Microstructural Evolution During a Solid State Tube Pinch Weld of Type 304l Stainless Steel

2021 ◽  
Vol 143 (5) ◽  
Author(s):  
Paul S. Korinko

Abstract Microstructure development is examined for a specialized spot weld that is used as a solid-state closure process for austenitic stainless steel tubing, referred to as pinch welding. In order to elucidate the microstructural evolution of the weld, a series of test welds were made at nominal conditions using tubing and production like components. These pinch welds normally terminate after twelve cycles of a 60 Hz AC weld process. In this study, production tubes were welded from one to twelve cycles and the microstructure and weld variables after each individual weld cycle number were characterized using radiography and optical metallography. Two electrochemical etchants were used to highlight different microstructural features. The study revealed that: (1) this type pinch weld is largely complete after about six cycles of 60 Hz AC current, half the weld time utilized; (2) the resistance, deformation, and closure length approach “steady-state” conditions after six cycles; and (3) both oxalic and nitric acid electrolytic etchants are useful for highlighting specific microstructural attributes of type 304 L stainless steel. Finally, two distinct microstructural regions can be identified for these welds: the edge of the weld, which is driven by concentrated deformation, recrystallization, and grain growth, and the center region, which is more typical of forge welding and micro-asperity breakdown followed by diffusion and grain-growth.

Author(s):  
Paul S. Korinko

Abstract Microstructure development is examined for a specialized spot weld that is used as a solid-state closure process for stainless steel tubing, referred to as pinch welding. In order to elucidate the microstructural evolution of the weld, a series of test welds were made at nominal conditions using both tubes, used in test articles and production like components. These pinch welds normally terminate after twelve cycles of a 60 Hz AC weld process. In this study, tubes with different thermal processing history were welded from one to twelve cycles and the microstructure and weld variables after each individual weld cycle number were characterized using radiography and optical metallography. Two etchants were used that highlighted different microstructural features. The study revealed that: (1) this type pinch weld is largely complete after about six cycles of 60 Hz AC current, half the weld time utilized; (2) the resistance, deformation, and closure length approach “steady state” conditions after six cycles; and (3) both oxalic and nitric acid electrolytic etchants are useful for highlighting specific microstructural attributes of type 304L stainless steel. Finally, two distinct microstructural regions can be identified for these welds: the edge of the weld which is driven by concentrated deformation, recrystallization and grain growth and the center region which is more typical of forge welding and micro-asperity breakdown followed by diffusion and grain-growth. The bond line of annealed tubes exhibits fewer indications and less contamination than that of the partially annealed and as-received cold worked tubes.


2006 ◽  
Vol 116-117 ◽  
pp. 681-685 ◽  
Author(s):  
Jing Yuan Li ◽  
Sumio Sugiyama ◽  
Jun Yanagimoto

Thixoforming or Semi-Solid Metal Forming offers many advantages in comparison with casting and conventional forging. The purpose of the present study is to provide the basic microstructure and deformation data for austenitic and ferritic stainless steel under mushy state. As well known, the stainless steels solidify in different modes according to the different chemical compositions. In this paper, microstructural evolution of austenitic stainless steel type 304 which solidifies in FA mode ( L → L +δ → L +δ +γ →δ +γ →γ ),austenitic stainless steel type 310S which solidifies in A mode ( L → L +γ →γ ), and ferritic stainless steel type 430 which solidifies in F mode ( L → L +δ →δ )are investigated during partial remelting by way of SIMA (Strain Induced Melted Activation). The results show that A and F mode of stainless steels melt directly at the grain boundary without phase transformation during reheating. A banded structure, originating from the primary dendritic segregation of the original ingots, is observed in type 310S steel during further heating. On the other hand, a perfect globular and insegregative two-phase semi-solid structure L +δ can be obtained while heated beyond the banded three-phase L +δ +γ semi-solid state in FA mode austenitic stainless steel type 304. This spheroidization can be attributed to the peritectic reaction occurred in the L +δ +γ semi-solid state. In addition, simple compression tests of these alloys in semi-solid state for varied combination of deformation rate and deformation temperature are conducted to examine the deformation behavior of stainless steel. Flow stress curves exhibit abrupt change in various alloys, even though in the same alloy such as type 304, various flow stresses are observed according to the difference in inner microstructure or morphology. Stress of type 310S steel shows the most reduction as the deformation temperature increasing at the same strain rate condition. The Liquid is centralized to periphery by the compression force in all deformed test pieces. Fracture, observed in all alloys except type 304 steel in globular L +δ semi-solid state, should be resulted from the lack of liquid in L +δ +γ state of type 304 steel and solidification crack in type 310S and type 430 steel. Deformation of solid particles occurs only in L +δ +γ state of type 304 steel. Last in this paper, various deformation mechanisms are proposed for various microstructures.


Alloy Digest ◽  
2003 ◽  
Vol 52 (2) ◽  

Abstract Carpenter Project 70+ Type 304/304L is a modified version of Type 304/304L stainless steel with improved machinability when compared to conventional 304 (Alloy Digest SS-418, revised September 1997) and 304L (Alloy Digest SS-513, revised November 1997). The alloys are nonhardenable austenitic chromium-nickel steels and are good general-purpose materials for simple and complex parts. This datasheet provides information on composition, physical properties, and elasticity. It also includes information on corrosion resistance as well as forming, heat treating, machining, and joining. Filing Code: SS-875. Producer or source: Carpenter Specialty Alloys.


2000 ◽  
Vol 625 ◽  
Author(s):  
John A. Brooks ◽  
Thomas J. Headley ◽  
Charles V. Robino

AbstractLaser deposits fabricated from two different compositions of 304L stainless steel powder were characterized to determine the nature of the solidification and solid state transformations. One of the goals of this work was to determine to what extent novel microstructures consisting of single-phase austenite could be achieved with the thermal conditions of the LENS process. Although ferrite-free deposits were not obtained, structures with very low ferrite content were achieved. It appeared that, with slight changes in alloy composition, this goal could be met via two different solidification and transformation mechanisms.


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