Selective Laser Melting of Graphene-Reinforced Inconel 718 Superalloy: Evaluation of Microstructure and Tensile Performance

Author(s):  
Yachao Wang ◽  
Jing Shi ◽  
Shiqiang Lu ◽  
Yun Wang

Graphene nanoplatelets (GNPs) have many outstanding properties, such as high mechanical strengths, light weight, and high electric conductivity. These unique properties make it an ideal reinforcement used for metal matrix composites (MMCs). In the past few years, many studies have been performed to incorporate GNPs into metal matrix and investigate the properties of obtained metal matrix composites. Meanwhile, fabrication of MMCs through laser-assisted additive manufacturing (LAAM) has attracted much attention in recent years due to the advantages of low waste, high precision, short production lead time, and high workpiece complexity capability. In this study, the two attractive features are combined to produce GNPs reinforced MMC using selective laser melting (SLM) process, one of the LAAM processes. The target metal matrix material is Inconel 718, a nickel-based Ni–Cr–Fe austenitic superalloy that possesses excellent workability and mechanical performance, and has wide applications in industries. In the experiment, pure Inconel 718 and GNPs reinforced Inconel 718 composites with two levels of GNPs content (i.e., 0.25 and 1 wt. %) are obtained by SLM. Note that before the SLM process, a novel powder mixture procedure is employed to ensure the even dispersion of GNPs in the Inconel 718 powders. Room temperature tensile tests are conducted to evaluate the tensile properties. Scanning electron microscopy (SEM) observations are conducted to analyze the fracture surface of materials and to understand the reinforcing mechanism. It is found that fabrication of GNPs reinforced MMC using SLM is a viable approach. The obtained composite possesses dense microstructure and significantly enhanced tensile strength. The ultimate tensile strengths (UTSs) are 997.8, 1296.3, and 1511.6 MPa, and the Young's moduli are 475, 536, and 675 GPa, for 0 wt. % (pure Inconel 718), 0.25 wt. %, and 1 wt. % GNP additions, respectively. The bonding between GNPs and matrix material appears to be strong, and GNPs could be retained during the SLM process. The strengthening effect and mechanisms involved in the composites are discussed. Load transfer, thermal expansion coefficient mismatch, and dislocation hindering are believed to be the three main reinforcing mechanisms involved. It should be noted that more work needs to be conducted in the future to obtain more comprehensive information regarding other static and dynamic properties and the high-temperature performances of the GNP-reinforced MMCs produced by SLM. Process parameter optimization should also be investigated.

Author(s):  
Yachao Wang ◽  
Jing Shi ◽  
Shiqiang Lu ◽  
Yun Wang

Graphene nanoplatelets (GNPs) have many outstanding properties, such as high mechanical strengths, light weight, and high electric conductivity. These unique properties make it an ideal reinforcement used for metal matrix composite (MMCs). In the past few years, many studies have been performed to incorporate GNPs into metal matrix and investigate the properties of obtained metal matrix composites. Meanwhile, fabrication of MMCs through laser assisted additive manufacturing (LAAM) has attracted much attention in recent years due to the advantages of low waste, high precision, short production lead time, and high workpiece complexity capability. In this study, the two attractive features are combined to produce GNPs reinforced MMC using selective laser melting (SLM) process, one of the LAAM processes. The target metal matrix material is Inconel 718, a nickel-based Ni-Cr-Fe austenitic superalloy that possesses excellent workability and mechanical performance and has wide applications in industries. Inconel 718 holds outstanding mechanical performance, corrosion, oxidation, and wear performance over a wide range of temperatures, making it an attractive superalloy used for high temperature service components. In the experiment, pure Inconel 718 and GNPs reinforced Inconel 718 composites with two levels of GNPs content (i.e., 0.25 and 1 wt.%) are obtained by SLM. Note that the SLM process, a novel powder mixture procedure is adopted to ensure the even dispersion of GNPs in the Inconel 718 powders. Room temperature tensile tests are conducted to evaluate the tensile properties. Scanning electron microscopy (SEM) observations are conducted to analyze the fracture surface of materials and to understand the reinforcing mechanism. It is found that fabrication of GNPs reinforced MMC using SLM is a viable approach. The obtained composite possesses dense microstructure and significantly enhanced tensile strength. The ultimate tensile strengths (UTS) are 997.8, 1296.3 and 1511.6 MPa, and the Young’s moduli are 475, 536, and 675 GPa, for 0 wt.% (pure Inconel 718), 0.25 wt.%, and 1 wt.% GNP additions, respectively. The bonding between GNPs and matrix material appears to be strong, and GNPs are well retained during the SLM process. The strengthening effect and mechanisms involved in the composites are discussed. Load transfer, thermal expansion coefficient mismatch, and dislocation hindering are believed to be the three main reinforcing mechanisms involved. It should be noted that more work needs to be conducted in the future to obtain more comprehensive information regarding other static and dynamic properties, and the high temperature performances of the GNP reinforced MMCs produced by SLM. Process parameter optimization should also be investigated.


Author(s):  
Jing Shi ◽  
Yachao Wang ◽  
Shiqiang Lu ◽  
Yun Wang

Selective laser melting (SLM) is an important additive manufacturing process. It applies focused laser energy to quickly melt and solidify material powders, and a controlled layered operation can result in a free form build that is often out of reach for machining processes. As such, it has attracted much attention in recent years. However, metal components produced by this process often have inferior mechanical properties, as compared with the counterparts by the traditional manufacturing processes. To strengthen the metal components by SLM, adding reinforcement particles and applying post treatment are regarded as the two effective ways. Although adding reinforcement particles to create metal matrix composites has been studied by researchers in literature, much fewer has been done to use post treatment processes to further improve the properties and performance of the metal matrix composites from SLM. In this study, a nano-TiC reinforced Inconel 718 composite is prepared using SLM technique. The material has 0.5 wt.% nano-TiC addition. Solid solution treatments at three levels of temperature (940, 980, 1020 °C) are carried out to evaluate the effect of the heat treatment methods on the microstructure and resulted mechanical properties of the composite material. The results of samples with and without heat treatment are also compared. SEM observations are carried out to analyze the microstructure of the composite and understand the reinforcing mechanism. Tensile tests are conducted to evaluate the mechanical properties of the formed composites. It is discovered that compared with the pure Inconel 718 by SLM, the Inconel 718-TiC composite exhibits improved ultimate tensile strength. Microscopy observation of as-built samples indicates that the dendritic structures of Inconel 718 is remarkably refined by the TiC particles. Suspected laves phase particles are observed in as-built Inconel-TiC composite, and they partially transform to large amount of needle-like δ phase during the solid solution treatment.


Author(s):  
D.I. Sukhov ◽  
◽  
S.V. Nerush ◽  
I.Yu. Efimochkin ◽  
F.N. Karachevchev ◽  
...  

The paper considers manufacturing of metal matrix composites (MMC) by means of selective laser melting. The heat-resistant nickel-based Ni–Cr–Mo–Nb–Al alloy was chosen as a matrix material, the Y2O3 oxide was chosen as a strengthener. After mechanical alloying the obtained powder was used in SLM for the production of a material. The synthesized material’s condition was examined after the SLM process and after hot isostatic pressing (HIP). In the structure the areas containing Y, Al and O-based compounds were found. The creep-rupture tests of samples after HIP and heat treatment were performed and the results were explained by fractographic analysis.


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