Synthesis and Characterization of Microencapsulated Phase Change Material of Magnesium Sulfate Heptahydrate/Urea Resin via Emulsion Polymerization Method

Author(s):  
Chenzhen Liu ◽  
Ling Ma ◽  
Zhonghao Rao ◽  
Yimin Li

In this study, Microencapsulated phase change material (MicroPCM) was successfully synthesized by emulsion polymerization method, using magnesium sulfate heptahydrate (MSH) as core material and urea resin (UR) as shell material. The surface morphology of the MicroPCM was tested by scanning electron microscopy (SEM) and optical microscope (OM). The thermal property and particle size were investigated by differential scanning calorimetry (DSC) and laser particle size analyzer (LPA), respectively. The chemical structure of microcapsule was analyzed by Fourier-transform infrared spectroscopy (FTIR).

2017 ◽  
Vol 140 (1) ◽  
Author(s):  
Chenzhen Liu ◽  
Ling Ma ◽  
Zhonghao Rao ◽  
Yimin Li

In this study, micro-encapsulated phase change material (microPCM) was successfully synthesized by emulsion polymerization method, using magnesium sulfate heptahydrate (MSH) as core material and urea resin (UR) as shell material. The surface morphologies and particle size distributions of the microPCM were tested by scanning electron microscopy (SEM) and laser particle size analyzer. The chemical structure of microPCM was analyzed by Fourier-transform infrared spectroscopy (FTIR). The thermal properties were investigated by differential scanning calorimetry (DSC) and thermal conductivity coefficient instrument, respectively.


2021 ◽  
pp. 196-214
Author(s):  
Mohan KHANDAGRE ◽  
Bhupendra GUPTA ◽  
Jyotı BHALAVI ◽  
Prashant BAREDAR

Energies ◽  
2019 ◽  
Vol 12 (11) ◽  
pp. 2164
Author(s):  
H.M. Shih ◽  
Yi-Pin Lin ◽  
L.P. Lin ◽  
Chi-Ming Lai

In this study, a heat management module containing a microencapsulated phase change material (mPCM) was fabricated from mPCM (core material: paraffin; melting temperature: 37 °C) and aluminum honeycomb structures (8 mm core cell). The aluminum honeycomb functioned both as structural support and as a heat transfer channel. The thermal management performance of the proposed module under constant-temperature boundary conditions was investigated experimentally. The thermal protection period of the module decreased as the Stefan number increased; however, increasing the subcooling factor could effectively enhance the thermal protection performance. When the cold-wall temperature TC was fixed at 17 °C and the initial hot wall temperature was 47–67 °C, the heat dissipation of the module was complete 140 min after the hot-wall heat supply was stopped. The time required to complete the heat dissipation increased to 280 min when TC increased to 27 °C.


2014 ◽  
Vol 1070-1072 ◽  
pp. 422-426
Author(s):  
Shan Lv ◽  
Zhong Zhu Qiu

Microencapsulated Phase change material can absorb and release large amounts of latent heat over a defined temperature range as its physical state changes. The microencapsulated PCM has high energy density and isothermal behavior during charging and discharging and can avoid the contradiction of the energy supply and demand unbalance in time and space. Meanwhile, the shell can separate the phase change material from the outside environment in order to protect the core material. But the super-cooling problem is a main barrier for microencapsulated PCM application. So this paper talks about how to dealing with super-cooling based on related literatures and gives an overview about the methodology in this area.


2020 ◽  
Vol 56 (3) ◽  
pp. 2176-2191
Author(s):  
Jun Li ◽  
Xiaoyun Zhu ◽  
Huichang Wang ◽  
Pengcheng Lin ◽  
Lisi Jia ◽  
...  

2021 ◽  
Vol 16 ◽  
pp. 155892502110295
Author(s):  
Abdus Shahid ◽  
Solaiman Miah ◽  
Abdur Rahim

Jute bags are widely used to carry food grains and other materials that may be prone to quality deterioration due to thermal fluctuation. Thermal and moisture properties play a significant role in the packaging materials in the form of a container. This study deals with the effect of microencapsulated phase change material (MPCM) with hydrophobic binder on thermal and moisture management properties of jute fabric. Jute fabric was treated with MPCM by pad-dry-cure method. The treated sample was characterized by thermogravimetric analysis (TGA), differential scanning colorimeter (DSC), scanning electron microscope (SEM), moisture management tester (MMT), and air permeability tester. The results revealed that MPCM treated jute fabric shows greater thermal stability and heat absorption ability of 10.58 J/g while changing from solid to liquid phase. The SEM image ensures even distribution of MPCMs on fabric surface and surface roughness was also observed using image processing software. The air permeability was found to decrease whereas the water repellency enhanced in the developed sample.


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