RTS - 1 - Galilei Decommissioning Project

2003 ◽  
Author(s):  
A. Boschi ◽  
E. Cimini ◽  
F. Pagni ◽  
L. Parracone ◽  
M. Pocai ◽  
...  
Keyword(s):  
Research Reactor ◽  
Thermal Flux ◽  
Spent Fuel ◽  
Radiological Risk ◽  
Radioactive Materials ◽  
Thermal Output ◽  
Protective Custody ◽  
First Time ◽  
Waste Characterisation

The RTS-1 “Galileo Galilei” is an open pool research reactor light water moderated and cooled. It had a maximum thermal output of 5 MWth and an average thermal flux of 5 E+13 n/cm2sec. It became critical for the first time on April 1963 and it was definitely shutdown in March 1980. The reactor is situated at CISAM (Joint Centre of Studies and Military Application - Italian Ministry of Defence), S. Piero a Grado, Pisa, Italy, and its decommissioning is in progress. In this paper the strategy adopted to achieve the green status of the reactor site is discussed, with particular attention on the different steps to be done according to the national laws. Emphasis is placed on the characteristics of two different conditions required, namely Passive Protective Custody, which is a step necessary to allow the decay of the radioactive materials present into the plant to decrease the radiological risk to operate safely, and Unconditioned Release, in which all the materials can be released without radiological restrictions. Another aspect discussed in this paper is the effort spent on the determination of the radioisotopic abundance of the reactor components, the personal dose evaluation due to the necessary activities to achieve two different status of “Passive Protective Custody” and “Unconditioned Release” and the waste characterisation. The necessary authorisations to start decommissioning has been obtained as far as concern the removal of spent fuel and the dismantling of some experimental equipments.

Nuclear Research Reactor RTS-1 “G. Galilei” Decommissioning: Preliminary Operations and Cutting Facilities

2004 ◽  
Author(s):  
A. Boschi ◽  
E. Cimini ◽  
L. Parracone ◽  
M. Pocai ◽  
M. Russo
Keyword(s):  
Research Reactor ◽  
Thermal Flux ◽  
Nuclear Research ◽  
Irradiation Channel ◽  
Radiological Risk ◽  
Radioactive Materials ◽  
Light Water ◽  
Military Application ◽  
Nuclear Research Reactor ◽  
First Time

The RTS-1 “Galileo Galilei” is an open pool research reactor with light water as moderator and coolant, it has a nominal power of 5 MWth and an average thermal flux of 5 E+13 n/cm2sec. It went critical for the first time on April 1963 and it was definitively shutdown in March 1980. The reactor is situated at CISAM (Joint Centre of Studies for Military Application - Italian Ministry of Defence), S. Piero a Grado, Pisa, Italy, and its decommissioning is in progress. In this paper the preliminary activities necessary to eliminate the most part of radioactive materials present into the plant are described. Emphasis is placed on the description of the “Irradiation Channel” facility, used to manage safely all the activated materials to be conditioned and on the MASCOT robot, used in the channel. All the conditioning devices to be used are described with particular consideration to the cleanness of the cutting process and the radiological risk due to the operations. The first cutting and conditioning operation carried on in the Galilei Reactor is described. This operation regards the conditioning of some experimental equipments used during the reactor life, with particular attention to the radiation protection of the personnel and to the control of radioactive emission.

Decommissioning Activities for Salaspils Research Reactor

2011 ◽  
Author(s):  
A. Abramenkovs ◽  
J. Malnacs
Keyword(s):  
Radioactive Waste ◽  
Research Reactor ◽  
Legal Aspects ◽  
Radioactive Wastes ◽  
Measurement Equipment ◽  
Radiation Measurement ◽  
Spent Fuel ◽  
Nuclear Facility ◽  
Radioactive Materials ◽  
Conceptual Study

