Arctic Exposure Studies of Vinyl Foams for Sandwich Composites

Author(s):  
Carlos D. Garcia ◽  
Raudel O. Avila ◽  
Pavana Prabhakar

Sea water and cold temperatures appear to have an adverse effect on naval materials resulting in the degradation of their mechanical properties. In this paper, the effects of sea water absorption and arctic conditioning have on the mechanical properties of divinycell foams are discussed. For this study, moisture absorption was periodically measured until weight gain equilibrium or saturation was reached for samples submerged in sea water and deionized water. Diffusivities and saturation values were obtained from moisture uptake curves. It was observed that the moisture content was higher for the vinyl foam samples submerged in deionized water compared to the samples submerged in synthetic sea water. Diffusivities were 9.227E-06 mm2sec and 1.390E-05 mm2sec for deionized water and sea water conditioning, respectively. Flexural and compression tests were then conducted on conditioned samples to compare their response against non-exposed samples. Experimental findings showed degradation in the flexural modulus and the compressive modulus for saturated wet samples and arctic-dry samples. This occurrence can be observed in both tests with more prominent reduction in its flexural modulus for arctic-dry samples and in compression for submerged in deionized water samples. Such a reduction is attributed to the degradation caused by the water, both deionized water and sea water, in the form of surface damage to specimens.

2020 ◽  
Vol 29 ◽  
pp. 2633366X2092652
Author(s):  
Kishora Shetty ◽  
Ramesh Bojja ◽  
Shylaja Srihari

Unidirectional carbon fiber-reinforced plastic (CFRP) IMA/M21E polymer composite was manufactured by standard autoclave curing method. This is a new aircraft-grade CFRP composite presently used in the manufacture of aircraft wing parts. Test specimens as per ASTM standards for weight gain, tensile and compression tests were obtained from this composite laminates. Some of the test specimens were subjected to hygrothermal (hot–wet) aging in an environmental chamber under three different conditions, that is, (i) 45°C/85% relative humidity (RH), (ii) 70°C/85% RH and (iii) 55°C/100% RH until reaching moisture absorption saturation. Matrix-dominated mechanical properties, that is, transverse tensile and longitudinal compression were determined for dry and hygrothermally aged test specimens. During mechanical testing in a servo-hydraulic test machine, the respective hygrothermal conditions were maintained while testing. It was noted that the rate of moisture absorption increases progressively and reaches saturation around 0.76–1.24 wt% depending on the aging conditions. Moisture absorption followed Fickian diffusion behavior in all the conditions of the study. Also, a software program was developed to predict the moisture content and time of saturation. The predicted results from this software program correlated with experimental results. It was observed that the presence of moisture reduced the tensile strength significantly by about 9–31% and compression strength by about 2–8%. Microscopic observation of tested samples was carried out using scanning electron microscope to study the failure behavior.


Materials ◽  
2019 ◽  
Vol 12 (7) ◽  
pp. 1145 ◽  
Author(s):  
Pooria Khalili ◽  
Xiaoling LIU ◽  
Zirui ZHAO ◽  
Brina Blinzler

Natural fibre-reinforced poly(lactic acid) (PLA) laminates were prepared by a conventional film stacking method from PLA films and natural fabrics with a cross ply layup of [0/90/0/90/0/90], followed by hot compression. Natural fibre (NF) nano-hydroxyapatite (nHA) filled composites were produced by the same manufacturing technique with matrix films that had varying concentrations of nHA in the PLA. Their flammability, thermal, moisture absorption and mechanical properties were analysed in terms of the amount of nHA. The flame behavior of neat PLA and composites evaluated by the UL-94 test demonstrated that only the composite containing the highest quantity of nHA (i.e., 40 wt% nHA in matrix) was found to achieve an FH-1 rating and exhibited no recorded burn rate, whereas other composites obtained only an FH-3. The thermal degradation temperature and mass residue were also observed, via thermogravimetric analysis, to increase when increasing concentrations of nHA were added to the NF composite. The tensile strength, tensile modulus and flexural modulus of the neat resin were found to increase significantly with the introduction of flax fibre. Conversely, moisture absorption was found to increase and mechanical properties to decrease with both the presence of NF and increasing concentrations of nHA, and subsequent mechanical properties experienced an obvious reduction.


