Characterization and Nozzle Test Experience of a Self Sealing Ceramic Matrix Composite for Gas Turbine Applications

Author(s):  
Eric P. Bouillon ◽  
Greg C. Ojard ◽  
G. Habarou ◽  
Patrick C. Spriet ◽  
Jean L. Lecordix ◽  
...  

Advanced materials have the potential to improve gas turbine engine durability. One general area of concern for durability is in the hot section components of the engine. Ceramic matrix composites offer improvements in durability at elevated temperatures with a corresponding reduction in weight for nozzles of gas turbine engines. Building on past material efforts, a next generation SiC/SiC composite with a self-sealing matrix has been developed for gas turbine applications. An extensive baseline test characterization has been done that shows the overall material suitability. Prior to ground engine testing, a reduced test matrix was undertaken to aggressively test the material in a long-term hold cycle at elevated temperatures and environments. This tensile low cycle fatigue testing was done in air and a 90% steam environment. While the steam environment aggressively attacked the material, no appreciable debit in material life was noted. Nondestructive testing and post test characterization of this testing were performed. After completion of the aggressive testing effort, two nozzle seals of constant thickness were fabricated and installed in an F100-PW-229 engine for accelerated mission testing. The self sealing CMC seals were tested for over 250 hours in accelerated conditions without damage. The results of the engine testing will be shown and overall conclusions drawn.

Author(s):  
Eric P. Bouillon ◽  
Patrick C. Spriet ◽  
Georges Habarou ◽  
Thibault Arnold ◽  
Greg C. Ojard ◽  
...  

Advanced materials are targeting durability improvement in gas turbine engines. One general area of concern for durability is in the hot section components of the engine. Ceramic matrix composites offer improvements in durability at elevated temperatures with a corresponding reduction in weight for nozzles of gas turbine engines. Building on past material efforts, ceramic matrix composites using a carbon and a SiC fiber with a self-sealing matrix have been developed for gas turbine applications. Prior to ground engine testing, a reduced test matrix was undertaken to aggressively test the material in a long-term hold cycle at elevated temperatures and environments. This tensile low cycle fatigue testing was done in air and a 90% steam environment. After completion of the aggressive testing effort, six nozzle seals were fabricated and installed in an F100-PW-229 engine for accelerated mission testing. The C fiber CMC and the SiC Fiber CMC were respectively tested to 600 and 1000 hours in accelerated conditions without damage. Engine testing is continuing to gain additional time and insight with the objective of pursuing the next phase of field service evaluation. Mechanical testing and post-test characterization results of this testing will be presented. The results of the engine testing will be shown and overall conclusions drawn.


Author(s):  
Michael J. L. Percival ◽  
Colin P. Beesley

Currently available Ceramic Matrix Composites (CMCs) have very low stress carrying capability if they are to achieve the service life required for application in gas turbine engines. As such, they are most likely to find their first applications in non-structural components with low mechanical loads, where the majority of the stress is thermally induced. The thermal cycling experienced in gas turbine engines, coupled with the necessary interfaces with surrounding metal components and other geometric features, means that these thermal stresses are often localised, but in order to produce a valid component design they may significantly exceed the maximum design stress. The aim of this paper is to discuss the implications for the life of the component of these excess stresses. This will cover the mechanisms for the propagation of localised damage in a strain controlled environment, and the effect of this damage on the thermal conductivity and hence on the induced thermal gradients and thermal strains. Strains corresponding to stresses considerably above the normally accepted design stress can be sustained for a considerable number of cycles, but the influence of extended time periods with damage at elevated temperatures remains unexplored.


Author(s):  
Andy Szweda ◽  
Steve Butner ◽  
John Ruffoni ◽  
Carlos Bacalski ◽  
Jay Lane ◽  
...  