In May 1995, the Latvian government decided to shut down the Salaspils Research Reactor (SRR). The reactor is out of operation since July 1998. A conceptual study for the decommissioning of SRR has been carried out by Noell-KRC-Energie- und Umwelttechnik GmbH at 1998–1999. The Latvian government decided to start the direct dismantling to “green field” in October 26, 1999. The upgrade of decommissioning and dismantling plan was performed in 2003–2004 years, which change the main goal of decommissioning to the “brown field”. The paper deals with the SRR decommissioning experience during 1999–2010. The main decommissioning stages are discussed including spent fuel and radioactive wastes management. The legal aspects and procedures for decommissioning of SRR are described in the paper. It was found, that the involvement of stakeholders at the early stages significantly promotes the decommissioning of nuclear facility. Radioactive waste management’s main efforts were devoted to collecting and conditioning of “historical” radioactive wastes from different storages outside and inside of reactor hall. All radioactive materials (more than 96 tons) were conditioned in concrete containers for disposal in the radioactive wastes repository “Radons” at Baldone site. The dismantling of contaminated and activated components of SRR systems is discussed in paper. The cementation of dismantled radioactive wastes in concrete containers is discussed. Infrastructure of SRR, including personal protective and radiation measurement equipment, for decommissioning purposes was upgraded significantly. Additional attention was devoted to the free release measurement’s technique. The certified laboratory was installed for supporting of all decommissioning activities. All non-radioactive equipments and materials outside of reactor buildings were released for clearance and dismantled for reusing or conventional disposing. Weakly contaminated materials from reactor hall were collected, decontaminated and removed for clearance measurements.

Disability as a social phenomenon

2020 ◽  
pp. 22-38
Author(s):  
Natalia Guseva ◽  
Vitaliy Berdutin
Keyword(s):  
Social Protection ◽  
Russian Society ◽  
Stage Model ◽  
High Quality ◽  
Rehabilitation Programs ◽  
Current State ◽  
The Social ◽  
Consistent Solution ◽  
First Time

At present, the problem of establishing disability is a point at issue in Russia. Despite the fact that medical criteria for disability are being developed very actively, high-quality methods for assessing social hallmarks are still lacking. Since disability is a phenomenon inherent in any society, each state forms a social and economic policy for people with disabilities in accordance with its level of development, priorities and opportunities. We have proposed a three-stage model, which includes a system for the consistent solution of the main tasks aimed at studying the causes and consequences of the problems encountered today in the social protection of citizens with health problems. The article shows why the existing approaches to the determination of disability and rehabilitation programs do not correspond to the current state of Russian society and why a decrease in the rate of persons recognized as disabled for the first time does not indicate an improvement in the health of the population. The authors proposed a number of measures with a view to correcting the situation according to the results of the study.

Phytochemical Constituents of Annona reticulata and their Cytotoxic Activity

2020 ◽  
Vol 17 (3) ◽  
pp. 206-210
Author(s):  
Ty Viet Pham ◽  
Thang Quoc Le ◽  
Anh Tuan Le ◽  
Hung Quoc Vo ◽  
Duc Viet Ho
Keyword(s):  
Cytotoxic Activity ◽  
Cell Lines ◽  
Structural Determination ◽  
Phytochemical Investigation ◽  
Ic50 Values ◽  
Phytochemical Constituents ◽  
First Time ◽  
Annona Reticulata

A phytochemical investigation of the leaves of Annona reticulata led to the isolation and structural determination of β-sitosterol (1), ent-pimara-8(14),15-dien-19-oic acid (2), ent-pimara- 8(14),15-dien-19-ol (3), quercetin (4), quercetin 3-O-α-L-arabinopyranoside (5), and a mixture of quercetin 3-O-β-D-galactopyranoside (6a) and quercetin 3-O-β-D-glucopyranoside (6b). Of these, compounds 2 and 3 were isolated from the genus Annona for the first time. Compound 3 showed strong cytotoxicity against SK-LU-1 and SW626 cell lines with IC50 values of 17.64 ± 1.07 and 19.79 ± 1.41 μg mL-1, respectively.

Development of an HPLC-UV Method for Quantification of Stattic

2019 ◽  
Vol 15 (6) ◽  
pp. 568-573
Author(s):  
Soheil Sedaghat ◽  
Ommoleila Molavi ◽  
Akram Faridi ◽  
Ali Shayanfar ◽  
Mohammad Reza Rashidi
Keyword(s):  
High Performance ◽  
Accurate Method ◽  
Plasma Samples ◽  
Promising Target ◽  
Relative Standard ◽  
Dimerization Inhibitor ◽  
Oncogenic Protein ◽  
First Time ◽  
Transcription 3

