Microstructure Modeling of Dynamically Recrystallized Grain Size of Sintered Al–4 wt % B4C Composite During Hot Upsetting

Author(s):  
R. Seetharam ◽  
S. Kanmani Subbu ◽  
M. J. Davidson

Grain size control of any engineering metal is very important in the hot upsetting process. Generally, the grain size directly controls the mechanical properties and performance of the material. Al–B4C composite finds extensive applications in nuclear industries, defense, and electronic industries. Therefore, the aim of this work is to study the dynamic recrystallization (DRX) behavior of Al–4 wt % B4C composite during the hot upsetting test. Experimental work was performed on sintered Al–4 wt % B4C preforms at various initial relative density (IRD) values of 80%, 85%, and 90%, and over the temperature range of 300–500 °C and strain rates range of 0.1–0.3 s−1. The DRXed grain size of Al–4 wt % B4C preforms for IRDes, and temperatures and strain rates were evaluated by using an optical microscope. The activation energy (Q) and Zener–Hollomon parameter of sintered Al–4 wt % B4C preforms were calculated for various deformation conditions and IRDes. The mathematical models of DRX were developed as a function of Zener–Hollomon parameter for various IRDes to predict the DRXed grain size. It was found that the DRXed grain size decreases with increasing Zener–Hollomon parameter. Verification tests were done between the measured and predicted DRXed grain size for various IRDes, and absolute and mean absolute error was found to be 9.92% and 8.58%, respectively.

Author(s):  
Ernest L. Hall ◽  
Lee E. Rumaner ◽  
Mark G. Benz

The intermetallic compound Nb3Sn is a type-II superconductor of interest because it has high values of critical current density Jc in high magnetic fields. One method of forming this compound involves diffusion of Sn into Nb foil containing small amounts of Zr and O. In order to maintain high values of Jc, it is important to keep the grain size in the Nb3Sn as small as possible, since the grain boundaries act as flux-pinning sites. It has been known for many years that Zr and O were essential to grain size control in this process. In previous work, we have shown that (a) the Sn is transported to the Nb3Sn/Nb interface by liquid diffusion along grain boundaries; (b) the Zr and O form small ZrO2 particles in the Nb3Sn grains; and (c) many very small Nb3Sn grains nucleate from a single Nb grain at the reaction interface. In this paper we report the results of detailed studies of the Nb3Sn/Nb3Sn, Nb3Sn/Nb, and Nb3Sn/ZrO2 interfaces.


2021 ◽  
pp. 138770
Author(s):  
Linlin Guan ◽  
Leiming Yu ◽  
Lijuan Wu ◽  
Shuyu Zhang ◽  
Yuting Lin ◽  
...  

1995 ◽  
Vol 102 (12) ◽  
pp. 5082-5087 ◽  
Author(s):  
Thomas Palberg ◽  
Wolfgang Mönch ◽  
Jürgen Schwarz ◽  
Paul Leiderer

2017 ◽  
Vol 544 ◽  
pp. 306-311 ◽  
Author(s):  
Shunsuke Tanaka ◽  
Kenta Okubo ◽  
Koji Kida ◽  
Miki Sugita ◽  
Takahiko Takewaki

2003 ◽  
Vol 89 (5) ◽  
pp. 616-622 ◽  
Author(s):  
Koji TAKANO ◽  
Ryuji NAKAO ◽  
Shigeo FUKUMOTO ◽  
Toshihiro TSUCHIYAMA ◽  
Setsuo TAKAKI

2019 ◽  
Vol 7 (21) ◽  
pp. 12987-12992 ◽  
Author(s):  
Seungju Seo ◽  
Il Jeon ◽  
Rong Xiang ◽  
Changsoo Lee ◽  
Hao Zhang ◽  
...  

Grain size control and boundary passivation of perovskite films are the key to obtaining efficient perovskite solar cells.


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