A Model for Bainite Formation at Isothermal Heat Treatment Conditions

Author(s):  
Gaganpreet Sidhu ◽  
Seshasai Srinivasan ◽  
Sanjiwan Bhole

Abstract An improved model is presented for the formation of bainitic structures during isothermal heat treatment conditions. The model based on displacive mechanism consists of a new expression for the volume fraction of bainite as a function of time, incorporating a temperature and chemical composition-based expression for the number density of initial nucleation sites and limiting the volume fraction of bainite. The model has been validated with respect to experimental data of high- as well as low-carbon steels. It has been found that the isothermal transformation kinetics is well predicted for all steels.

2021 ◽  
Author(s):  
Gaganpreet Sidhu

Analytical models have been developed for the transformation kinetics, microstructure analysis and the mechanical properties in bainitic steels. Three models are proposed for the bainitic transformation based on the chemical composition and the heat treatment conditions of the steel as inputs: (1) thermodynamic model on kinetics of bainite transformation, (2) improved thermo-statistical model that eliminates the material dependent empirical constants and (3) an artificial neural network model to predict the volume fraction of bainite. Neural networks have also been used to model the hardness of high carbon steels, subjected to isothermal heat treatment. Collectively, for a steel of given composition and subjected to a particular isothermal heat treatment, the models can be used to determine the volume fraction of bainitic phase and the material hardness values. The models have been extensively validated with the experimental data from literature as well as from three new high carbon experimental steels with various alloying elements that were used in the present work. For these experimental steels, data on the volume fraction of phases (via X-ray diffraction), yield strength (via compression tests) and hardness were obtained for various combinations of isothermal heat treatment times and temperatures. The heat treated steels were subjected to compression and hardness tests and the data have been used to develop a new correlation between the yield stress and the hardness. It was observed that while all three experimental steels exhibit a predominantly nanostructured bainite microstructure, the presence of Co and Al in one of the steels accelerated and maximized the nano-bainitic transformation within a reasonably short isothermal transformation time. Excellent yield strength (>1.7 GPa) and good deformability were observed in this steel after isothermal heat treatment at a low temperature of 250C for a relatively short duration of 24 hours.


2021 ◽  
Author(s):  
Gaganpreet Sidhu

Analytical models have been developed for the transformation kinetics, microstructure analysis and the mechanical properties in bainitic steels. Three models are proposed for the bainitic transformation based on the chemical composition and the heat treatment conditions of the steel as inputs: (1) thermodynamic model on kinetics of bainite transformation, (2) improved thermo-statistical model that eliminates the material dependent empirical constants and (3) an artificial neural network model to predict the volume fraction of bainite. Neural networks have also been used to model the hardness of high carbon steels, subjected to isothermal heat treatment. Collectively, for a steel of given composition and subjected to a particular isothermal heat treatment, the models can be used to determine the volume fraction of bainitic phase and the material hardness values. The models have been extensively validated with the experimental data from literature as well as from three new high carbon experimental steels with various alloying elements that were used in the present work. For these experimental steels, data on the volume fraction of phases (via X-ray diffraction), yield strength (via compression tests) and hardness were obtained for various combinations of isothermal heat treatment times and temperatures. The heat treated steels were subjected to compression and hardness tests and the data have been used to develop a new correlation between the yield stress and the hardness. It was observed that while all three experimental steels exhibit a predominantly nanostructured bainite microstructure, the presence of Co and Al in one of the steels accelerated and maximized the nano-bainitic transformation within a reasonably short isothermal transformation time. Excellent yield strength (>1.7 GPa) and good deformability were observed in this steel after isothermal heat treatment at a low temperature of 250C for a relatively short duration of 24 hours.


Metals ◽  
2021 ◽  
Vol 11 (7) ◽  
pp. 1036
Author(s):  
Eduardo Colin García ◽  
Alejandro Cruz Ramírez ◽  
Guillermo Reyes Castellanos ◽  
José Federico Chávez Alcalá ◽  
Jaime Téllez Ramírez ◽  
...  

Ductile iron camshafts low alloyed with 0.2 and 0.3 wt % vanadium were produced by one of the largest manufacturers of the ductile iron camshafts in México “ARBOMEX S.A de C.V” by a phenolic urethane no-bake sand mold casting method. During functioning, camshafts are subject to bending and torsional stresses, and the lobe surfaces are highly loaded. Thus, high toughness and wear resistance are essential for this component. In this work, two austempering ductile iron heat treatments were evaluated to increase the mechanical properties of tensile strength, hardness, and toughness of the ductile iron camshaft low alloyed with vanadium. The austempering process was held at 265 and 305 °C and austempering times of 30, 60, 90, and 120 min. The volume fraction of high-carbon austenite was determined for the heat treatment conditions by XRD measurements. The ausferritic matrix was determined in 90 min for both austempering temperatures, having a good agreement with the microstructural and hardness evolution as the austempering time increased. The mechanical properties of tensile strength, hardness, and toughness were evaluated from samples obtained from the camshaft and the standard Keel block. The highest mechanical properties were obtained for the austempering heat treatment of 265 °C for 90 min for the ADI containing 0.3 wt % V. The tensile and yield strength were 1200 and 1051 MPa, respectively, while the hardness and the energy impact values were of 47 HRC and 26 J; these values are in the range expected for an ADI grade 3.


2021 ◽  
Vol 1016 ◽  
pp. 732-737
Author(s):  
Junya Kobayashi ◽  
Hiroto Sawayama ◽  
Naoya Kakefuda ◽  
Goroh Itoh ◽  
Shigeru Kuraoto ◽  
...  

