Extrusion of highly porous silicon nitride ceramics with bimodal pore structure and improved gas permeability

2017 ◽  
Vol 101 (2) ◽  
pp. 520-524 ◽  
Author(s):  
Guang-Peng Jiang ◽  
Jian-Feng Yang
Keyword(s):  
Silicon Nitride ◽  
Porous Silicon ◽  
Pore Structure ◽  
Gas Permeability ◽  
Nitride Ceramics ◽  
Highly Porous ◽  
Bimodal Pore Structure

scholarly journals Preparation of Porous Silicon Nitride Ceramics by Microwave Sintering and Its Performance Evaluation

2019 ◽  
Author(s):  
Chun-fang Xiao ◽  
Bing Han
Keyword(s):  
Silicon Nitride ◽  
Porous Silicon ◽  
Pore Structure ◽  
Microwave Sintering ◽  
Total Porosity ◽  
Boundary Phase ◽  
Sintering Process ◽  
Preparation Methods ◽  
Nitride Ceramics ◽  
Properties Of Materials

In this paper, the preparation methods of porous silicon nitride materials with controllable dielectric constant and pore structure were systematically studied. By using microwave sintering technology, porous silicon nitride materials with high closed pore ratio were prepared by adjusting the content of sintering additives and sintering process parameters, and controlling the grain boundary phase and pore structure and size. The effects of sintering conditions on the total porosity, closed porosity, pore structure and dielectric properties of materials were systematically studied.

Characterization of porous silicon nitride ceramics using bentonite as binder and sintering additive

2009 ◽  
Vol 60 (5) ◽  
pp. 456-460 ◽  
Author(s):  
Guang-Peng Jiang ◽  
Jian-Feng Yang ◽  
Ji-Qiang Gao ◽  
Koichi Niihara
Keyword(s):  
Silicon Nitride ◽  
Porous Silicon ◽  
Sintering Additive ◽  
Nitride Ceramics

Effects of Sintering Additives on the Microstructure and Mechanical Properties of Silicon Nitride Ceramics by GPS

2010 ◽  
Vol 105-106 ◽  
pp. 27-30 ◽  
Author(s):  
Wei Ru Zhang ◽  
Feng Sun ◽  
Ting Yan Tian ◽  
Xiang Hong Teng ◽  
Min Chao Ru ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Fracture Toughness ◽  
Phase Transformation ◽  
Silicon Nitride ◽  
Porous Silicon ◽  
Flexural Strength ◽  
Relative Density ◽  
Sintering Additives ◽  
Microstructure And Mechanical Properties ◽  
Nitride Ceramics

Silicon nitride ceramics were prepared by gas pressure sintering (GPS) with different sintering additives, including La2O3, Sm2O3 and Al2O3. Effect of sintering additives on the phase-transformation, microstructure and mechanical properties of porous silicon nitride ceramics was investigated. The results show that the reaction of sintering additives each other and with SiO2 had key effects on the phase-transformation, grain growing and grain boundaries. With 9MPa N2 atmosphere pressure, holding 1h at 1850°C, adding 10wt% one of the La2O3, Sm2O3, Al2O3, porous silicon nitride was prepared and the relative density was 78%, 72%, 85% respectively. The flexural strength was less than 500MPa, and the fracture toughness was less than 4.8MPam1/2. Dropping compounds sintering additives, such as La2O3+Al2O3, Sm2O3+Al2O3 effectively improves the sintering and mechanical properties. The relative density was 99.2% and 98.7% with 10wt% compounds sintering additives. The grain ratio of length to diameter was up to 1:8. The flexural strength was more than 900MPa, and the fracture toughness was more than 8.9MPam1/2.

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