screws, and in 4 weeks than 2 weeks healing periods. The Nb implants had better biomechanical and biological properties than the commercially pure titanium implants and can be used as an alternative dental implant.

scholarly journals Dissipative soliton resonance as a guideline for high-energy pulse laser oscillators

2010 ◽  
Vol 27 (11) ◽  
pp. 2336 ◽  
Author(s):  
Philippe Grelu ◽  
Wonkeun Chang ◽  
Adrian Ankiewicz ◽  
Jose M. Soto-Crespo ◽  
Nail Akhmediev
Keyword(s):  
Pulse Laser ◽  
High Energy ◽  
Dissipative Soliton ◽  
Soliton Resonance ◽  
Laser Oscillators ◽  
Energy Pulse

scholarly journals Cigarette Smoke and E-Cigarette Vapor Dysregulate Osteoblast Interaction With Titanium Dental Implant Surface

2019 ◽  
Vol 45 (1) ◽  
pp. 2-11 ◽  
Author(s):  
Mahmoud Rouabhia ◽  
Humidah Alanazi ◽  
Hyun Jin Park ◽  
Reginaldo Bruno Gonçalves
Keyword(s):  
Adverse Effects ◽  
Cigarette Smoke ◽  
Dental Implant ◽  
Caspase 3 ◽  
Titanium Implant ◽  
Implant Surface ◽  
Implant Material ◽  
Dental Implant Surface ◽  
Titanium Dental Implant ◽  
Osteoblast Attachment

The purpose of this study was to determine the possible deleterious effects of e-cigarette vapor on osteoblast interaction with dental implant material. Osteoblasts were cultured onto Ti6Al4V titanium implant disks and were then exposed or not to whole cigarette smoke (CS), as well as to nicotine-rich (NR) or nicotine-free (NF) e-vapor for 15 or 30 minutes once a day for 1, 2, or 3 days, after which time various analyses were performed. Osteoblast growth on the titanium implant disks was found to be significantly (P < .001) reduced following exposure to CS and to the NR and NF e-vapors. Osteoblast attachment to the dental implant material was also dysregulated by CS and the NR and NF e-vapors through a decreased production of adhesion proteins such as F-actin. The effects of CS and e-cigarette vapor on osteoblast growth and attachment were confirmed by reduced alkaline phosphatase (ALP) activity and tissue mineralization. The adverse effects of CS and the NR and NF e-vapors on osteoblast interaction with dental implant material also involved the caspase-3 pathway, as the caspase-3 protein level increased following exposure of the osteoblasts to CS or e-vapor. It should be noted that the adverse effects of CS on osteoblast growth, attachment, ALP, and mineralized degradation were greater than those of the NR and NF e-vapors, although the latter did downregulate osteoblast interaction with the dental implant material. Overall results suggest the need to consider e-cigarettes as a possible contributor to dental implant failure and/or complications.

Microstructure and Property of Fe-Based Alloy Modified Layer on 304 Stainless Steel by High-Energy Pulse Laser-Like Cladding (HPLC)

2016 ◽  
Vol 879 ◽  
pp. 2255-2260 ◽  
Author(s):  
C.H. Zhang ◽  
Y.F. Jia ◽  
M. Guan ◽  
C.L. Wu ◽  
J.Z. Tan ◽  
...  
Keyword(s):  
Stainless Steel ◽  
Pulse Laser ◽  
Cavitation Erosion ◽  
Erosion Resistance ◽  
High Energy ◽  
Wear Testing ◽  
304 Stainless Steel ◽  
Energy Pulse ◽  
Modified Layer ◽  
Cavitation Erosion Resistance

Fe-based alloy modified layers were prepared on 304 stainless steels by high-energy pulse laser-like cold welding cladding technique. The microstructure, composition and phase constituents of the cladding layers were analyzed using SEM, EDS and XRD, respectively. The microhardness, friction-wear and cavitation erosion resistance were also investigated using microhardness tester, pin-on-disk wear-testing machine and ultrasonic vibrator. Experimental results showed that Fe-based alloy modified layer was mainly composed of α-Fe matrix phase and skeleton-like Cr23C6, Cr7C3 carbide reinforced phase, which was dispersively distributed into α-Fe matrix. The microhardness and friction coefficients of Fe-based alloy modified layer were 600HV and 0.4, respectively, indicating an improved wear resistance. The weight loss rate and average erosion depth of the modified layer was 1/5 and 1/10 that of 304 stainless steel in 3.5% NaCl solution after 5-h cavitation erosion test, respectively. The erosion crater depth of the modified layer was uniform, indicating that the cavitation erosion resistance of the modified layer was much better than that of the 304 stainless steel.

Electron microscopy study of shock synthesis of silicides

1993 ◽  
Vol 51 ◽  
pp. 1162-1163
Author(s):  
Kenneth S. Vecchio
Keyword(s):  
Shock Wave ◽  
Plastic Deformation ◽  
Close Contact ◽  
Microscopy Study ◽  
High Energy ◽  
Electron Microscopy Study ◽  
Powder Materials ◽  
Porous Powder ◽  
Wave Effects ◽  
Wave Passage

Shock-induced reactions (or shock synthesis) have been studied since the 1960’s but are still poorly understood, partly due to the fact that the reaction kinetics are very fast making experimental analysis of the reaction difficult. Shock synthesis is closely related to combustion synthesis, and occurs in the same systems that undergo exothermic gasless combustion reactions. The thermite reaction (Fe2O3 + 2Al -> 2Fe + Al2O3) is prototypical of this class of reactions. The effects of shock-wave passage through porous (powder) materials are complex, because intense and non-uniform plastic deformation is coupled with the shock-wave effects. Thus, the particle interiors experience primarily the effects of shock waves, while the surfaces undergo intense plastic deformation which can often result in interfacial melting. Shock synthesis of compounds from powders is triggered by the extraordinarily high energy deposition rate at the surfaces of the powders, forcing them in close contact, activating them by introducing defects, and heating them close to or even above their melting temperatures.

scholarly journals The Impact of Dental Implant Surface Modifications on Osseointegration and Biofilm Formation

2021 ◽  
Vol 10 (8) ◽  
pp. 1641
Author(s):  
Stefanie Kligman ◽  
Zhi Ren ◽  
Chun-Hsi Chung ◽  
Michael Angelo Perillo ◽  
Yu-Cheng Chang ◽  
...  
Keyword(s):  
Dental Implant ◽  
Biofilm Formation ◽  
Bacterial Colonization ◽  
Surface Modifications ◽  
Implant Surface ◽  
Oral Rehabilitation ◽  
Surface Design ◽  
Polyether Ether Ketone ◽  
Dental Implant Surface ◽  
The Impact

Implant surface design has evolved to meet oral rehabilitation challenges in both healthy and compromised bone. For example, to conquer the most common dental implant-related complications, peri-implantitis, and subsequent implant loss, implant surfaces have been modified to introduce desired properties to a dental implant and thus increase the implant success rate and expand their indications. Until now, a diversity of implant surface modifications, including different physical, chemical, and biological techniques, have been applied to a broad range of materials, such as titanium, zirconia, and polyether ether ketone, to achieve these goals. Ideal modifications enhance the interaction between the implant’s surface and its surrounding bone which will facilitate osseointegration while minimizing the bacterial colonization to reduce the risk of biofilm formation. This review article aims to comprehensively discuss currently available implant surface modifications commonly used in implantology in terms of their impact on osseointegration and biofilm formation, which is critical for clinicians to choose the most suitable materials to improve the success and survival of implantation.

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