Ordered Au Nanodisk and Nanohole Arrays: Fabrication and Applications

Author(s):  
Yue Bing Zheng ◽  
Bala Krishna Juluri ◽  
Brian Kiraly ◽  
Tony Jun Huang

We have utilized nanosphere lithography (NSL) to fabricate ordered Au nanodisk and nanohole arrays on substrates and have studied the localized surface plasmon resonance (LSPR) of the arrays. Through these investigations, we demonstrate that the angle-dependent behavior of the LSPR in the Au nanodisk arrays enables real-time observation of exciton-plasmon couplings. In addition, we show that the NSL-fabricated Au nanohole arrays can be applied as templates for patterning micro-/nanoparticles under capillary force. The unique structural and plasmonic characteristics of the Au nanodisk and nanohole arrays, as well as the low-cost and high-throughput NSL-based nanofabrication technique, render these arrays excellent platforms for numerous engineering applications.

Author(s):  
Tieyu Gao ◽  
Yue Bing Zheng ◽  
Bala Krishna Juluri ◽  
Tony Jun Huang

We have fabricate ordered Au nanodisk and nanohole arrays on glass substrates using nanosphere lithography (NSL) combined with reactive ion etching (RIE) techniques. The morphology and size distribution of the Au nanodisks and nanoholes were examined with scanning electron microscopy (SEM) and atomic force microscopy (AFM). The sensitivity of the localized surface plasmon resonance (LSPR) of the Au nanodisk arrays to change in the surroundings’ refractive index was evaluated by integrating the Au nanodisk arrays into microfluidic channels. In addition, we show that the NSL-fabricated Au nanohole arrays can be applied as templates for patterning micro-/nano-particles under capillary force. The unique structural and optical characteristics of the Au nanodisk and nanohole arrays, as well as the low-cost and high-throughput of NSL-based nanofabrication technique, render these arrays excellent platforms for numerous engineering applications.


Nanomaterials ◽  
2019 ◽  
Vol 9 (11) ◽  
pp. 1557 ◽  
Author(s):  
Shujahadeen B. Aziz ◽  
Govar Hussein ◽  
M. A. Brza ◽  
Sewara J. Mohammed ◽  
R. T. Abdulwahid ◽  
...  

Interconnected spherical metallic silver nanoparticles (Ag NPs) were synthesized in the current study using a green chemistry method. The reduction of silver ions to Ag NPs was carried out with low-cost and eco-friendly quince leaves. For the first time, it was confirmed that the extract solution of quince leaves could be used to perform green production of Ag NPs. Fourier transform infrared spectroscopy (FTIR) was conducted to identify the potential biomolecules that were involved in the Ag NPs. The results depicted that the biosynthesis of Ag NPs through the extract solution of quince leaf was a low-cost, clean, and safe method, which did not make use of any contaminated element and hence, had no undesirable effects. The majority of the peaks in the FTIR spectrum of quince leaf extracts also emerged in the FTIR spectrum of Ag NPs but they were found to be of less severe intensity. The silver ion reduction was elaborated in detail on the basis of the FTIR outcomes. In addition, through X-ray diffraction (XRD) analysis, the Ag NPs were also confirmed to be crystalline in type, owing to the appearance of distinct peaks related to the Ag NPs. The creation of Ag NPs was furthermore confirmed by using absorption spectrum, in which a localized surface plasmon resonance (LSPR) peak at 480 nm was observed. The LSPR peak achieved in the present work was found to be of great interest compared to those reported in literature. Field emission scanning electron microscopy (FESEM) images were used to provide the morphology and grain size of Ag NPs. It was shown from the FESEM images that the Ag NPs had interconnected spherical morphology.


Nanomaterials ◽  
2019 ◽  
Vol 9 (7) ◽  
pp. 1019 ◽  
Author(s):  
Yun Liu ◽  
Ning Zhang ◽  
Ping Li ◽  
Li Yu ◽  
Shimeng Chen ◽  
...  

There are many potential applications for biosensors that can provide real-time analysis, such as environmental monitoring and disease prevention. In this study, we investigated a simple strategy for real-time protein detection, which had the advantages of affordability, fast response, portability, and ease of use. A robust quantification of protein interaction was achieved by combining capillary localized surface plasmon resonance (LSPR) sensors and complementary metal–oxide–semiconductor (CMOS) image sensors. Gold nanoparticles were modified on the inner wall of the capillary, which was used as a microfluidic channel and sensing surface. We functionalized one of the LSPR sensors using ligand bound to gold nanoparticle. Our proposed biosensing platform could be easily multiplexed to achieve high throughput screening of biomolecular interactions, and it has the potential for use in disposable sensors. Moreover, the sensing signal was enhanced by the extinction effect of gold nanoparticles. The experimental results showed that our device could achieve qualitative identification and quantitative measurement of transferrin and immunoglobulin G (IgG). As a field-portable and low-cost optical platform, the proposed LSPR biosensing device is broadly applicable to various protein binding tests via a similar self-assembly of organic ultrathin films.


The Analyst ◽  
2021 ◽  
Author(s):  
Jittrapun Soongsong ◽  
Jamras Lerdsri ◽  
Jaroon Jakmunee

A colorimetric aptasensor for chlorpyrifos detection utilizing localized surface plasmon resonance (LSPR) of gold nanoparticles (AuNPs) aggregation coupling with a specific aptamer and cationic polyethyleneimine (PEI) has been developed. The...


2021 ◽  
pp. 2100653
Author(s):  
Gyeong‐Su Park ◽  
Kyung Suk Min ◽  
Hyuksang Kwon ◽  
Sangwoon Yoon ◽  
Sangwon Park ◽  
...  

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