A Study of Acoustic Emission Produced by Strength Test on Bio-Ceramics: Dependency of AE Duration Time and Mean Frequency on the Material Property

Author(s):  
Mitsuyuki Nakayama

Comparing the mechanical characteristics of bio-ceramics with a elaborate bone, there are two important conditions required for biomaterial. First, the strength must be three times larger than that of a elaborate bone. Second, Young’s modulus must be two or three times larger than that. However, still the biomaterial hasn’t developed which satisfies these conditions. The purpose of this research is to improve the strength of bio-ceramics. It was discussed how the duration time and mean frequency of acoustic emission (AE) parameters depend on time. These parameters are calculated with AE wave on breaking test of a bio-ceramics. The following main results were obtained. First, AE generating pattern is changed by the property of the materials. Second, in tetragonal zirconia polycrystals (TZP), the phase transformation has affected AE parameters. Consequently, it was shown that AE parameters had the material dependability.

Author(s):  
Mitsuyuki Nakayama ◽  
Hideto Suzuki

Comparing the mechanical characteristics of bio-ceramics with the elaborate bone, there are two important conditions required for it. First, the strength must be three times larger than that of the elaborate bone. Second, Young’s modulus must be two or three times larger than that. However, the biomaterial which satisfies these conditions hasn’t developed. So, it is the main purpose of this research to clarify the relation between stress and deflection on strength test of bio-ceramics, and to get the fundamental data for improvement. In this paper, it is discussed how such quantity as deflection, stress and stress increasing rate are related. As the result, the following characteristics were found. First, deflection and the breaking stress increase as an average grain diameter of bio-ceramics becomes small. Second, the behavior of the stress increasing rate to deflection can be classified into two types. These are the fluctuation type and the stable type. Third, the experimental equations are obtained against the maximum deflection. One is for the breaking stress, and the other is for the maximum stress increasing rate. From the discussion, it was found that the characteristics of stress and deflection depended on such material properties of bio-ceramics as Young’s modulus, an average grain diameter, and micro-structure of the biomaterials.


2020 ◽  
Author(s):  
Jackie E. Kendrick ◽  
Lauren N. Schaefer ◽  
Jenny Schauroth ◽  
Andrew F. Bell ◽  
Oliver D. Lamb ◽  
...  

Abstract. Volcanoes represent one of the most critical geological settings for hazard modelling due to their propensity to both unpredictably erupt and collapse, even in times of quiescence. Volcanoes are heterogeneous at multiple scales, from porosity which is variably distributed and frequently anisotropic to strata that are laterally discontinuous and commonly pierced by fractures and faults. Due to variable and, at times, intense stress and strain conditions during and post-emplacement, volcanic rocks span an exceptionally wide range of physical and mechanical properties. Understanding the constituent materials' attributes is key to improving the interpretation of hazards posed by the diverse array of volcanic complexes. Here, we examine the spectrum of physical and mechanical properties presented by a single dome-forming eruption at a dacitic volcano, Mount Unzen (Japan) by testing a number of isotropic and anisotropic lavas in tension and compression and using monitored acoustic emission (AE) analysis. The lava dome was erupted as a series of 13 lobes between 1991–1995, and its ongoing instability means much of the volcano and its surroundings remain within an exclusion zone today. During a field campaign in 2015, we selected 4 representative blocks as the focus of this study. The core samples from each block span range in porosity from 9.14 to 42.81 %, and permeability ranges from 1.54 × 10−14 to 2.67 × 10−10 m2 (from 1065 measurements). For a given porosity, sample permeability varies by > 2 orders of magnitude is lower for macroscopically anisotropic samples than isotropic samples of similar porosity. An additional 379 permeability measurements on planar block surfaces ranged from 1.90 × 10−15 to 2.58 × 10−12 m2, with a single block having higher standard deviation and coefficient of variation than a single core. Permeability under confined conditions showed that the lowest permeability samples, whose porosity largely comprises microfractures, are most sensitive to effective pressure. The permeability measurements highlight the importance of both scale and confinement conditions in the description of permeability. The uniaxial compressive strength (UCS) ranges from 13.48 to 47.80 MPa, and tensile strength (UTS) using the Brazilian disc method ranges from 1.30 to 3.70 MPa, with crack-dominated lavas being weaker than vesicle-dominated materials of equivalent porosity. UCS is lower in saturated conditions, whilst the impact of saturation on UTS is variable. UCS is between 6.8 and 17.3 times higher than UTS, with anisotropic samples forming each end member. The Young's modulus of dry samples ranges from 4.49 to 21.59 GPa and is systematically reduced in water-saturated tests. The interrelation of porosity, UCS, UTS and Young's modulus was modelled with good replication of the data. Acceleration of monitored acoustic emission (AE) rates during deformation was assessed by fitting Poisson point process models in a Bayesian framework. An exponential acceleration model closely replicated the tensile strength tests, whilst compressive tests tended to have relatively high early rates of AEs, suggesting failure forecast may be more accurate in tensile regimes, though with shorter warning times. The Gutenberg-Richter b-value has a negative correlation with connected porosity for both UCS and UTS tests which we attribute to different stress intensities caused by differing pore networks. b-value is higher for UTS than UCS, and typically decreases (positive Δb) during tests, with the exception of cataclastic samples in compression. Δb correlates positively with connected porosity in compression, and negatively in tension. Δb using a fixed sampling length may be a more useful metric for monitoring changes in activity at volcanoes than b-value with an arbitrary starting point. Using coda wave interferometry (CWI) we identify velocity reductions during mechanical testing in compression and tension, the magnitude of which is greater in more porous samples in UTS but independent of porosity in UCS, and which scales to both b-value and Δb. Yet, saturation obscures velocity changes caused by evolving material properties, which could mask damage accrual or source migration in water-rich environments such as volcanoes. The results of this study highlight that heterogeneity and anisotropy within a single system not only add uncertainty but also have a defining role in the channelling of fluid flow and localisation of strain that dictate a volcano's hazards and the geophysical indicators we use to interpret them.