Background: Signal transducer and activator of transcription 3 (STAT3), an oncogenic protein found constitutively active in many types of human malignancies, is considered to be a promising target for cancer therapy. Objective: In this study for the first time, a simple and accurate method has been developed for the determination of a STAT3 dimerization inhibitor called stattic in aqueous and plasma samples. Methods: A reverse-phase high-performance liquid chromatography (RP-HPLC) composed of C18 column as stationary phase, and the mixture of acetonitrile (60%) and water (40%) as mobile phase with a UV detection at 215 nm were applied for quantification of stattic. The developed method was validated by Food and Drug Administration (FDA) guideline. Results: The method provided a linear range between 1-40 and 2.5-40 µg mL-1 for aqueous and plasma samples, respectively, with a correlation coefficient of 0.999. The accuracy (as recovery) of the developed method was found to be between 95-105% for aqueous medium and 85-115% for plasma samples. The precision (as relative standard deviation) for aqueous and plasma samples was less than 6% and 15%, respectively. The sensitivity of the developed method based on FDA guideline was 1 µg mL-1 for aqueous and 2.5 µg mL-1 for plasma samples. Conclusion: These results show that the established method is a fast and accurate quantification for stattic in aqueous and plasma samples.

Carbon dots derived from Fusobacterium nucleatum for intracellular determination of Fe3+ and bioimaging both in vitro and in vivo

2021 ◽  
Author(s):  
Lijuan Liu ◽  
Shengting Zhang ◽  
Xiaodan Zheng ◽  
Hongmei Li ◽  
Qi Chen ◽  
...  
Keyword(s):  
Carbon Dots ◽  
Fusobacterium Nucleatum ◽  
Living Cells ◽  
First Time ◽  
Fluorescent Carbon Dots ◽  
Fluorescent Carbon

Fusobacterium nucleatum has been employed for the first time to synthesize fluorescent carbon dots which could be applied for the determination of Fe3+ ions in living cells and bioimaging in vitro and in vivo with excellent biocompatibility.

scholarly journals Experimental investigation to characterize simple versus multi scaling analysis of hydraulic conductivity at a mesoscale

2021 ◽  
Author(s):  
Guglielmo Federico Antonio Brunetti ◽  
Samuele De Bartolo ◽  
Carmine Fallico ◽  
Ferdinando Frega ◽  
Maria Fernanda Rivera Velásquez ◽  
...  
Keyword(s):  
Hydraulic Conductivity ◽  
Spatial Variability ◽  
Hydraulic Properties ◽  
Scaling Laws ◽  
Scaling Analysis ◽  
Field Scale ◽  
Porous Formation ◽  
Proper Design ◽  
First Time

AbstractThe spatial variability of the aquifers' hydraulic properties can be satisfactorily described by means of scaling laws. The latter enable one to relate the small (typically laboratory) scale to the larger (typically formation/regional) ones, therefore leading de facto to an upscaling procedure. In the present study, we are concerned with the spatial variability of the hydraulic conductivity K into a strongly heterogeneous porous formation. A strategy, allowing one to identify correctly the single/multiple scaling of K, is applied for the first time to a large caisson, where the medium was packed. In particular, we show how to identify the various scaling ranges with special emphasis on the determination of the related cut-off limits. Finally, we illustrate how the heterogeneity enhances with the increasing scale of observation, by identifying the proper law accounting for the transition from the laboratory to the field scale. Results of the present study are of paramount utility for the proper design of pumping tests in formations where the degree of spatial variability of the hydraulic conductivity does not allow regarding them as “weakly heterogeneous”, as well as for the study of dispersion mechanisms.

scholarly journals Potentiometric Response of Solid-State Sensors Based on Ferric Phosphate for Iron(III) Determination

Sensors ◽  
2021 ◽  
Vol 21 (5) ◽  
pp. 1612
Author(s):  
Andrea Paut ◽  
Ante Prkić ◽  
Ivana Mitar ◽  
Perica Bošković ◽  
Dražan Jozić ◽  
...  
Keyword(s):  
Silver Sulfide ◽  
Potential Change ◽  
Linear Potential ◽  
Response Characteristics ◽  
Potentiometric Response ◽  
Best Response ◽  
Body Design ◽  
Long Lifetime ◽  
First Time

