A Pressure-Shear Plate Impact Experiment for Studying the Rheology of Lubricants at High Pressures and High Shearing Rates

1987 ◽  
Vol 109 (2) ◽  
pp. 215-222 ◽  
Author(s):  
K. T. Ramesh ◽  
R. J. Clifton

A new plate impact configuration is described for subjecting lubricants to simple shearing motion under uniform hydrostatic pressure. Thin layers (∼50 μm thick) of the lubricant are confined between two hard metallic plates which are subjected to impact by a parallel plate that is inclined relative to the direction of approach in order to induce both pressure and shear loading. Stress waves in the hard plates are monitored by laser interferometry; all measurements are made before unloading waves arrive from the periphery. For approximately one microsecond the compressed lubricant is subjected to a simple shearing motion and a continuous record of the shear stress and shear rate is obtained. Results presented for the lubricant 5P4E at pressures of 1-5 GPa and shear rates of approximately 9 × 105 s−1 show good agreement with available data on the dependence of the limiting shear stress on the confining pressure at lower pressures and lower shearing rates.

1996 ◽  
Vol 118 (1) ◽  
pp. 162-168 ◽  
Author(s):  
Y. Zhang ◽  
K. T. Ramesh

Knowledge of the behavior of lubricants over a wide range of pressures and shear rates is fundamental to an understanding of elastohydrodynamic (EHD) lubrication. The mechanical properties of elastohydrodynamic lubricants have been measured by a number of researchers under the conditions of low pressures and low shear rates, as well as under high pressures and high shear rates. This paper presents experimental results for the synthetic lubricant 5P4E subjected to moderate pressures (60 MPa to 700 MPa) and high shear rates (105 s−1) using the technique of pressure-shear plate impact. Thin layers (25 μm thick) of the lubricant are confined between two hard elastic plates; the assembly is subjected to impact by a parallel plate in a manner designed to induce both compression and shear loading. For approximately 1 μs the compressed lubricant is subjected to a simple shearing motion; during that time, continuous records of the shear stress and shear rate are obtained using laser interferometry. Three test configurations were used in order to cover the pressure range, and special techniques were developed for preparing the specimen sandwich. The pressure range covered includes both the liquid and glassy states of the lubricant. The results show that a limiting shear stress model is an appropriate model for lubricant behavior under these conditions. The experimental results also show little change in the lubricant shearing behavior across the glass transition.


The Eyring theory of viscous flow suggests that lubricating oils should exhibit shear thinning when the shear stress exceeds about 5 MPa. The results of friction experiments in rolling-contact disc machines where very high pressures are generated in the lubricant film support this prediction, but are open to the criticism that the fluid is subjected to a high pressure for such a short time ( ca . 10 -4 s) that an equilibrium state may not be reached. In the present investigation the appropriate condition of the lubricant is achieved, not by subjecting it to very high pressures but by maintaining it in the supercooled state. The lubricant is thus in a condition of equili­brium and the shear experiments are carried out at atmospheric pressure. The lubricant specimen is retained in a suitably adapted split Hopkinson torsion bar, and at the high rates of shear applied ( ca . 10 4 s -1 ) the shear stress at sufficiently low temperatures can exceed 5 MPa. By this tech­nique the shear pulse is applied for a sufficiently short time ( ca . 10 -3 s) to avoid viscous heating of the sample, which bedevils normal viscometry at high shear rates. Two fluids were tested: polyphenyl ether 5P4E and a mineral oil Shell HVI 650. Nonlinearity in the shear-stress-shear-strain-rate relation was found when the stress exceeded about 3 MPa. The elastic shear modulus G ∞ was also measured, yielding ca . 500 MPa for 5P4E and ca . 50 MPa for HVI 650.These values compare with ca . 1100 MPa and 300 MPa as found by the high-frequency oscillating shear technique at small strains.


