The Effect of Process Parameters on the Structural Energetic Properties of Additively Manufactured Reactive Structures

Author(s):  
Trevor J. Fleck ◽  
Timothy D. Manship ◽  
Steven F. Son ◽  
Jeffrey F. Rhoads

Abstract This paper investigates the ability of an aluminum-fluoropolymer energetic material to act as a multifunctional energetic structural material (MESM). The mechanical properties of the material were determined by performing quasi-static tensile testing of 3D printed dogbones. Samples were prepared with and without particle loading, as well as with different print directions, in order to gain a fundamental understanding of how these parameters affect the mechanical properties of the material. Larger truss samples were printed in order to simulate realistic structural elements. Samples were printed in different directions and burned to determine this parameter’s effect on the combustion performance of the material. The aluminum polyvinylidene fluoride mixtures considered were shown to have viable structural capabilities as well as sufficient combustion performance. The structural energetic capabilities of the formulations considered, paired with the material’s ability to be 3D printed, could enable a number of interesting applications in the aerospace and defense industry.

2021 ◽  
Vol 2 (4) ◽  
pp. 942-955
Author(s):  
Carmela Riccio ◽  
Marco Civera ◽  
Oliver Grimaldo Ruiz ◽  
Perla Pedullà ◽  
Mariana Rodriguez Reinoso ◽  
...  

Different mechanical properties characterise the materials of 3D printed components, depending on the specific additive manufacturing (AM) process, its parameters, and the post-treatment adopted. Specifically, stereolithography (SLA) uses a photopolymerisation technique that creates solid components through selective solidification. In this study, 72 specimens were 3D printed using 12 commercial-grade methacrylate resins and tested under uniaxial tensile loads. The resin specimens were evaluated before and after curing. The recommended cure temperature and time were followed for all materials. The stress-strain curves measured during the testing campaign were evaluated in terms of maximum tensile strength, Young’s modulus, ductility, resilience, and toughness. The results reveal that the curing process increases the material stiffness and resistance to tensile loads. However, it was found that the curing process generally reduces the plasticity of the resins, causing a more or less marked brittle behaviour. This represents a potential limitation to the use of SLA 3D printing for structural elements which require some plasticity to avoid dangerous sudden failures.


2021 ◽  
pp. 1-18
Author(s):  
N. Vinoth Babu ◽  
N. Venkateshwaran ◽  
N. Rajini ◽  
Sikiru Oluwarotimi Ismail ◽  
Faruq Mohammad ◽  
...  

Materials ◽  
2020 ◽  
Vol 14 (1) ◽  
pp. 126
Author(s):  
Viktoria Hoppe ◽  
Patrycja Szymczyk-Ziółkowska ◽  
Małgorzata Rusińska ◽  
Bogdan Dybała ◽  
Dominik Poradowski ◽  
...  

The purpose of this work is to obtain comprehensive reference data of the Ti-13Nb-13Zr alloy base material: its microstructure, mechanical, and physicochemical properties. In order to obtain extensive information on the tested materials, a number of examination methods were used, including SEM, XRD, and XPS to determine the phases occurring in the material, while mechanical properties were verified with static tensile, compression, and bending tests. Moreover, the alloy’s corrosion resistance in Ringer’s solution and the cytotoxicity were investigated using the MTT test. Studies have shown that this alloy has the structure α’, α, and β phases, indicating that parts of the β phase transformed to α’, which was confirmed by mechanical properties and the shape of fractures. Due to the good mechanical properties (E = 84.1 GPa), high corrosion resistance, as well as the lack of cytotoxicity on MC3T3 and NHDF cells, this alloy meets the requirements for medical implant materials. Ti-13Nb-13Zr alloy can be successfully used in implants, including bone tissue engineering products and dental applications.


