Effect of Post Heat Treatment on the Microstructure and Tensile Properties of Nano TiC Particulate Reinforced Inconel 718 by Selective Laser Melting

2020 ◽  
Vol 142 (5) ◽  
Author(s):  
Yachao Wang ◽  
Jing Shi
Keyword(s):  
Electron Microscopy ◽  
Heat Treatment ◽  
Selective Laser Melting ◽  
Inconel 718 ◽  
Solution Treatment ◽  
Nano Particles ◽  
Solution Temperature ◽  
Laser Melting ◽  
Post Heat Treatment ◽  
Particulate Reinforced

Abstract To strengthen the metal components by selective laser melting (SLM), adding reinforcement particles and applying post treatments are generally regarded as the two effective means. However, how post heat treatment affects the properties of nano particulate reinforced metal composites obtained by laser additive manufacturing (AM) processes has rarely been studied. In this study, Inconel 718 matrix composite reinforced by 0.5 wt% nano TiC particles was prepared using SLM. To evaluate the effect of the heat treatment routines on the performance of the SLM-produced composite, two levels of solution temperature (980 and 1100 °C) were designed, and the solution treatment was followed by a standard two-step aging (720 °C for 8 h and 620 °C for 8 h). Scanning electron microscopy (SEM) and electron backscatter diffraction (EBSD) observations were performed to examine the microstructure, and transmission electron microscopy (TEM) observation was conducted to characterize the morphologies of incorporated nano particles and precipitated phases. Tensile tests were conducted to evaluate the mechanical properties of the formed composites. It was found that nano particles can effectively strengthen the metal matrix under both as-built and heat-treated conditions, and the material undergoes static recrystallization during the post heat treatment. Also, it was discovered that nano TiC particles play an important role in refining the microstructure of Inconel 718 composite below 980 °C. The maximum tensile strength of 1370 MPa was observed under 980 °C + aging condition, representing a 16% increase as compared with the unreinforced Inconel 718.

Effect of Solution Treatment on Microstructure and Mechanical Properties of Graphene Nanoplatelets Reinforced Inconel 718 Composites by Selective Laser Melting

2016 ◽  
Author(s):  
Yachao Wang ◽  
Jing Shi ◽  
Xiaoyang Deng ◽  
Shiqiang Lu
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Additive Manufacturing ◽  
Selective Laser Melting ◽  
Inconel 718 ◽  
Solution Treatment ◽  
Graphene Nanoplatelets ◽  
Filler Material ◽  
Strengthening Effect ◽  
Laser Melting

Graphene nanoplatelets (GNPs) have many outstanding properties, such as high mechanical strengths, light weight, and high electric conductivity. These unique properties make it an ideal filler material for various composites. On the other hand, the development MMNCs (metal matrix nanocomposites) through additive manufacturing (AM) processes has become a major innovation in the field of advanced structural materials, owing to shorter production lead time, less material waste, high production flexibility. It is of great innovativeness to have the attractive features combined to produce GNPs reinforced MMNCs using AM techniques. In addition, metal components produced by laser assisted additive manufacturing (LAAM) methods usually have inferior mechanical properties, as compared to the counterparts by the traditional metal forming processes. To achieve optimized mechanical properties, the obtained MMNCs are subjected to various post treatment routines and the effect of post heat treatment on material properties is investigated. In this study, pure Inconel 718 and GNPs reinforced IN718 with 1.1 vol.% and 4.4 vol.% filler material are fabricated by selective laser melting (SLM). Room temperature tensile tests are conducted to evaluate the tensile properties. Scanning electron microscopy (SEM) observations are conducted to analyze the microstructure of materials and to understand the reinforcing mechanism. It is found that fabrication of GNPs reinforced MMC using SLM is a viable approach. The obtained composites possess dense microstructure and enhanced tensile strength. The strengthening effect and mechanisms involved in the composites are discussed. Solution treatments at three levels of temperature (940, 980, and 1020°C) for 1 hour period are carried out to evaluate the effect of the heat treatment on the material microstructure and therefore the resulted mechanical properties of the composite material. The results of samples with and without heat treatment are also compared. The experiments results indicate that that addition of GNPs into Inconel 718 results in significant strength improvement. Moreover, at any volume content of reinforcement, higher solution treatment leads to lower strength, mainly due to coarsened microstructure. The addition of GNPs effectively inhibits the grain growth during the post heat process and the average grain size is significantly refined compared to unreinforced samples. Moreover, through the investigation of various strengthening mechanisms, it is found that Orowan strengthening effect is small and can be neglected for both as-built and heat treated conditions. Load transfer effect is the dominating strengthening effect among all contributors and solution treatment significantly reduces thermal mismatch strengthening.

scholarly journals Effects of post heat treatment on the microstructure evolution of Inconel 718 manufactured by selective laser melting

2021 ◽  
Vol 8 (9) ◽  
pp. 095801
Author(s):  
Tao Song ◽  
Zhixiang Xue ◽  
Guanbing Ma ◽  
Yang Chen ◽  
Shuxian Yuan ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Selective Laser Melting ◽  
Microstructure Evolution ◽  
Inconel 718 ◽  
Laser Melting ◽  
Post Heat Treatment

Microstructural Evolution and Phase Transformation on the X-Y Surface of Inconel 718 Ni-Based Alloys Fabricated by Selective Laser Melting under Different Heat Treatment

2019 ◽  
Vol 38 (2019) ◽  
pp. 229-236
Author(s):  
Peng Liu ◽  
Siyu Sun ◽  
Meiqing Cao ◽  
Jianhong Gong ◽  
Jiaying Hu
Keyword(s):  
Heat Treatment ◽  
Solid Solution ◽  
Phase Transformation ◽  
Selective Laser Melting ◽  
Inconel 718 ◽  
Solution Process ◽  
Surface Hardness ◽  
Solution Temperature ◽  
Air Cooling ◽  
Laser Melting

AbstractMicrostructure, hardness, precipitates and phase transformation on the X-Y surface of Inconel 718 Ni-based alloys fabricated by selective laser melting (SLM) were studied before and after a suitable heat treatment. The test results show that the obvious weld beads structure was observed on the surface of the as-built alloys, and the microstructure shows seriously inhomogeneous with distributing columnar crystals and fine dendrites. When the 720°C, 3 h/furnace cooling+620°C and 3 h/air cooling was used, the columnar and small dendritic crystals begun to transform into bulk crystals, and the weld beads structure disappeared instantly. The X-Y surface hardness of alloys is about HV490-540, which is higher than the one of other heat treatment processes. With the increase of solid solution temperature, the microstructure on the surface of alloys shows an obvious refining characterization. The hardness value on the surface was also reduced gradually. The typical columnar crystals, dendrites, intermetallic compounds and precipitated hardening phase (Cr-Fe-Mo-Ni, FeNi and Ni8Nb) were also reduced or could not be found. Under the solid solution process of 950°C, the fine homogeneous δ phase and γ′ phase in the grain or near the grain boundary had an important effect on the suitable surface hardness value (HV476-500) of alloys.

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