Polymers ◽  
2021 ◽  
Vol 13 (15) ◽  
pp. 2542
Author(s):  
Junxiu Lv ◽  
Xiaoyuan Zhang

This study mainly investigates the prediction models of shear parameters and dynamic creep instability for asphalt mixture under different high temperatures to reveal the instability mechanism of the rutting for asphalt pavement. Cohesive force c and internal friction angle φ in the shear strength parameters for asphalt mixture were obtained by the triaxial compressive strength test. Then, through analyzing the influence of different temperatures on parameters c and φ, the prediction models of shear strength parameters related to temperature were developed. Meanwhile, the corresponding forecast model related to confining pressure and shear strength parameters was obtained by simplifying the calculation method of shear stress level on the failure surface under cyclic loading. Thus, the relationship of shear stress level with temperature was established. Furthermore, the cyclic time FN of dynamic creep instability at 60 °C was obtained by the triaxial dynamic creep test, and the effects of confining pressure and shear stress level were considered. Results showed that FN decreases exponentially with the increase in stress levels under the same confining pressure and increases with the increase in confining pressure. The ratio between shear stress level and corresponding shear strength under the same confining pressure was introduced; thus, the relationship curve of FN with shear stress level can eliminate the effect of different confining pressures. The instability prediction model of FN for asphalt mixture was established using exponential model fitting analysis, and the rationality of the model was verified. Finally, the change rule of the parameters in the instability prediction model was investigated by further changing the temperature, and the instability forecast model in the range of high temperature for the same gradation mixture was established by the interpolation calculation.


2021 ◽  
Author(s):  
Ademola Balogun ◽  
Toyin Odutola ◽  
Yakubu Balogun

Abstract This research examines the use of 75nm Zinc Oxide nanoparticles (Nano ZnO) and Polyethylene Butene (PEB) in reducing the viscosity of Nigerian waxy crude oil. The rheology of the crude oil was studied by measuring the viscosity and shear stress of crude samples contaminated with varying concentration of PEB (500ppm, 1000ppm, 2000ppm, 3000ppm, 4000ppm and 5000ppm), varying concentrations of Nano ZnO (1wt%, 2wt%, 3wt% and 4wt%) and different blends of PEB and Nano ZnO at temperatures of between 10°C to 35°C and shear rates from 1.7 to 1020s-1. From Rheological Modelling analysis conducted, the Power law pseudoplastic model was the best fit for the experimental data with a regression coefficient of 0.99. Analysis of crude sample before addition of inhibitor showed evidence of non-Newtonian fluid behaviour as the shear stress-shear rate relationship curves were nonlinear due to wax precipitation at low temperatures (10°C to 15°C). The waxy crude demonstrated shear thinning behaviour with increasing shear rates (increasing turbulence) and the viscosity reduced with increasing temperature. The addition of inhibitors (PEB, Nano ZnO and their blends) effected Newtonian fluid behaviour in the crude samples as the shear stress-shear rate relationship curves were linear at all temperatures under study. The optimum concentration of the inhibitors in this study is 2000ppm PEB (causing 33% viscosity reduction) and 1wt% Nano ZnO (effecting 26% viscosity reduction). The best concentration of the blend was 2000ppm PEB blended with 1wt% Nano ZnO which effected a viscosity reduction of 41%. The research demonstrates the novel application of the blend of Nano ZnO and PEB in improving flowability of Nigerian waxy crude oil especially in offshore conditions with prevailing cold temperatures.


2018 ◽  
Vol 2018 ◽  
pp. 1-12
Author(s):  
Fei Wang ◽  
Ping Cao ◽  
Yu Chen ◽  
Qing-peng Gao ◽  
Zhu Wang

In order to investigate the influence of the joint on the failure mode, peak shear strength, and shear stress-strain curve of rock mass, the compression shear test loading on the parallel jointed specimens was carried out, and the acoustic emission system was used to monitor the loading process. The joint spacing and joint overlap were varied to alter the relative positions of parallel joints in geometry. Under compression-shear loading, the failure mode of the joint specimen can be classified into four types: coplanar shear failure, shear failure along the joint plane, shear failure along the shear stress plane, and similar integrity shear failure. The joint dip angle has a decisive effect on the failure mode of the specimen. The joint overlap affects the crack development of the specimen but does not change the failure mode of the specimen. The joint spacing can change the failure mode of the specimen. The shear strength of the specimen firstly increases and then decreases with the increase of the dip angle and reaches the maximum at 45°. The shear strength decreases with the increase of the joint overlap and increases with the increase of the joint spacing. The shear stress-displacement curves of different joint inclination samples have differences which mainly reflect in the postrupture stage. From monitoring results of the AE system, the variation regular of the AE count corresponds to the failure mode, and the peak value of the AE count decreases with the increase of joint overlap and increases with the increase of joint spacing.


