scholarly journals Measurements of the Flow in the Vicinity of an Additively Manufactured Turbine Leading-Edge Using X-Ray Particle Tracking Velocimetry

2020 ◽  
Vol 142 (5) ◽  
Author(s):  
Alex Ruiz ◽  
Kamel Fezzaa ◽  
Jayanta Kapat ◽  
Samik Bhattacharya
Keyword(s):  
Velocity Field ◽  
Turbine Blade ◽  
Particle Tracking ◽  
High Speed ◽  
Particle Tracking Velocimetry ◽  
National Laboratory ◽  
Argonne National Laboratory ◽  
Leading Edge ◽  
Inlet Channel ◽  
X Ray

Abstract X-ray particle tracking velocimetry (PTV) is performed, for the first time, to measure the velocity field inside a leading-edge of a turbine blade made by laser-additive-manufacturing (LAM) process. The traditional showerhead holes were replaced by a porous matrix in the leading-edge. The flow through such a leading-edge piece cannot be faithfully recreated by traditional prototype testing methods due to the surface roughness and imperfections caused by LAM process. Hence, direct measurement is the only option. However, it is difficult to measure flow inside such pieces with traditional velocimetry measurements due to the existence of metallic walls. Moreover, small internal size and high flow speeds call for a measurement technique with high spatial and temporal resolutions. To address these issues, we performed time-resolved X-ray PTV using the Advanced Photon Source (APS) synchrotron facility at the Argonne National Laboratory (ANL). A hydraulic system was constructed to run water, mixed with seeding particles, through the leading-edge piece. A high-speed camera captured the images of the seeding particles, which were later processed to create particle tracks. The time-averaged velocity field showed distinct pairs of vortices located in front of the porous outlet inside the leading-edge piece. The inlet channel showed reversed flow due to partial obstruction by the porous inlet of the test piece. Such knowledge of the flow field inside a leading-edge of a turbine blade will help us to design better cooling paths leading to higher cooling efficiency and increased life-span of a turbine blade.

Investigation of microstructural changes in impacted polyurea coatings using small angle X-ray scattering (SAXS)

2011 ◽  
Vol 26 (2) ◽  
pp. 149-154 ◽  
Author(s):  
Edward Balizer ◽  
Jeffry Fedderly ◽  
Gilbert Lee ◽  
Susan Bartyczak ◽  
Willis Mock
Keyword(s):  
Strain Hardening ◽  
Small Angle ◽  
High Speed ◽  
Soft Segment ◽  
National Laboratory ◽  
Argonne National Laboratory ◽  
Steel Cylinder ◽  
X Ray ◽  
X Ray Scattering ◽  
Ray Scattering

Three polyureas with decreasing soft segment molecular weights of 1000, 650, and a 250/1000 blend were molded onto circular steel plates and then impacted with a high speed (275 m/s) conical-shaped steel cylinder. The polyurea layer of the post mortem bilayers was characterized on a molecular level by small angle synchrotron X-ray scattering (SAXS) at the Advanced Photon Source at the Argonne National Laboratory. Analysis revealed that the hard domains of the polyureas with lower molecular weight soft segments reformed and oriented over a greater area of the coating, thus increasing the polymer strain hardening and resulting in visibly less out of plane bilayer deformation. This agrees with the hypothesis that polymer strain hardening is a mechanism that retards necking failure of the metal plate.

scholarly journals Quantitative analysis of dribble volumes and rates using three-dimensional reconstruction of X-ray and diffused back-illumination images of diesel sprays

2019 ◽  
Vol 21 (1) ◽  
pp. 43-54 ◽  
Author(s):  
Vitaliy Sechenyh ◽  
Daniel J Duke ◽  
Andrew B Swantek ◽  
Katarzyna E Matusik ◽  
Alan L Kastengren ◽  
...  
Keyword(s):  
High Speed ◽  
Imaging System ◽  
Process Analysis ◽  
National Laboratory ◽  
Argonne National Laboratory ◽  
Injection Pressure ◽  
X Ray ◽  
Temperature Conditions ◽  
Processing Approach ◽  
Wide Range