Materials ◽  
2021 ◽  
Vol 14 (14) ◽  
pp. 4039
Author(s):  
Tajammul Hussain M. Mysore ◽  
Arun Y. Patil ◽  
G. U. Raju ◽  
N. R. Banapurmath ◽  
Prabhakar M. Bhovi ◽  
...  

This paper investigates the physical and mechanical properties of bighorns of Deccani breed sheep native from Karnataka, India. The exhaustive work comprises two cases. First, rehydrated (wet) and ambient (dry) conditions, and second, the horn coupons were selected for longitudinal and lateral (transverse) directions. More than seventy-two samples were subjected to a test for physical and mechanical property extraction. Further, twenty-four samples were subjected to physical property testing, which included density and moisture absorption tests. At the same time, mechanical testing included analysis of the stress state dependence with the horn keratin tested under tension, compression, and flexural loading. The mechanical properties include the elastic modulus, yield strength, ultimate strength, failure strain, compressive strength, flexural strength, flexural modulus, and hardness. The results showed anisotropy and depended highly on the presence of water content more than coupon orientation. Wet conditioned specimens had a significant loss in mechanical properties compared with dry specimens. The observed outcomes were shown at par with results for yield strength of 53.5 ± 6.5 MPa (which is better than its peers) and a maximum compressive stress of 557.7 ± 5 MPa (highest among peers). Young’s modulus 6.5 ± 0.5 GPa and a density equivalent to a biopolymer of 1.2 g/cc are expected to be the lightest among its peers; flexural strength 168.75 MPa, with lowest failure strain percentage of 6.5 ± 0.5 and Rockwell hardness value of 60 HRB, seem best in the class of this category. Simulation study identified a suitable application area based on impact and fatigue analysis. Overall, the exhaustive experimental work provided many opportunities to use this new material in various diversified applications in the future.


2014 ◽  
Vol 2014 ◽  
pp. 1-13 ◽  
Author(s):  
Salah U. Hamim ◽  
Raman P. Singh

Hydrophilic nature of epoxy polymers can lead to both reversible and irreversible/permanent changes in epoxy upon moisture absorption. The permanent changes leading to the degradation of mechanical properties due to combined effect of moisture and elevated temperature on EPON 862, Nanomer I.28E, and Somasif MAE clay-epoxy nanocomposites are investigated in this study. The extent of permanent degradation on fracture and flexural properties due to the hygrothermal aging is determined by drying the epoxy and their clay-epoxy nanocomposites after moisture absorption. Significant permanent damage is observed for fracture toughness and flexural modulus, while the extent of permanent damage is less significant for flexural strength. It is also observed that permanent degradation in Somasif MAE clay-epoxy nanocomposites is higher compared to Nanomer I.28E clay-epoxy nanocomposites. Fourier transform infrared (FTIR) spectroscopy revealed that both clays retained their original chemical structure after the absorption-desorption cycle without undergoing significant changes. Scanning electron microscopy (SEM) images of the fracture surfaces provide evidence that Somasif MAE clay particles offered very little resistance to crack propagation in case of redried specimens when compared to Nanomer I.28E counterpart. The reason for the observed higher extent of permanent degradation in Somasif MAE clay-epoxy system has been attributed to the weakening of the filler-matrix interface.


2020 ◽  
Vol 6 (3) ◽  
pp. 459-469 ◽  
Author(s):  
Xiong Liang-Xiao ◽  
Chen Cong

Durability of cement mortar and concrete materials under sea water condition is always an important research topic. The objective of this work is to understand the mechanical properties of corroded cement mortar after high temperature, the cement mortar specimens after high temperature were placed in water and sodium sulfate solution, and then the uniaxial compression tests were carried out on the cement mortar specimens after corroded. Test results show that both the differences of compressive strength and strain at the peak stress after high temperature caused by high temperature, are relatively small when the specimens are eroded in water, and the differences are relatively high when the specimens are eroded in sodium sulfate solution. The compressive strength of the cement mortar specimens under normal temperature eroded in sodium sulfate solution is highest, and that eroded in water is lowest. The compressive strength of specimen after high temperature eroded in water is highest and that eroded in sodium sulfate solution is lowest. The strain at the peak stress of specimen, whether after high temperature or not, is highest when eroded in sodium sulfate solution, and that eroded in water is lowest. At present, there are few research results about the mechanical properties of concrete first after high temperature and then after sea water corrosion. The work in this paper can enrich the results in this area.


