Correlation Between Microstructure and Mechanical Properties in an Inconel 718 Deposit Produced Via Electron Beam Freeform Fabrication

Author(s):  
Wesley A. Tayon ◽  
Ravi N. Shenoy ◽  
MacKenzie R. Redding ◽  
R. Keith Bird ◽  
Robert A. Hafley

Electron beam freeform fabrication (EBF3), a metallic layer-additive manufacturing process, uses a high-power electron beam in conjunction with a metal feed wire to create a molten pool on a substrate, which on solidification produces a component of the desired configuration made of sequentially deposited layers. During the build-up of each solidified layer, the substrate is translated with respect to the electron beam and the feed wire. EBF3 products are similar to conventional cast products with regard to the as-deposited (AD) microstructure and typical mechanical properties. Inconel 718 (IN 718), a high-temperature superalloy with attractive mechanical and oxidation properties well suited for aerospace applications, is typically used in the wrought form. The present study examines the evolution of microstructure, crystallographic texture, and mechanical properties of a block of IN 718 fabricated via the EBF3 process. Specimens extracted out of this block, both in the AD and in a subsequently heat treated (HT) condition, were subjected to (1) microstructural characterization using scanning electron microscopy (SEM); (2) in-plane elastic modulus, tensile strength, and microhardness evaluations; and (3) crystallographic texture characterization using electron backscatter diffraction (EBSD). Salient conclusions stemming from this study are: (1) mechanical properties of the EBF3-processed IN 718 block are strongly affected by texture as evidenced by their dependence on orientation relative to the EBF3 fabrication direction, with the AD EBF3 properties generally being significantly reduced compared to wrought IN 718; (2) significant improvement in both strength and modulus of the EBF3 product to levels nearly equal to those for wrought IN 718 may be achieved through heat treatment.

Materials ◽  
2021 ◽  
Vol 14 (19) ◽  
pp. 5856
Author(s):  
Pragya Mishra ◽  
Pia Åkerfeldt ◽  
Farnoosh Forouzan ◽  
Fredrik Svahn ◽  
Yuan Zhong ◽  
...  

Laser powder bed fusion (L-PBF) has attracted great interest in the aerospace and medical sectors because it can produce complex and lightweight parts with high accuracy. Austenitic stainless steel alloy 316 L is widely used in many applications due to its good mechanical properties and high corrosion resistance over a wide temperature range. In this study, L-PBF-processed 316 L was investigated for its suitability in aerospace applications at cryogenic service temperatures and the behavior at cryogenic temperature was compared with room temperature to understand the properties and microstructural changes within this temperature range. Tensile tests were performed at room temperature and at −196 °C to study the mechanical performance and phase changes. The microstructure and fracture surfaces were characterized using scanning electron microscopy, and the phases were analyzed by X-ray diffraction. The results showed a significant increase in the strength of 316 L at −196 °C, while its ductility remained at an acceptable level. The results indicated the formation of ε and α martensite during cryogenic testing, which explained the increase in strength. Nanoindentation revealed different hardness values, indicating the different mechanical properties of austenite (γ), strained austenite, body-centered cubic martensite (α), and hexagonal close-packed martensite (ε) formed during the tensile tests due to mechanical deformation.


2011 ◽  
Vol 409 ◽  
pp. 29-34 ◽  
Author(s):  
Alexandre Bois-Brochu ◽  
Franck Armel Tchitembo Goma ◽  
Carl Blais ◽  
Daniel Larouche ◽  
Raynald Gauvin ◽  
...  

Utilization of aluminium-lithium alloys in aerospace applications requires an understanding of how processing and product geometry impact their microstructure, crystallographic texture and mechanical properties. In this paper, the effect of various microstructural features as well as deformation textures on the static mechanical properties of Al-Li extruded components has been investigated. These relationships are discussed with regard to two 2099-T83 extruded sections, i.e. a cylindrical extrusion and an integrally stiffened panel (ISP). The ISP typically shows an unrecrystallized microstructure with varying texture depending on the location along its cross section while the cylindrical extrusions present a strong fibre texture. The anisotropy is noticeable in tensile and compressive tests for both types of extrusions.


Materials ◽  
2019 ◽  
Vol 12 (8) ◽  
pp. 1293 ◽  
Author(s):  
Michele Calandri ◽  
Shuo Yin ◽  
Barry Aldwell ◽  
Flaviana Calignano ◽  
Rocco Lupoi ◽  
...  

Nickel-based Inconel 718 is a very good candidate for selective laser melting (SLM). During the SLM process, Inconel 718 develops a complex and heterogeneous microstructure. A deep understanding of the microstructural features of the as-built SLM material is essential for the design of a proper post-process heat treatment. In this study, the microstructure of as-built SLM Inconel 718 was investigated at different length scales using optical microscopy (OM), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). Electron backscatter diffraction (EBSD) was also used to analyze the grain morphology and crystallographic texture. Grains elongated in the build direction and crossing several deposited layers were observed. The grains are not constrained by the laser tracks or by the melt pools, which indicates epitaxial growth controls the solidification. Each grain is composed of fine columnar dendrites that develop along one of their <100> axes oriented in the direction of the local thermal gradient. Consequently, prominent <100> crystallographic texture was observed and the dendrites tend to grow to the build direction or with occasional change of 90° at the edge of the melt pools. At the dendrite length scale, the microsegregation of the alloying elements, interdendritic precipitates, and dislocations was also detected.


Materials ◽  
2019 ◽  
Vol 12 (19) ◽  
pp. 3061 ◽  
Author(s):  
Jiajia Qiu ◽  
Min Zhang ◽  
Zhunli Tan ◽  
Guhui Gao ◽  
Bingzhe Bai

A bainite/martensite multiphase rail is treated by the controlled-cooling process with different finish-cooling temperatures. The simulated temperature–time curves of the position of 5 mm and 15 mm below the rail tread (P5 and P15) express different trends. P5 has greater impact toughness and lower tensile strength than P15. Microstructural characterization was carried out by conducting scanning electron microscopy, X-ray diffraction, electron backscatter diffraction, and transmission electron microscopy. The greater tensile strength is due to the dispersed ε-carbides hindering the movement of dislocations. The greater impact toughness is attributed to the filmy retained austenite and the smaller effective grain with high-angle boundary. Finite element modeling (FEM) and microstructural characterization reasonably explain the changes of mechanical properties. The present work provides experimental and theoretical guidance for the development of rail with excellent mechanical properties.


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