Post-injection fuel dribble is known to lead to incomplete atomisation and combustion due to the release of slow-moving, and often surface-bound, liquid fuel after the end of injection. This can have a negative effect on engine emissions, performance and injector durability. To better quantify this phenomenon, we developed an image-processing approach to measure the volume of ligaments produced during the end of injection. We applied our processing approach to an Engine Combustion Network ‘Spray B’ 3-hole injector, using datasets from 220 injections generated by different research groups, to decouple the effect of gas temperature and pressure on the fuel dribble process. High-speed X-ray phase-contrast images obtained at room temperature conditions (297 K) at the Advanced Photon Source at Argonne National Laboratory, together with diffused back-illumination images captured at a wide range of temperature conditions (293–900 K) by CMT Motores Térmicos were analysed and compared quantitatively. We found a good agreement between image sets obtained by Argonne National Laboratory and CMT Motores Térmicos using different imaging techniques. The maximum dribble volume within the field of view of the imaging system and the mean rate of fuel dribble were considered as characteristic parameters of the fuel dribble process. Analysis showed that the absolute mean dribble rate increases with temperature when injection pressure is higher than 1000 bar and slightly decreases at high injection pressures (>500 bar) when temperature is close to 293 K. Larger maximum volumes of the fuel dribble were observed at lower gas temperatures (∼473 K) and low gas pressures (<30 bar), with a slight dependence on injection pressure.

scholarly journals High Speed X-Ray Imaging for Nozzle Exit Velocity and Density Distribution Measurements of GDI Nozzles

2017 ◽  
Author(s):  
Raphael Distler ◽  
Christoph Hamann ◽  
Martin Krämer ◽  
Eberhard Kull ◽  
Michael Wensing ◽  
...  
Keyword(s):  
High Speed ◽  
Phase Contrast ◽  
Force Measurement ◽  
National Laboratory ◽  
Measurement Techniques ◽  
Argonne National Laboratory ◽  
X Ray ◽  
X Ray Imaging ◽  
Primary Breakup ◽  
Nozzle Exit Velocity

Investigation of the primary breakup region of gasoline sprays is important for future nozzle development. It improvesthe principal understanding of inner nozzle flow and spray breakup. It also allows validating and developingCFD models. Due to the high optical density common measurement techniques like Phase Doppler Anemometryreach their limit in optical dense sprays as in the primary breakup region. High Speed X-Ray Imaging is capable tomeasure 2D velocity distributions directly at the spray hole exit. For generating the intense X-Ray beam the synchrotronAdvanced Photon Source at Argonne National Laboratory is used. Passing through the spray the X-Raybeam is changed by two different physical principles: absorption and phase contrast. Absorption can be applied tomeasure the density of the spray. Phase contrast is used to visualize the borders of droplets and ligaments withhigh contrast. The accelerated electron bunches inside the synchrotron have a constant period length to each other.This leads to an accurate pulsed X-Ray beam (periodicity: 68 ns). The use of multi exposure with very short X-Raypulses (17 ns) shows the traveled distance of the spray droplets and ligaments. The spray speed (150-250 m/s) iscalculated by dividing these distances with the time gap between two X-Ray pulses. The X-Ray measured densitydistributions and velocity distributions are combined to calculate the spray force rate. The so gained force rate isvalidated with a spray force measurement performed at the Spray Momentum Test Bench (SMTB) at ContinentalAutomotive GmbH. The study is focusing on the measurement setup of High Speed X-Ray Imaging at ArgonneNational Laboratory and the evaluation algorithms.DOI: http://dx.doi.org/10.4995/ILASS2017.2017.4598

Synchrotron X-ray studies of metal-organic framework M2(2,5-dihydroxyterephthalate), M = (Mn, Co, Ni, Zn) (MOF74)