1964 ◽  
Vol 19 (1) ◽  
pp. 127-133 ◽  
Author(s):  
S. E. Charm ◽  
W. McComis ◽  
G. Kurland

A structural model developed for kaolin suspensions was applied to blood in order to determine the structure and strength of the red cell suspensions. The yield stress of red cell suspensions determined in settling experiments agreed with the yield stress determined from shear stress-shear rate information employing Casson's equation. Theoretical considerations indicate that the shear stress-shear rate curve for blood should approach a straight line. This was found to be true at shear rates above 40 sec-1. The slope of this line was predicted from calculations based on sedimentation experiments and a modified Einstein's equation. The data suggest that the curvature of the shear stress-shear rate plot at low shear rates is due to aggregates of cells which break down under increasing shear rate, resulting finally in individual flocs. It is suggested that a floc consists of one to four cells with adhering plasma. The aggregate was calculated to have twice as much plasma associated with it as does a floc. However, the size of the aggregate could not be determined since the number of flocs associated with an aggregate could not be determined. shear stress-shear rate curve; red cell floc; red cell aggregate; sedimentation rate; blood viscosity and flow Submitted on February 28, 1963


2020 ◽  
Vol 6 (4) ◽  
pp. 489-501
Author(s):  
C. Kettenbeil ◽  
Z. Lovinger ◽  
S. Ravindran ◽  
M. Mello ◽  
G. Ravichandran

Author(s):  
Leonard F. Pease ◽  
Arich J. Fuher ◽  
Judith A. Bamberger ◽  
Carolyn A. Burns ◽  
Richard C. Daniel ◽  
...  

Abstract Slurries and sludges across the United States Department of Energy (DOE) complex rank among the most rheologically interesting. Their composition is heterogeneous, spanning a very broad range of particle sizes, densities, and interparticle forces. All exhibit shear thinning, some have yield stresses, and many are thixotropic. Despite the variety, these complex fluids are often represented using the historic Bingham fluid model, which fits higher shear rate data to a simple straight line. The intercept provides a yield stress, which has been a key design parameter in construction of large-scale waste processing facilities. However, many radioactive wastes are simply not Bingham fluids, and this representation extrapolates poorly across low to intermediate shear rates that are characteristic of typical processing conditions. Indeed, processing shear rates as high as 200 1/s, which has been a typical minimum shear rate used in fitting the Bingham fluid model, are seldom encountered in nuclear waste processing. Therefore, more realistic rheological models are necessary to accurately predict waste processing performance. Pacific Northwest National Laboratory (PNNL) recently re-evaluated the rheology of reconstituted Hanford REDOX (reduction-oxidation) process sludge waste against a wide variety of rheological models including the Bingham, Cross, Cross with yield stress, Carreau, biviscous, Herschel-Bulkley (which includes a power law dependence), Casson, and Gay models. They found that all of the models provided a closer fit than the Bingham model and that the biviscous model and Cross with yield stress model were convincing. However, reconstituted Hanford REDOX sludge waste is but one type of DOE waste and a direct contrast, and comparison of these three models against undiluted, unmixed tank waste (actual not simulant) has not been performed previously. Therefore, the purpose of this paper is to evaluate the rheology of actual tank waste with these more accurate rheological models. In this paper, we evaluate select rheological data for slurry samples from Hanford’s AZ-101, AZ-102, and SY-101 waste tanks. In each of these cases, we find that Cross’ model with yield stress and the biviscous model significantly outperform the Bingham fluid model. Furthermore, the AZ-101 data also shows that the shear stress peak at startup significantly exceeds the Bingham yield stress, which is commonly observed in the initial moments of rheological measurements on simulants. Remarkably, Cross’ model may empirically accommodate an initial spike in shear stress at modest shear rates. These are important observations because computational and analytical fluid dynamics simulations rely on rheological constitutive models for accurately and conservatively predicting waste processing performance. These findings suggest the need for better rheological modeling of and validation against radioactive waste.


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