Author(s):  
Mitusyuki Nakayama ◽  
Hideto Suzuki

Recently, advanced material used as a bio-ceramic is developed. These materials have one of the important features that characteristics of biocompatibility are improved considerably. However, these advanced materials include some problems that the strength of bio-ceramics decreases in accordance with improvement of biocompatibility. In this paper, it is the main purpose to accurate the acoustic emission characteristics of bio-ceramics on the breaking test, which has never been discussed enough. Therefore, AE parameters are calculated with the wave form of AE signal emitted on the breaking test. Next, the relation between AE parameters and material property of bio-ceramics are discussed in order to accurate the effectiveness of micro-structure elements to mechanical characteristics. As a result, it is found that AE parameters have remarkable dependence on micro-structure element in the body of bio-ceramics. Consequently, it is clarified that the acoustic emission method gives good agreement with the mechanical characteristics.


Materials ◽  
2019 ◽  
Vol 12 (10) ◽  
pp. 1677 ◽  
Author(s):  
Ningning Song ◽  
Ziyuan Wang ◽  
Yan Xing ◽  
Mengfei Zhang ◽  
Peng Wu ◽  
...  

Microscopical nonuniformity of mechanical properties caused by phase transformation is one of the main reasons for the failure of the materials in engineering applications. Accurate measurement of the mechanical properties of each phase is of virtual importance, in which the traditional approach like Vickers hardness cannot accomplish, due to the large testing range. In this study, nanoindentation is firstly used to analyze the mechanical properties of each phase and demonstrate the phase transformation in thermal barrier coatings during high-temperature aging. The distribution of T-prime metastable tetragonal phase, cubic and tetragonal phase is determined by mapping mode of nanoindentation and confirmed with X-ray diffraction and scanning electron microscope observation. The results show that during 1300 °C aging, the phase transition of metastable Yttria-Stabilized Zirconia induces the quick decrease of T′ phase content and an increase of T and C phases accordingly. It is found that there are some fluctuations in the mechanical properties of individual phase during annealing. The hardness and Young’s modulus of T′ increase at first 9 h, due to the precipitation of Y3+ lean T phase and then decrease to a constant value accompanied by the precipitation of Y3+ rich C phase. The relevant property of C phases also increases a little firstly and then decreases to a constant, due to the homogenization of Y3+ content, while the hardness and Young’s modulus of T phase remain unchanged. After aging of 24h the hardness of T′, C and T phases are 20.5 GPa, 21.3 GPa and 19.1 GPa, respectively. The Young’s modulus of T′, C and T phases are 274 GPa, 275 GPa and 265 GPa, respectively. Present work reveals the availability of nanoindentation method to demonstrate the phase transformation and measure mechanical properties of composites. It also provides an efficient application for single phase identification of ceramics.


2012 ◽  
Vol 503 ◽  
pp. 308-311
Author(s):  
Han Chen ◽  
Hua Rong

Large-scale measurement of material property is not suit for the MEMS thin-film. Research the in-situ measuring method for material property of the MEMS thin-film is urgently. A center-anchored circular plate is adopted as the test structure here. The resonance frequency of the circular plate is measured to extract the Young’s modulus of a MEMS thin-film. The accuracy of this non-contact in-situ measuring method has been verified by CoventorWare. The inferences of the stress gradient have been analyzed. The advantages of the test structure and the measuring method present here also have been discussed.


Author(s):  
Mitsuyuki Nakayama ◽  
Hideto Suzuki

Recently, ceramics has been using widely as living body material. It is called “bioceramics”. Both strength and elasticity of a living body material need almost three times larger than that of elaborate bone. However, it is difficult to satisfy the condition. So bioceramics is inferior to an elaborate bone. The purpose of this research is to obtain a basic data for improving the mechanical characteristics of bioceramics by the Acoustic Emission (AE) method. It was discussed how average roughness depends on mechanical characteristic and AE parameter of bioceramics. The following results were obtained. The first, the bioceramics showed a positive correlation between sound velocity and Kurtosis, that is one of the important parameter for the surface roughness. The second, it was clarified that same relation was obtained between Kurtosis and such mechanical parameters as stress, Young’s modulus and hardness. The third, these results were in accordance with the theory of fracture mechanics for fine ceramics reported independently by Rice and Aoki.