2012 ◽  
Vol 27 (4) ◽  
pp. 256-262 ◽  
Author(s):  
W. Wong-Ng ◽  
J. A. Kaduk ◽  
H. Wu ◽  
M. Suchomel
Keyword(s):  
Powder Diffraction ◽  
Metal Organic Framework ◽  
National Laboratory ◽  
Argonne National Laboratory ◽  
Lattice Parameter ◽  
X Ray ◽  
Metal Organic ◽  
Sorbent Materials ◽  
Diffraction Patterns ◽  
Unsaturated Metal Sites

M2(dhtp)·nH2O (M = Mn, Co, Ni, Zn; dhtp = 2,5-dihydroxyterephthalate), known as MOF74, is a family of excellent sorbent materials for CO2 that contains coordinatively unsaturated metal sites and a honeycomb-like structure featuring a broad one-dimensional channel. This paper describes the structural feature and provides reference X-ray powder diffraction patterns of these four isostructural compounds. The structures were determined using synchrotron diffraction data obtained at beam line 11-BM at the Advanced Photon Source (APS) in the Argonne National Laboratory. The samples were confirmed to be hexagonal R 3 (No. 148). From M = Mn, Co, Ni, to Zn, the lattice parameter a of MOF74 ranges from 26.131 73(4) Å to 26.5738(2) Å, c from 6.651 97(5) to 6.808 83(8) Å, and V ranges from 3948.08 Å3 to 4163.99 Å3, respectively. The four reference X-ray powder diffraction patterns have been submitted for inclusion in the Powder Diffraction File (PDF).

scholarly journals NDE Development for Ceramics for Advanced Heat Engines

1991 ◽  
Author(s):  
R. W. McClung ◽  
D. R. Johnson
Keyword(s):  
Computed Tomography ◽  
Process Development ◽  
Low Voltage ◽  
National Laboratory ◽  
Argonne National Laboratory ◽  
Ceramic Technology ◽  
X Ray ◽  
Oak Ridge ◽  
Heat Engines ◽  
X Ray Computed

Following an assessment of needs for NDT and characterization of ceramics for the DOE program, Ceramic Technology for Advanced Heat Engines (CTAHE), many NDT projects have been implemented under the sponsorship of CTAHE to address the needs. Tasks at Argonne National Laboratory have involved X-ray computed tomography and nuclear magnetic resonance imaging. The Oak Ridge National Laboratory has emphasized high-frequency ultrasonics, low-voltage radiography, and an advanced system for X-ray computed tomography. A brief investigation was made by Radiation Sciences, Inc., into the feasibility of synchrotron-computed tomography for ceramics. New programs recently initiated at Allison and Garrett integrate ultrasonics, radiography, and other methods into a major effort on life prediction. New programs at Norton and GTE on advanced processing of ceramics also place heavy emphasis on several methods of NDT for process development and control. Initial work on NDT standards has begun in ASTM Committees E-7 and C-28.

scholarly journals A study on the relationship between internal nozzle geometry and injected mass distribution of eight ECN Spray G nozzles.

2017 ◽  
Author(s):  
Katarzyna E Matusik ◽  
Daniel J Duke ◽  
Nicholas Sovis ◽  
Andrew B Swantek ◽  
Christopher F Powell ◽  
...  
Keyword(s):  
Mass Distribution ◽  
National Laboratory ◽  
Argonne National Laboratory ◽  
Gasoline Direct Injection ◽  
Nozzle Geometry ◽  
Hole Density ◽  
Full Spectrum ◽  
Length Scales ◽  
X Ray ◽  
The Relationship