Various high strength steel sheets for weight reduction and safety improvement of vehicles have been developed. TRIP-aided steel with transformation induced plasticity of the retained austenite has high strength and ductility. Conventional TRIP-aided steels are subjected to austempering process after austenitizing. Generally, elongation and formability of TRIP-aided steel are improved by finely dispersed retained austenite in BCC phase matrix. The finely dispersed retained austenite and grain refinement of TRIP-aided steel can be achieved by hot rolling with heat treatment. Therefore, the improvement of mechanical properties of TRIP-aided steel is expected from the manufacturing process with hot rolling and then isothermal transformation process. In this study, thermomechanical heat treatment is performed by combining hot rolling and isothermal holding as the manufacturing process of TRIP-aided steel sheets. The complex phase matrix is obtained by hot rolling and then isothermal holding. Although the hardness of the hot rolled and isothermal held TRIP-aided steel is decreased, the volume fraction of retained austenite is increased.


2018 ◽  
Vol 941 ◽  
pp. 329-333 ◽  
Author(s):  
Jiang Ying Meng ◽  
Lei Jie Zhao ◽  
Fan Huang ◽  
Fu Cheng Zhang ◽  
Li He Qian

In the present study, the effects of ausforming on the bainitic transformation, microstructure and mechanical properties of a low-carbon rich-silicon carbide-free bainitic steel have been investigated. Results show that prior ausforming shortens both the incubation period and finishing time of bainitic transformation during isothermal treatment at a temperature slightly above the Mspoint. The thicknesses of bainitic ferrite laths are reduced appreciably by ausforming; however, ausforming increases the amount of large blocks of retained austenite/martenisite and decreases the volume fraction of retained austenite. And accordingly, ausforming gives rise to significant increases in both yield and tensile strengths, but causes noticeable decreases in ductility and impact toughness.


1978 ◽  
Vol 20 (10) ◽  
pp. 811-815
Author(s):  
M. N. Georgiev ◽  
V. N. Danilov ◽  
N. Ya. Mezhova ◽  
I. V. Nikitin ◽  
P. S. Sokolov

2014 ◽  
Vol 789 ◽  
pp. 314-319
Author(s):  
Yu Lai Chen ◽  
Hong He ◽  
Fei Fang

The microstructure evolution of as-cast 0Cr32Ni7Mo4N hyper duplex stainless steel during the isothermal heat treatment in the temperature range of 800°C-1300°Cwas studied in the present investigation. The morphologies and precipitates were observed and determined by using optical microscope (OM), scanning electron microscope (SEM) and energy dispersive spectroscopy (EDS). The results show that eutectoid decomposition reaction (δ→σ+γ2) take place in ferrite (δ) phase during isothermal heat treatment in the temperature range of 800°C-1000°C. Sigma (σ) phase and secondary austenite (γ2) phase coexist as cellular structure. Lamellar Cr2N precipitates in δ phase mostly when isothermal heat treatment at 800°Cand 850°C, while it only appears in γ phase between 900°C and 1050°C. As the annealing temperature rising, the quantity of σ phase, Cr2N and γ2 phase decreases. The volume fraction ratio of ferrite and austenite is stable between 1100°C and 1300°C, and γ → δ transformation is hard to occur.


2010 ◽  
Vol 152-153 ◽  
pp. 628-633
Author(s):  
Fa Yun Zhang ◽  
Jian Xiong Ye ◽  
Hong Yan

Effects of SiC particle and holding time on microstructure evolution of SiCP/AZ61 composites during semi-solid isothermal heat treatment method were studied, and evolution mechanism of semi-solid microstructure of composites was discussed. The results indicated that the process of microstructure evolution of SiCP/AZ61 composites by the isothermal holding at the temperatures of 595°C for different times (0min~90min) experienced in succession the rapid merging of the secondary dendritic arms →large massive structure→melting and separating of the local grain boundary →spheroidization of the gains →slowing growth of globular microstructure. Synthetically, after isothermal holding at 595°C for 30min to 60min the favorable semi-solid microstructure can be obtained; Compared with the monolithic AZ61alloy, microstructure of SiCP/AZ61 composites during semi-solid isothermal heat-treatment was finer as a result of entering of Sic particle, and with the increasing of SiC particle volume fraction, globular gain size was smaller.


2007 ◽  
Vol 534-536 ◽  
pp. 673-676 ◽  
Author(s):  
Ahmet Güral ◽  
Süleyman Tekeli ◽  
Dursun Özyürek ◽  
Metin Gürü

The effect of repeated quenching heat treatment on microstructure and dry sliding wear behavior of low carbon PM steel was investigated. For this purpose, atomized iron powder was mixed with 0.3 % graphite and 1 % Ni powders. The mixed powders were cold pressed and sintered at 1200°C for 30 min under pure Ar gas atmosphere. Some of the sintered specimens were intercritically annealed at 760°C and quenched in water (single quenching). The other sintered specimens were first fully austenized at 890°C and water quenched. These specimens were then intercritically annealed at 760°C and re-quenched in water. The martensite volume fraction in the double quenched specimens was higher than that of the single quenched specimen. Wear tests were carried out on the single and double quenched specimens under dry sliding wear condition using a pin-on-disk type machine at constant load and speed. The experimental results showed that the wear coefficient effectively decreased in the double quenched specimen.


2018 ◽  
Vol 1 (1) ◽  
pp. 26-30
Author(s):  
Enikő Réka Fábián ◽  
Áron Kótai

Abstract During our investigation lath martensite was produced in low carbon steels by austenitization at 1200 °C/20 min, and the cooling of samples in ice water. The samples were tempered at a range of temperatures. The tempering effects on microstructure and on mechanical proprieties were investigated. Some samples with lath martensite microstructure were cold rolled and heat treated at different temperatures. Recrystallization was observed after heat treatment at 600-700 °C.


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