2021 ◽  
pp. 073168442110140
Author(s):  
Hossein Ramezani-Dana ◽  
Moussa Gomina ◽  
Joël Bréard ◽  
Gilles Orange

In this work, we examine the relationships between the microstructure and the mechanical properties of glass fiber–reinforced polyamide 6,6 composite materials ( V f = 54%). These materials made by thermocompression incorporate different grades of high fluidity polyamide-based polymers and two types of quasi-UD glass fiber reinforcement. One is a classic commercial fabric, while the other specially designed and manufactured incorporates weaker tex glass yarns (the spacer) to increase the planar permeability of the preform. The effects of the viscosity of the polymers and their composition on the wettability of the reinforcements were analyzed by scanning electron microscopy observations of the microstructure. The respective influences of the polymers and the spacer on the mechanical performance were determined by uniaxial tensile and compression tests in the directions parallel and transverse to the warp yarns. Not only does the spacer enhance permeability but it also improves physical and mechanical properties: tensile longitudinal Young’s modulus increased from 38.2 GPa to 42.9 GPa (13% growth), tensile strength increased from 618.9 MPa to 697 MPa (3% growth), and decrease in ultimate strain from 1.8% to 1.7% (5% reduction). The correlation of these results with the damage observed post mortem confirms those acquired from analyses of the microstructure of composites and the rheological behaviors of polymers.


2021 ◽  
Vol 13 (4) ◽  
pp. 2407
Author(s):  
Guang-Zhu Zhang ◽  
Xiao-Yong Wang ◽  
Tae-Wan Kim ◽  
Jong-Yeon Lim ◽  
Yi Han

This study shows the effect of different types of internal curing liquid on the properties of alkali-activated slag (AAS) mortar. NaOH solution and deionized water were used as the liquid internal curing agents and zeolite sand was the internal curing agent that replaced the standard sand at 15% and 30%, respectively. Experiments on the mechanical properties, hydration kinetics, autogenous shrinkage (AS), internal temperature, internal relative humidity, surface electrical resistivity, ultrasonic pulse velocity (UPV), and setting time were performed. The conclusions are as follows: (1) the setting times of AAS mortars with internal curing by water were longer than those of internal curing by NaOH solution. (2) NaOH solution more effectively reduces the AS of AAS mortars than water when used as an internal curing liquid. (3) The cumulative heat of the AAS mortar when using water for internal curing is substantially reduced compared to the control group. (4) For the AAS mortars with NaOH solution as an internal curing liquid, compared with the control specimen, the compressive strength results are increased. However, a decrease in compressive strength values occurs when water is used as an internal curing liquid in the AAS mortar. (5) The UPV decreases as the content of zeolite sand that replaces the standard sand increases. (6) When internal curing is carried out with water as the internal curing liquid, the surface resistivity values of the AAS mortar are higher than when the alkali solution is used as the internal curing liquid. To sum up, both NaOH and deionized water are effective as internal curing liquids, but the NaOH solution shows a better performance in terms of reducing shrinkage and improving mechanical properties than deionized water.


2021 ◽  
Vol 11 (12) ◽  
pp. 5317
Author(s):  
Rafał Malinowski ◽  
Aneta Raszkowska-Kaczor ◽  
Krzysztof Moraczewski ◽  
Wojciech Głuszewski ◽  
Volodymyr Krasinskyi ◽  
...  

