Characterization of Crystallographic Texture of ERW Welded and Heat-Treated API X70 Pipeline Steel

Author(s):  
Nitin Sharma ◽  
Yiyu Wang ◽  
Leijun Li ◽  
Neil Anderson ◽  
Muhammad Rashid

Abstract The impact toughness of high frequency electric resistance welded (ERW) line pipe depends on the steel chemical composition, welding procedure, and post-welding heat treatment. Among several microstructural factors that may influence the impact toughness of high frequency electric resistance welded bond line, the crystallographic texture factor is often assumed, but not sufficiently studied. The evolution of texture during high frequency electric resistance welding and simulated post-welding heat treatments (PWHT) of API X70 pipeline steel was characterized using X-ray diffraction (XRD) and electron backscatter diffraction (EBSD). Results of a texture factor calculated using the θ/2θ XRD scans indicated that following the post-weld normalizing treatment, the texture factor of {100} planes for the weld bond line appeared to have increased with the increase in post-weld normalizing temperature. The texture factor results obtained from θ/2θ XRD scans were further verified by using the EBSD on the CVN tested samples in the regions near the fracture path. The XRD texture factor was also used to correlate the evolution of crystallographic texture and Charpy toughness for the PWHT samples. Based on the observations from both XRD and EBSD, the {100} crystallographic orientation of planes in the notched direction correlates well with the cleavage fracture planes of the Charpy impact tested samples. Therefore, the post-weld heat treatment should be designed to minimize any preferred crystallographic texture with {100} planes in the bond line, to promote ductile fracture and improved bond line impact toughness at low temperatures.

2012 ◽  
Vol 182-183 ◽  
pp. 1554-1558
Author(s):  
Yi Yuan Cheng ◽  
Zi Zhen Chen ◽  
Yong Jun Niu ◽  
Zheng Fang Wang

In this paper, SEM, EPMA, and micro shear experimental method were applied to analyse the structure, inclusion morphology and composition, micro-area strength and toughness of the X70 pipeline steel girth weld joint. The results show that inclusions are mainly nonmetallic oxides, sulfides and calcium compounds. The length of inclusions can be up to 1mm, which have substantially reduced the strength and toughness of weld joint. By the combining effect of internal and external force, cracks tend to initiate around inclusions and propagate along the direction of inclusions, and finally reduce the impact toughness of girth weld.


Author(s):  
Nitin Kumar Sharma ◽  
Rangasayee Kannan ◽  
Leijun Li ◽  
Neil Anderson ◽  
Muhammad Rashid ◽  
...  

2005 ◽  
Vol 297-300 ◽  
pp. 2391-2396 ◽  
Author(s):  
Zheng Yang ◽  
Chun Yong Huo ◽  
Wanlin Guo

The effects of thickness, notch orientation and delamination cracks on the impact toughness of X70 pipeline steel are investigated experimentally by use of the instrumented Charpy impact tests at different temperatures. The couple effect of delamination cracks, thickness, notch orientation and temperature is discovered. The delamination cracks have certain direction, and their amount and size are related to the temperature and the specimen thickness. Though the delaminating orientations of T-S and T-L specimen are not same, the reasons for both T-S and T-L specimen delaminating are that the weak interfaces in the specimens are pulled apart by the stress perpendicular to them. The delamination cracks can improve the actual impact toughness of X70 pipeline steel both T-L and T-S specimens. The effect of delamination cracks on the actual impact toughness changes with the thickness and the temperature. The couple effect of wall thickness, defect orientation and working temperature of pipeline must be taken into account in safe assessment of pipeline.


2013 ◽  
Vol 690-693 ◽  
pp. 2270-2274
Author(s):  
Qiu Rong Ma ◽  
Hong Da Chen ◽  
Yan Hua Li ◽  
He Li

Tensile and impact toughness test on X100 line pipe with different pre-strain at different aging temperature were conducted to study the effect of pre-strain and aging temperature on properties of X100 line pipe. The result shows that yield strength and tensile strength of X100 line pipe would increase significantly with the introduction of pre-strain, while the impact toughness would decrease significantly. Effect of strain aging on tensile properties of X100 line pipe are more significantly. The yield strength, and tensile strength would increase significantly with the introduction of strain aging both transversal and longitudinal direction.