2014 ◽  
Vol 875-877 ◽  
pp. 1642-1646
Author(s):  
Jing Zhang

Alumina and zirconia are important materials for energy and optical applications. In this study, the effect of thermal cycling on grain size and residual stress was reported. Residual stress was measured using X-ray diffraction (XRD) sin2ψ method for the as-received and the samples after thermal cycling up to 900 cycles. For alumina, the measured residual stress is approximately 96 MPa in tensile for the as-received material, and increases to its highest value of 480 MPa after 650 thermal cycles. The residual stress decreases from 480 MPa to 96 MPa in tensile with increased thermal cycling from 650 to 900 cycles. The crystallized grain size calculated from the diffraction pattern shows that the mean crystallized grain size is about 93 nm for the as-received and increases to 232 nm after 650 thermal cycles. This result is consistent with the enlarged grain size observed by scanning electron microscopy for the alumina after 650 thermal cycles reported earlier. With continued thermal cycling up to 900 cycles, the crystallized grain size is greatly reduced to 104 nm. It suggests that evolution of the crystallized grain size is correlated with the residual stress. For yttria-stabilized tetragonal zirconia (Y-TZP), the mechanical properties at room temperature, are consistent with the property values provided by the manufacturer. The Young’s modulus of shows a non-linear inverse relationship with increasing temperature. The degradation of the Young’s modulus mostly occurs prior to 400 °C and to a less extent in the temperature range of 400 °C up to 850 °C. The Vickers hardness number for the as-received Y-TZP material decreases to a very small extent after 560 thermal cycles and increases approximately 2%, after 1200 thermal cycles. This is consistent with the trend of the Young’s modulus for thermal-cycled specimens.


2007 ◽  
Vol 16 (2) ◽  
pp. 096369350701600
Author(s):  
Yuxi Yu

By introducing hetero-element aluminum into ceramic precursor and then sintering, polycrystalline, stoichiometric SiC fibres can be prepared. Two types of aluminum-containing SiC fibres were fabricated by the use of aluminum-containing polycarbosilane (Al-PCS). The air-cured Al-PCS fibres were pyrolyzed in inert gas up to 13 50 °C to obtain SiC(OAl) fibres, which were converted into SiC(Al) fibres by heating in argon up to 1800 °C. The properties and performances of SiC(OAl) and SiC(Al) fibres were studied by chemical element analysis, scanning electron microscopy (SEM), X-ray diffraction (XRD), tensile strength test, heat resistance and creep resistance. These results show SiC(Al) are polycrystalline SiC fibres, have a near stoichiometric composition. The tensile strength, Young's modulus and diameter of the SiC(OAl) fibres are 2.6 GPa, 210 GPa, 12 μm, respectively. The tensile strength, Young's modulus and diameter of the SiC(Al) fibres are 2.1 GPa, 405 GPa, 10 μm, respectively. The SiC(Al) fibres have higher thermal stability, and better creep resistance than the SiC(OAl), the Nicalon and the Hi-Nicalon fibres.


2017 ◽  
Vol 894 ◽  
pp. 85-88
Author(s):  
Singh Ramesh ◽  
Wai Jin Kelvin Chew ◽  
H.C. Alexender Chee ◽  
C.Y. Tan

The effect of flyash (FA) additions of 0.05 wt% to 1 wt% on yttria-stabilized tetragonal zirconia polycrystals (Y-TZP), sintered in air at temperatures ranging from 1250°C to 1500°C, was examined. The bulk density, Young’s modulus, Vickers hardness and fracture toughness for each addition were determined while ageing behaviour were observed by subjecting them to superheated steam at 180°C/10 bar in an autoclave for 24 hours. Additions of FA, particularly of 0.05 wt% and 0.1 wt%, were found to be beneficial in aiding densification and increasing Young’s modulus beyond 200 GPa for sintering temperatures up to 1350°C. A common trend was observed for the Vickers hardness of all additions including undoped; hardness continues to rise from 1250°C and peaked at 1350°C before gradually decreasing as the sintering temperature increases further. No pronounced effect of flyash was seen on the fracture toughness of all samples. The ageing resistance of Y-TZP improved with addition of FA resulting in relatively lower amount of ageing-induced tetragonal to monoclinic phase transformation exhibited by doped samples compared to the undoped.


2014 ◽  
Vol 783-786 ◽  
pp. 1307-1312 ◽  
Author(s):  
Masaaki Nakai ◽  
Mitsuo Niinomi ◽  
Junko Hieda ◽  
Ken Cho ◽  
Kengo Narita ◽  
...  

In order to meet the requirements of the patients and surgeons simultaneously for spinal fixation applications, beta (β) -type Ti-Mo alloys with self-tunable Young’s modulus due to deformation have been developed to prevent the stress-shielding effect for patients and to suppress springback for surgeons. In this study, the effects of Mo on the deformation-induced omega-phase transformation were investigated and then the Mo content in binary Ti-Mo alloys was optimized in order to achieve a large increase in Young’s modulus via deformation-induced omega-phase transformation, leading to suppression of springback.


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