The need for the development of new biodegradable materials and modification of the properties the current ones possess has essentially increased in recent years. The aim of this study was the comparison of changes occurring in poly(ε-caprolactone) (PCL) due to its modification by high-energy electron beam derived from a linear electron accelerator, as well as the addition of natural fibers in the form of cut hemp fibers. Changes to the fibers structure in the obtained composites and the geometrical surface structure of sample fractures with the use of scanning electron microscopy were investigated. Moreover, the mechanical properties were examined, including tensile strength, elongation at break, flexural modulus and impact strength of the modified PCL. It was found that PCL, modified with hemp fibers and/or electron radiation, exhibited enhanced flexural modulus but the elongation at break and impact strength decreased. Depending on the electron radiation dose and the hemp fibers content, tensile strength decreased or increased. It was also found that hemp fibers caused greater changes to the mechanical properties of PCL than electron radiation. The prepared composites exhibited uniform distribution of the dispersed phase in the polymer matrix and adequate adhesion at the interface between the two components.


2020 ◽  
Vol 72 (1) ◽  
Author(s):  
Hirofumi Niiya ◽  
Kenichi Oda ◽  
Daisuke Tsuji ◽  
Hiroaki Katsuragi

Abstract The formation of aggregates consisting of snow, water, and tephra has been reported in small-scale experiments on three-phase flows containing tephra, water, and snow, representing lahars triggered by snowmelt. Such aggregates reduce the mobility of mud flow. However, the formation mechanism of such aggregates under various conditions has not been investigated. To elucidate the formation conditions and mechanical properties of the aggregates, we performed mixing experiments with materials on a rotating table and compression tests on the resulting aggregates with a universal testing machine in a low-temperature room at $$0\,^{\circ }\text {C}$$ 0 ∘ C . From experiments with varying component ratios of the mixture and tephra diameter, the following results were obtained: (i) the aggregate grew rapidly and reached maturity after a mixing time of 5 min; (ii) the mass of aggregates increased with snow concentration, exhibiting an approximately linear relationship; (iii) single aggregates with large mass formed at lower and higher tephra concentrations, whereas multiple aggregates with smaller mass were observed at intermediate concentrations; (iv) the shape of the aggregate satisfied the similarity law for an ellipsoid; (v) the compressive mechanical behavior could be modeled by an empirical nonlinear model. The obtained mechanical properties of the aggregates were independent of the experimental conditions; (vi) scaling analysis based on the Reynolds number and the strength of the aggregates showed that the aggregates cannot form in ice-slurry lahars. Our findings suggest that low-speed lahars containing snow and ice are likely to generate aggregates, but snow and ice in the ice-slurry lahars are dispersed without such aggregates.


Author(s):  
D. C. Gornig ◽  
R. Maletz ◽  
P. Ottl ◽  
M. Warkentin

Abstract Objective The aim of the study was to evaluate the influence of filler content, degradation media and time on the mechanical properties of different dental composites after in vitro aging. Materials and Methods Specimens (1 mm3) of three commercially available composites (GrandioSO®, Arabesk Top®, Arabesk Flow®) with respect to their filler content were stored in artificial aging media: artificial saliva, ethanol (60%), lactic acid (pH 5) and citric acid (pH 5). Parameters (Vickers microhardness, compressive strength, elastic modulus, water sorption and solubility) were determined in their initial state (control group, n = 3 for microhardness, n = 5 for the other parameters) and after 14, 30, 90 and 180 days (n = 3 for microhardness, n = 5 for the other parameters for each composite group, time point and media). Specimens were also characterized with dynamic-mechanical-thermal analysis (compression tests, F =  ± 7 N; f = 0.5 Hz, 1 Hz and 3.3 Hz; t = 0–170 °C). Results Incorporation of fillers with more than 80 w% leads to significantly better mechanical properties under static and dynamic compression tests and a better water sorption behavior, even after chemical degradation. The influence of degradation media and time is of subordinate importance for chemical degradation. Conclusion Although the investigated composites have a similar matrix, they showed different degradation behavior. Since dentine and enamel occur only in small layer thickness, a test specimen geometry with very small dimensions is recommended for direct comparison. Moreover, the use of compression tests to determine the mechanical parameters for the development of structure-compatible and functionally adapted composites makes sense as an additional standard. Clinical relevance Preferential use of highly filled composites for occlusal fillings is recommended.


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