Oxide/Oxide Ceramic Matrix Composites (CMCs) are an attractive class of materials for gas turbine hot section applications. The oxide fiber reinforcement and inherent matrix porosity contributes to favorable fracture toughness and thereby enhanced resistance against impact by foreign objects. Also, the oxide composition ensures superior environmental resistance against accelerated attack by corrosive species in the gas turbine hot section and resulting surface recession typically observed in silicon-based ceramic monolithic and composite materials. Under a program sponsored by the US National Institute of Standards and Technology (NIST) a hybrid oxide/oxide CMC system has been developed with potential application for stationary gas turbine hot section components. COI Ceramics, Inc. has fabricated subscale and full scale combustor liners which have been evaluated in rig and engine testing at Solar, and in field testing in a Solar Centaur® 50S engine at a commercial end user site. Following the conclusion of the NIST program in June 2003 the engine field testing is being continued under a Solar-led program sponsored by the US Dept. of Energy (DOE). As of November 2004, a hybrid oxide/oxide CMC outer combustor liner has accumulated 12,582 field test hours with 63 starts and an extensive material experience base has been developed. The paper will summarize the progress to-date for this hybrid CMC combustor liner development and demonstration, including selected fabrication approach, NDE, and rig/engine test experience.


2020 ◽  
Vol 299 ◽  
pp. 37-42
Author(s):  
O.A. Fomina ◽  
Andrey Yu. Stolboushkin

A model of the transition layer between the shell and the core of a ceramic matrix composite from coal waste and clay has been developed. The chemical, granulometric and mineral compositions of the beneficiation of carbonaceous mudstones and clay were studied. The technological and ceramic properties of raw materials for the samples manufacturing were determined. The method of manufacturing multilayer ceramic samples from coal waste, clay and their mixture is given. The number of transition layers in the contact zone between the clay shell and the core from coal wastes is determined. The deformation and swelling phenomena of model samples from coal wastes, clay, and their mixtures were revealed at the firing temperature of more than 1000 °C. The formation of a reducing ambient in the center of the sample with insufficient air flow is shown. The influence of the carbonaceous particles amount and the ferrous form iron oxide in the coal wastes on the processes of expansion of multilayer samples during firing has been established.


Author(s):  
N. Kedir ◽  
C. Gong ◽  
L. Sanchez ◽  
M. J. Presby ◽  
S. Kane ◽  
...  

Erosion behavior of a large number of gas-turbine grade ceramic matrix composites (CMCs) was assessed using fine to medium grain garnet erodents at velocities of 200 and 300 m/s at ambient temperature. The CMCs used in the current work were comprised of nine different SiC/SiCs, one SiC/C, one C/SiC, one SiC/MAS, and one oxide/oxide. Erosion damage was quantified with respect to erosion rate and the damage morphology was assessed via SEM and optical microscopy in conjunction with 3-D image mapping. The CMCs response to erosion appeared to be very complicated due to their architectural complexity, multiple material constituents, and presence of pores. Effects of architecture, material constituents, density, matrix hardness, and elastic modulus of the CMCs were taken into account and correlated to overall erosion behavior. The erosion of monolithic ceramics such as silicon carbide and silicon nitrides was also examined to gain a better understanding of the governing damage mechanisms for the CMC material systems used in this work.


2000 ◽  
Vol 122 (2) ◽  
pp. 212-218 ◽  
Author(s):  
Karren L. More ◽  
Peter F. Tortorelli ◽  
Mattison K. Ferber ◽  
Larry R. Walker ◽  
James R. Keiser ◽  
...  

A high-temperature, high-pressure, tube furnace has been used to evaluate the long term stability of different monolithic ceramic and ceramic matrix composite materials in a simulated combustor environment. All of the tests have been run at 150 psia, 1204°C, and 15 percent steam in incremental 500 h runs. The major advantage of this system is the high sample throughput; >20 samples can be exposed in each tube at the same time under similar exposure conditions. Microstructural evaluations of the samples were conducted after each 500 h exposure to characterize the extent of surface damage, to calculate surface recession rates, and to determine degradation mechanisms for the different materials. The validity of this exposure rig for simulating real combustor environments was established by comparing materials exposed in the test rig and combustor liner materials exposed for similar times in an actual gas turbine combustor under commercial operating conditions. [S0742-4795(00)02402-9]


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