Nondestructive Evaluation of Some Medical Prosthesis Components Made From Syntherized Zirconium Oxides Using US Spectroscopy

Author(s):  
Raimond Grimberg ◽  
Adriana Savin ◽  
Rozina Steigmann ◽  
Alina Bruma ◽  
Sorin Leitoiu

This paper presents the resonant ultrasound spectroscopy method that allows, in principle, the determination of the density changing, elastic and geometrical properties of the object to be examined. The method is applied at the noninvasive evaluation of the femoral head prosthetic and of the artificial cervical discs made from yttria stabilized tetragonal zirconia. In the case of density changing, the spectral lines are displacing to smaller frequencies and in the case of the cracks, supplementary peaks appear.

Author(s):  
Adriana Savin ◽  
Mihai Liviu Craus ◽  
Rozina Steigmann

This paper presents a possibility to use Resonant Ultrasound Spectroscopy as nondestructive evaluation method for ceramic elements of prosthesis such as ceramic femoral heads. With this method can be emphasized the incorrect sintering of these elements as well as eventually cracks. If the number of resonance peaks is big enough, the elements of elasticity matrix can be determined, demonstrated by effective measurements on zirconia with different stabilizers cylindrical samples taken into study.


2018 ◽  
Vol 64 (246) ◽  
pp. 669-674
Author(s):  
COLIN M. SAYERS

ABSTRACTMeasured elastic stiffnesses of ice polycrystals decrease with increasing temperature due to a decrease in grain boundary stiffness with increasing temperature. In this paper, we represent grain boundaries as imperfectly bonded interfaces, across which traction is continuous, but displacement may be discontinuous. We express the additional compliance due to grain boundaries in terms of a second-rank and a fourth-rank tensor, which quantify the effect on elastic wave velocities of the orientation distribution as well as the normal and shear compliances of the grain boundaries. Measurement of the elastic stiffnesses allows determination of the components of these tensors. Application of the method to resonant ultrasound spectroscopy measurements made on ice polycrystals enables determination of the ratio BN/BS of the normal to shear compliance of the grain boundaries, which are found to be more compliant in shear than in compression. The ratio BN/BS is small at low temperatures, but increases as temperature increases, implying that the normal compliance increases relative to the shear compliance as temperature increases.


2006 ◽  
Vol 321-323 ◽  
pp. 1576-1579
Author(s):  
Yong Moo Cheong ◽  
Young Suk Kim

Zirconium alloys are used for many applications in nuclear components, such as the pressure tube material in a pressurized heavy water reactor, nuclear fuel cladding, etc. One of the problems during the operation of a nuclear reactor is the degradation of the zirconium alloys, which is due to an increase of the hydrogen content in the zirconium alloy. Therefore a non-destructive determination of the hydrogen concentration in zirconium alloy is one of the important issues that need to be addressed. The resonant ultrasound spectroscopy (RUS) technique is evaluated for a characterization of the hydrogen concentration in Zr-2.5Nb alloy. Referring to the terminal solid solubility for dissolution (TSSD) of Zr-2.5Nb alloy, the plot of the mechanical damping coefficient (Q-1) versus the temperature or the deviation of the resonant frequency for the temperature (df/dT) versus the temperature was correlated for the hydrogen concentration in Zr-2.5Nb alloy. It was found that the temperature at an abrupt change of the slope can be correlated with the hydrogen concentration of the Zr-2.5Nb alloy.


Metals ◽  
2020 ◽  
Vol 10 (10) ◽  
pp. 1383
Author(s):  
Petr Sedlák ◽  
Michaela Janovská ◽  
Lucie Bodnárová ◽  
Oleg Heczko ◽  
Hanuš Seiner

We discuss the suitability of laser-based resonant ultrasound spectroscopy (RUS) for the characterization of soft shearing modes in single crystals of shape memory alloys that are close to the transition temperatures. We show, using a numerical simulation, that the RUS method enables the accurate determination of the c′ shear elastic coefficient, even for very strong anisotropy, and without being sensitive to misorientations of the used single crystal. Subsequently, we apply the RUS method to single crystals of three typical examples of shape memory alloys (Cu-Al-Ni, Ni-Mn-Ga, and NiTi), and discuss the advantages of using the laser-based contactless RUS arrangement for temperature-resolved measurements of elastic constants.


2010 ◽  
Vol 2010 ◽  
pp. 1-13 ◽  
Author(s):  
G. Li ◽  
J. R. Gladden

The measurement of elastic constants plays an important role in condensed matter physics and materials characterization. This paper presents the resonant ultrasound spectroscopy (RUS) method for the determination of elastic constants in a single crystal or amorphous solid. In RUS, the measured resonance spectrum of a properly prepared sample and other information such as geometry, density, and initial estimated elastic constants are used to determine the elastic constants of the material. We briefly present the theoretical background and applications to specific materials; however, the focus of this review is on the technical applications of RUS, especially those for high-temperature measurements.


2018 ◽  
Author(s):  
Carly Michelle Donahue ◽  
Peter Andreas Schulze ◽  
David Steven Moore ◽  
Timothy James Ulrich, II

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