2017 ◽  
Vol 36 (8) ◽  
pp. 825-830 ◽  
Author(s):  
Su-Fen Tao ◽  
Yun-Jin Xia ◽  
Fu-Ming Wang ◽  
Jie Li ◽  
Ding-Dong Fan

AbstractCircle quenching and tempering (CQ&T), intercritical quenching and tempering (IQ&T) and regular quenching and tempering (Q&T) were used to study the influence of heat treatment techniques on the low temperature impact toughness of steel EQ70 for offshore structure. The steels with 2.10 wt. % Ni (steel A) and 1.47 wt. % Ni (steel B) were chosen to analyze the effect of Ni content on the low temperature impact toughness of steel EQ70 for offshore structure. The fracture morphologies were examined by using a scanning electron microscope (SEM, JSM-6480LV), and microstructures etched by 4 vol. % nitric acid were observed on a type 9XB-PC optical microscope. The results show that the impact toughness of steel A is higher than that of steel B at the same test temperature and heat treatment technique. For steel B, the energy absorbed is, in descending order, CQ&T, Q&T and IQ&T, while for steel A, that is CQ&T, IQ&T and Q&T. The effects of heat treatment on the low temperature impact toughness are different for steels A and B, the absorbed energy changes more obviously for steel A. The results can be significant references for actual heat treatment techniques in steel plant.


2017 ◽  
Vol 24 (Supp02) ◽  
pp. 1850028
Author(s):  
BINFENG LU ◽  
YUNXIA CHEN ◽  
MENGJIA XU

(Cr, Fe)7C3/[Formula: see text]-Fe composite layer has been in situ synthesized on a low carbon steel surface by vacuum electron beam VEB irradiation. The synthesized samples were then subdued to different heat treatments to improve their impaired impact toughness. The microstructure, impact toughness and wear resistance of the heat-treated samples were studied by means of optical microscope (OM), X-ray diffraction (XRD), scanning electron microscope (SEM), microhardness tester, impact test machine and tribological tester. After heat treatment, the primary and eutectic carbides remained in their original shape and size, and a large number of secondary carbides precipitated in the iron matrix. Since the Widmanstatten ferrite in the heat affected zone (HAZ) transformed to fine ferrite completely, the impact toughness of the heat-treated samples increased significantly. The microhardness of the heat-treated samples decreased slightly due to the decreased chromium content in the iron matrix. The wear resistance of 1000[Formula: see text]C and 900[Formula: see text]C heat-treated samples was almost same with the as-synthesized sample. While the wear resistance of the 800[Formula: see text]C heat-treated one decreased slightly because part of the austenite matrix had transformed to ferrite matrix, which reduced the bonding of carbides particulates.


2013 ◽  
Vol 834-836 ◽  
pp. 816-819 ◽  
Author(s):  
Li Jun Tan ◽  
Jun Qiao Wang ◽  
Qing Qun Wang ◽  
Xin Long Chen ◽  
Si Zhu Zhou

The tensile and impact properties of SAE4320 and SAE8620 alloys were investigated. Various heat treatments were applied to these two alloys, including different pre-heat treatment. The results shown that after Carburizing and Quenching, both SAE4320 and SAE8620 alloys were highly sensitively to V-notches for their impact samples. In any case, SAE4320 alloy revealed higher tensile strength, better impact toughness and deformation property. Previous work shown that after Carburizing and Quenching, the impact toughness of SAE8620 alloy was too low, the products made of it was very dangerous. Based on the results, a new advanced product was made of SAE4320 alloy instead of SAE8620 alloy. And the new product exhibited good properties. The impact value of the new product far exceeded the older products.


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