Gasoline direct injection (GDI) nozzles are manufactured to meet geometric specifications with length scales onthe order of a few hundred microns. The machining tolerances of these nominal dimensions are not always knowndue to the difficulty in accurately measuring such small length scales in a nonintrusive fashion. To gain insight intothe variability of the machined dimensions as well as any effects that this variability may have on the fuel spraybehavior, a series of measurements of the internal geometry and fuel mass distribution were performed on a set ofeight nominally duplicate GDI “Spray G” nozzles provided by the Engine Combustion Network. The key dimensionsof each of the eight nozzle holes were measured with micron resolution using full spectrum x-ray tomographicimaging at the 7-BM beamline of the Advanced Photon Source at Argonne National Laboratory. Fuel densitydistributions at 2 mm downstream of the nozzle tips were obtained by performing x-ray radiography measurementsfor many lines of sight. The density measurements reveal nozzle-to-nozzle as well as hole-to-hole density variations.The combination of high-resolution geometry and fuel distribution datasets allows spray phenomena to be linked tospecific geometric characteristics of the nozzle, such as variability in the hole lengths and counterbore diameters,and the hole inlet corner radii. This analysis provides important insight into which geometrical characteristics ofthe nozzles may have the greatest importance in the development of the injected sprays, and to what degreethese geometric variations might account for the total spray variability. The goal of this work is then to further theunderstanding of the relationship between internal nozzle geometry and fuel injection, provide input to improvecomputational models, and ultimately aid in optimizing injector design for higher fuel efficiency and lower emissionsengines.DOI: http://dx.doi.org/10.4995/ILASS2017.2017.4766

On the structure of aragonite

2005 ◽  
Vol 61 (2) ◽  
pp. 129-132 ◽  
Author(s):  
E. N. Caspi ◽  
B. Pokroy ◽  
P. L. Lee ◽  
J. P. Quintana ◽  
E. Zolotoyabko
Keyword(s):  
High Resolution ◽  
National Laboratory ◽  
Argonne National Laboratory ◽  
Orthorhombic Symmetry ◽  
X Ray ◽  
Impurity Atoms ◽  
Synchrotron Powder Diffraction ◽  
Refinement Procedure ◽  
Photon Source

High-resolution synchrotron powder diffraction measurements were carried out at the 32-ID beamline of the Advanced Photon Source of Argonne National Laboratory in order to clarify the structure of geological aragonite, a widely abundant polymorph of CaCO3. The investigated crystals were practically free of impurity atoms, as measured by wavelength-dispersive X-ray spectroscopy in scanning electron microscopy. A superior quality of diffraction data was achieved by using the 11-channel 111 Si multi-analyzer of the diffracted beam. Applying the Rietveld refinement procedure to the high-resolution diffraction spectra, we were able to extract the aragonite lattice parameters with an accuracy of about 20 p.p.m. The data obtained unambiguously confirm that pure aragonite crystals have orthorhombic symmetry.

First X-Ray Microprobe and Microspectroscopy Results From The Gsecars Sector At The Advanced Photon Source

1997 ◽  
Vol 3 (S2) ◽  
pp. 905-906
Author(s):  
Mark L. Rivers ◽  
Stephen R. Sutton ◽  
Peter Eng ◽  
Matthew Newville
Keyword(s):  
National Laboratory ◽  
Argonne National Laboratory ◽  
Third Generation ◽  
X Rays ◽  
Environmental Sciences ◽  
X Ray ◽  
State Determination ◽  
X Ray Absorption ◽  
The Magnetic Field ◽  
Photon Source

The Advanced Photon Source (APS) at Argonne National Laboratory is a third-generation synchrotron x-ray source, optimized for producing x-rays from undulators. Such undulator sources provide extremely bright, quasi-monochromatic radiation which is ideal for an x-ray microprobe. Such microprobes can be used for trace element quantification with x-ray fluorescence, or for chemical state determination with x-ray absorption spectroscopy. The GeoSoilEnviroCARS (GSECARS) sector at the APS is building an x-ray microprobe for research in earth, planetary, soil and environmental sciences.The GSECARS undulator source is a standard APS Undulator “A” which is a 3.3 cm period device with 72 periods. The energies of the undulator peaks can be varied by adjusting the gap, and hence the magnetic field of the undulator. The energy of the first harmonic can be varied in this way from approximately 3.1 keV to 14 keV. A measured undulator spectrum is shown in Figure 1.

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