Calibration Techniques in Ultrahigh-Pressure Apparatus

1961 ◽  
Vol 83 (2) ◽  
pp. 207-213 ◽  
Author(s):  
F. P. Bundy

Pressure and temperature calibration of ultrahigh-pressure apparatus is described. Pressure calibration up to 30 kilobars has been established accurately. Above this pressures are not known with sufficient absolute accuracy to compare results reliably with theoretical predictions of behavior of matter. The effect of pressure on temperature-sensing devices, like thermocouples, have been measured over temperature intervals of 100 deg C up to pressures of the order of 100 kilobars. The effect on some thermocouples is appreciable.

Sensors ◽  
2018 ◽  
Vol 18 (12) ◽  
pp. 4239 ◽  
Author(s):  
Dasom Lee ◽  
Kwon Park ◽  
Changhyun Lee ◽  
Sang-Jin Choi

The Distributed Temperature Sensing (DTS) profiles obtained during well completion of a CO2 monitoring well were analyzed to characterize each well completion process in terms of temperature anomalies. Before analysis, we corrected the depth by redistributing the discrepancy, and then explored three temperature calibration methods. Consequently, we confirmed the depth discrepancy could be well corrected with conventional error redistribution techniques. Among three temperature calibration methods, the conventional method shows the best results. However, pointwise methods using heat coil or in-well divers also showed reliable accuracy, which allows them to be alternatives when the conventional method is not affordable. The DTS data revealed that each well completion processes can be characterized by their own distinctive temperature anomaly patterns. During gravel packing, the sand progression was monitorable with clear step-like temperature change due to the thermal bridge effect of sand. The DTS data during the cementing operation, also, clearly showed the progression up of the cement slurry and the exothermic reaction associated with curing of cement. During gas lift operations, we could observe the effect of casing transition as well as typical highly oscillating thermal response to gas lifting.


1977 ◽  
Vol 55 (4) ◽  
pp. 370-377 ◽  
Author(s):  
A. A. Haasz

Theoretical predictions were obtained for the effect of reflected nitrogen molecules on rotational temperature measurements with rocketborne electron beam fluorescence probes in the free molecular flow regime. Calculations for a typical payload (Black Brant AEF-II-118 flown from Fort Churchill, Man., Canada) indicate that the effect of reflected molecules can be significant and should be considered in the derivation of the theoretical temperature calibration curves.


RSC Advances ◽  
2020 ◽  
Vol 10 (37) ◽  
pp. 22156-22163
Author(s):  
Hitoshi Nabata ◽  
Makito Takagi ◽  
Kenichiro Saita ◽  
Satoshi Maeda

In this study, we focused on the effect of pressure on the crystal structures of dioxides of group 14 elements, i.e. SiO2, GeO2, and CO2.


Author(s):  
David Dickey

Abstract It is necessary to understand the limitations of an automated InfraRed (IR) system when using it for temperature measurements. These systems correct for emissivity of the test sample by heating the unpowered sample and taking radiance measurements at two temperatures. For the specific sample that was analyzed, the temperature of the area of interest of the powered sample was higher than the two temperatures used for emissivity correction. This resulted in a significant error in the temperature calculated by the system. The use of direct radiance measurements provided an accurate measurement of the sample temperature.


2021 ◽  
Author(s):  
Sariga C. Lal ◽  
I. N. Jawahar ◽  
G. Subodh

Group theoretical predictions obtained from Raman and IR spectra emphasize the structure of B-site ordered double perovskites Ba2R2/3TeO6 (R =Y, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu) with ubiquitous...


1967 ◽  
Vol 1 (2) ◽  
pp. 62-64 ◽  
Author(s):  
R. Wielebinski

The accuracy of the absolute value of solar flux depends on the temperature calibration techniques and the knowledge of the gain of the aerial used for the measurements. Recent advances in low-noise receivers, microwave components, and amplifier stability have reduced considerably the errors due to temperature calibration techniques. At present the knowledge of the gain of the aerial used for calibrations (usually a pyramidal horn) presents the largest source of doubt of an absolute calibration. Investigations of this problem suggest that a ‘standard gain horn’ should be employed at all observatories in absolute solar calibrations.


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