A novel ion-selective electrode with membranes based on iron(III) phosphate and silver sulfide integrated into a completely new electrode body design has been developed for the determination of iron(III) cations. The best response characteristics with linear potential change were found in the iron(III) concentration range from 3.97× 10−5 to 10−2 mol L−1. The detection limit was found to be 2.41× 10−5 mol L−1 with a slope of –20.53 ± 0.63 and regression coefficient of 0.9925, while the quantification limit was 3.97× 10−5 M. The potential change per concentration decade ranged from –13.59 ± 0.54 to –20.53 ± 1.56 for Electrode Body 1 (EB1) and from –17.28 ± 1.04 to –24 ± 1.87 for Electrode Body 2 (EB2), which is presented for the first time in this work. The prepared electrode has a long lifetime and the ability to detect changes in the concentration of iron cations within 20 s. Membrane M1 showed high recoveries in the determination of iron cations in iron(III) standard solutions (98.2–101.2%) as well as in two different pharmaceuticals (98.6–106.5%). This proves that this type of sensor is applicable in the determination of ferric cations in unknown samples, and the fact that all sensor parts are completely manufactured in our laboratory proves the simplicity of the method.

scholarly journals Determination of Flavonoids Compounds of Three Species and Different Harvesting Periods in Crataegi folium Based on LC-MS/MS

Molecules ◽  
2021 ◽  
Vol 26 (6) ◽  
pp. 1602
Author(s):  
Ya-Ping Guo ◽  
Hong Yang ◽  
Ya-Li Wang ◽  
Xiao-Xiang Chen ◽  
Ke Zhang ◽  
...  
Keyword(s):  
Quantitative Analysis ◽  
Qualitative Analysis ◽  
Quantitative Method ◽  
Total Content ◽  
Qualitative And Quantitative Analysis ◽  
Pharmacological Activities ◽  
Time Saving ◽  
Qualitative And Quantitative ◽  
First Time

Crataegi folium have been used as medicinal and food materials worldwide due to its pharmacological activities. Although the leaves of Crataegus songorica (CS), Crataegus altaica (CA) and Crataegus kansuensis (CK) have rich resources in Xinjiang, China, they can not provide insights into edible and medicinal aspects. Few reports are available on the qualitative and quantitative analysis of flavonoids compounds of their leaves. Therefore, it is necessary to develop efficient methods to determine qualitative and quantitative flavonoids compounds in leaves of CS, CA and CK. In the study, 28 unique compounds were identified in CS versus CK by qualitative analysis. The validated quantitative method was employed to determine the content of eight flavonoids of the leaves of CS, CA and CK within 6 min. The total content of eight flavonoids was 7.8–15.1 mg/g, 0.1–9.1 mg/g and 4.8–10.7 mg/g in the leaves of CS, CA and CK respectively. Besides, the best harvesting periods of the three species were from 17th to 26th September for CS, from 30th September to 15th October for CA and CK. The validated and time-saving method was successfully implemented for the analysis of the content of eight flavonoids compounds in CS, CA and CK for the first time.

scholarly journals Fast and Reliable Multiresidue Analysis of Aromas in Wine by Means of Gas Chromatography Coupled with Triple Quadrupole Mass Spectrometry

Analytica ◽  
2021 ◽  
Vol 2 (2) ◽  
pp. 38-49
Author(s):  
Ettore Guerriero ◽  
Massimo Iorizzo ◽  
Marina Cerasa ◽  
Ivan Notardonato ◽  
Bruno Testa ◽  
...  
Keyword(s):  
Direct Injection ◽  
Headspace Analysis ◽  
White Wine ◽  
Quadrupole Mass ◽  
Multiresidue Analysis ◽  
Liquid Liquid Extraction ◽  
Volatile Organic ◽  
Steel Tank ◽  
First Time

The paper would like to show a direct injection into GC-MS/QqQ for the determination of secondary aromas in white wine samples fermented in two different ways. The procedure has been compared with more traditional methods used in this field, i.e., headspace analysis and liquid–liquid extraction. The application of such direct injection, for the first time in the literature, allows us to analyze Volatile Organic Compounds (VOCs) in the range 0.1–100 µg mL−1, with Limits of Detection (LODs) and Limits of Quantification (LOQs) between 0.01–0.05 µg mL−1 and 0.03–0.09 µg mL−1, respectively, intraday and interday below 5.6% and 8.5%, respectively, and recoveries above 92% at two different fortification levels. The procedure has been applied to real wine samples: it evidences how the fermentation in wood (cherry) barrel yields higher VOC levels than ones in wine fermented in steel tank, causing production of different secondary aromas and different relative flavors.

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