Analysis and Testing of Dynamic Micromechanical Behavior of Composite Materials at Elevated Temperatures

1996 ◽  
Vol 118 (4) ◽  
pp. 554-560 ◽  
Author(s):  
R. H. Pant ◽  
R. F. Gibson

This paper describes the use of a recently developed high temperature impulse-frequency response apparatus to directly measure dynamic modulus and internal damping of high temperature composite materials, matrix materials, and reinforcing fibers as a function of temperature. An extensional vibration test was used for determination of the complex Young’s modulus of fiber specimens as a function of temperature. A flexural vibration test was used for determination of the complex flexural modulus of matrix and unidirectional composite specimens (0 and 90 deg fiber orientations) as a function of temperature. These results were obtained from tests done on two different fiber reinforced composite materials: boron/epoxy (B/E) and Silicon Carbide/Ti-6Al-4V (SiC/Ti). The results from these tests were then used to assess the validity of micromechanics predictions of composite properties at elevated temperatures. Micromechanics predictions of composite moduli and damping at elevated temperatures show good agreement with measured values for the 0 deg case (longitudinal) but only fair agreement for the 90 deg case (transverse). In both cases, the predictions indicate the correct trends in the properties.

2010 ◽  
Vol 44 (21) ◽  
pp. 2487-2507 ◽  
Author(s):  
G. Vargas ◽  
F. Mujika

The aim of this work is to compare from an experimental point of view the determination of in-plane shear strength of unidirectional composite materials by means of two off-axis tests: three-point flexure and tensile. In the case of the off-axis three-point flexure test, the condition of small displacements and the condition of lift-off between the specimen and the fixture supports have been taken into account. Some considerations regarding stress and displacement fields are presented. The in-plane shear characterization has been performed on a carbon fiber reinforced unidirectional laminate with several fiber orientation angles: 10°, 20°, 30°, and 45°. Test conditions for both off-axis experimental methods, in order to ensure their applicability, are presented. Off-axis flexure test is considered more suitable than off-axis tensile test for the determination of in-plane shear strength.


2007 ◽  
Vol 16 (6) ◽  
pp. 096369350701600 ◽  
Author(s):  
Theodore E. Matikas

Fibre reinforced metallic composite materials are being considered for a number of applications because of their attractive mechanical properties as compared to monolithic metallic alloys. An engineered interphase, including the bond strength between the composite's constituents, contributes to a large extent to the improvement of strength and stiffness properties of this class of materials. However, in high temperature applications, where combination of cyclic loading with environmental effects is expected, consideration should be given to interphase degradation, especially in the vicinity of stress risers, such as notches and holes. The applicability of damage tolerance analysis in structural components made of titanium matrix composite materials designed to operate under high temperature environments would depend on the availability of adequate characterization methods for the evaluation of interfacial degradation. The objective of this paper is to provide a basic understanding of interfacial degradation mechanisms due to oxidation in environmentally exposed titanium-based composites subjected to cyclic stresses. A non-destructive method has been developed enabling high-resolution monitoring of interfacial damage initiation and accumulation as well as surface/subsurface cracking behaviour during interrupted fatigue tests. This nondestructive technique is based on surface acoustic wave propagation in the composites and can detect minute changes in elastic properties of the interfacial region due to elevated temperatures as well as oxygen effects.


1995 ◽  
Vol 27/28 (3) ◽  
pp. 253-259 ◽  
Author(s):  
Joseph Giral ◽  
Daniel Hernandez ◽  
Bruno Rivoire ◽  
Jean-François Robert ◽  
Claude Royère ◽  
...  

2018 ◽  
Vol 272 ◽  
pp. 209-213 ◽  
Author(s):  
Milan Rydval ◽  
David Čítek ◽  
Jiří Kolísko ◽  
Zbyšek Pavlík

As part of the development and research of UHPC materials, the broad professional public deals mainly with the determination of the basic physical and mechanical parameters, in particular the compressive strength, that is considered as a determining parameter for these cement-based composites. The strength of the composite material is determined under normal laboratory conditions. Fine cement-based composite materials are increasingly used not only for academic purposes but also for practical applications. Therefore, it is necessary to focus on other parameters that determine these new Hi-Tech materials. The mechanical properties of materials at elevated temperatures belong to an area that is not properly defined not only in the Czech Republic but also in the world. Research into the behavior of these composite materials and their thermal loading can provide additional information and basics to expand these building materials such as France, USA, Japan and other countries around the world. In the Czech standards applicable to the design of concrete structures subjected to thermal stress, the values of the reduction coefficient Kc, θ are used only for commonly used dense concrete and also for expanded concrete. It is clear that these values cannot be used for fine-grained composite materials with cement binder reinforced hybrid reinforcements. The aim of the paper is to determine and describe the behavior of these materials in the temperature range of 20 ° C to 1000 ° C for two test modes that affect residual strength and high temperature strength.


Author(s):  
M. Larsen ◽  
R.G. Rowe ◽  
D.W. Skelly

Microlaminate composites consisting of alternating layers of a high temperature intermetallic compound for elevated temperature strength and a ductile refractory metal for toughening may have uses in aircraft engine turbines. Microstructural stability at elevated temperatures is a crucial requirement for these composites. A microlaminate composite consisting of alternating layers of Cr2Nb and Nb(Cr) was produced by vapor phase deposition. The stability of the layers at elevated temperatures was investigated by cross-sectional TEM.The as-deposited composite consists of layers of a Nb(Cr) solid solution with a composition in atomic percent of 91% Nb and 9% Cr. It has a bcc structure with highly elongated grains. Alternating with this Nb(Cr) layer is the Cr2Nb layer. However, this layer has deposited as a fine grain Cr(Nb) solid solution with a metastable bcc structure and a lattice parameter about half way between that of pure Nb and pure Cr. The atomic composition of this layer is 60% Cr and 40% Nb. The interface between the layers in the as-deposited condition appears very flat (figure 1). After a two hour, 1200 °C heat treatment, the metastable Cr(Nb) layer transforms to the Cr2Nb phase with the C15 cubic structure. Grain coarsening occurs in the Nb(Cr) layer and the interface between the layers roughen. The roughening of the interface is a prelude to an instability of the interface at higher heat treatment temperatures with perturbations of the Cr2Nb grains penetrating into the Nb(Cr) layer.


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