Metals ◽  
2021 ◽  
Vol 11 (3) ◽  
pp. 524
Author(s):  
Maider Arana ◽  
Eneko Ukar ◽  
Iker Rodriguez ◽  
Amaia Iturrioz ◽  
Pedro Alvarez

With the advent of disruptive additive manufacturing (AM), there is an increasing interest and demand of high mechanical property aluminium parts built directly by these technologies. This has led to the need for continuous improvement of AM technologies and processes to obtain the best properties in aluminium samples and develop new alloys. This study has demonstrated that porosity can be reduced below 0.035% in area in Al-Mg samples manufactured by CMT-based WAAM with commercial filler metal wires by selecting the correct shielding gas, gas flow rate, and deposition strategy (hatching or circling). Three phase Ar+O2+N2O mixtures (Stargold®) are favourable when the hatching deposition strategy is applied leading to wall thickness around 6 mm. The application of circling strategy (torch movement with overlapped circles along the welding direction) enables the even build-up of layers with slightly thicker thickness (8 mm). In this case, Ar shielding gas can effectively reduce porosity if proper flow is provided through the torch. Reduced gas flows (lower than 30 Lmin) enhance porosity, especially in long tracks (longer than 90 mm) due to local heat accumulation. Surprisingly, rather high porosity levels (up to 2.86 area %) obtained in the worst conditions, had a reduced impact on the static tensile test mechanical properties, and yield stress over 110 MPa, tensile strength over 270 MPa, and elongation larger than 27% were achieved either for Ar circling, Ar hatching, or Stargold® hatching building conditions. In all cases anisotropy was lower than 11%, and this was reduced to 9% for the most appropriate shielding conditions. Current results show that due to the selected layer height and deposition parameters there was a complete re-melting of the previous layer and a thermal treatment on the prior bottom layer that refined the grain size removing the original dendritic and elongated structure. Under these conditions, the minimum reported anisotropy levels can be achieved.


Polymers ◽  
2021 ◽  
Vol 13 (9) ◽  
pp. 1394
Author(s):  
Yong Sang Cho ◽  
So-Jung Gwak ◽  
Young-Sam Cho

In this study, we investigated the dual-pore kagome-structure design of a 3D-printed scaffold with enhanced in vitro cell response and compared the mechanical properties with 3D-printed scaffolds with conventional or offset patterns. The compressive modulus of the 3D-printed scaffold with the proposed design was found to resemble that of the 3D-printed scaffold with a conventional pattern at similar pore sizes despite higher porosity. Furthermore, the compressive modulus of the proposed scaffold surpassed that of the 3D-printed scaffold with conventional and offset patterns at similar porosities owing to the structural characteristics of the kagome structure. Regarding the in vitro cell response, cell adhesion, cell growth, and ALP concentration of the proposed scaffold for 14 days was superior to those of the control group scaffolds. Consequently, we found that the mechanical properties and in vitro cell response of the 3D-printed scaffold could be improved by kagome and dual-pore structures through DfAM. Moreover, we revealed that the dual-pore structure is effective for the in vitro cell response compared to the structures possessing conventional and offset patterns.


2020 ◽  
Vol 90 (21-22) ◽  
pp. 2399-2410 ◽  
Author(s):  
Shahbaj Kabir ◽  
Hyelim Kim ◽  
Sunhee Lee

This study has investigated the physical properties of 3D-printable shape memory thermoplastic polyurethane (SMTPU) filament and its 3D-printed sinusoidal pattern obtained by fused deposition modeling (FDM) technology. To investigate 3D filaments, thermoplastic polyurethane (TPU) and SMTPU filament were examined by conducting infrared spectroscopy, x-ray diffraction (XRD), dynamic mechanical thermal analysis (DMTA), differential scanning calorimetry (DSC) and a tensile test. Then, to examine the 3D-printed sinusoidal samples, a sinusoidal pattern was developed and 3D-printed. Those samples went through a three-step heating process: (a) untreated state; (b) 5 min heating at 70°C, cooling for 30 min at room temperature; and (c) a repeat of step 2. The results obtained by the three different heating processes of the 3D-printed sinusoidal samples were examined by XRD, DMTA, DSC and the tensile test to obtain the effect of heating or annealing on the structural and mechanical properties. The results show significant changes in structure, crystallinity and thermal and mechanical properties of SMTPU 3D-printed samples due to the heating steps. XRD showed the increase in crystallinity with heating. In DMTA, storage modulus, loss modulus and the tan σ peak position also changed for various heating steps. The DSC result showed that the Tg for different steps of the SMTPU 3D-printed sample remained almost the same at around 51°C. The tensile property of the TPU 3D-printed sinusoidal sample decreased in terms of both load and elongation with increased heating processes, while for the SMTPU 3D-printed sinusoidal sample, the load decreased but elongation increased about 2.5 times.


2020 ◽  
Author(s):  
Qinfei Xu ◽  
Yingshuang Shang ◽  
Zilong Jiang ◽  
Zhaoyang Wang ◽  
Chenyi Zhou ◽  
...  

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