On-line measurement of biomass using colloid dielectric probe and open-ended cell. Determination of the aggregation threshold

Author(s):  
M. Merabet
2001 ◽  
Vol 44 (2-3) ◽  
pp. 269-276 ◽  
Author(s):  
G. Ruban ◽  
Y. Yuperd ◽  
B. Laveau ◽  
E. Lucas

Continuous pollution measurement is interesting to optimize the operation of sanitary facilities as well as to minimize the stormwater discharges. An experimental study was carried out for the determination of Suspended Solids (SS) and Chemical Oxygen Demand (COD) concentrations in combined sewers using ultraviolet and visible absorbances. The maintenance of the measurement system requires six hours a month for the cleaning of the hydraulic feeding system and adjustment of the optical device. The feeding system developed increased the representativeness and reliability of the pollution measurement, but needs to be validated on other measurement sites. The determination of SS concentrations from visible absorbances requires 2 calibration curves for dry and rainy weather respectively. The corresponding accuracies appear satisfactory when compared with the results of standard sampling/laboratory analysis. The accuracy of COD determination from ultraviolet absorbance is less satisfactory, but could perhaps be improved taking into account another parameter. Then the optical measurement of SS and COD is interesting to determine average or long term pollution loads, for example the yearly impact of urban stormwater discharges. With this kind of continuous and on-line measurement, it is possible to react with short delay to unexpected phenomena which could damage the environment or water treatment efficiency.


2000 ◽  
Vol 33 (1) ◽  
pp. 10-25 ◽  
Author(s):  
Stefan Zaefferer

A new computer program for on-line crystallographic analysis in transmission electron microscopy (TEM) is presented. The program is based on the fast on-line determination of single-crystal orientations from Kikuchi and spot patterns. Spot patterns, which are particularly useful in the case of highly deformed metals, are analyzed by a new digital image processing procedure. This procedure improves the precision and ease of the orientation measurement. The program permits the on-line measurement of glide systems characterized by the Burgers vector and the crystallographic line direction of dislocations and their glide planes. The determination of twin systems, based on the misorientation calculation for any crystal structure, is included as well. The possibility of determining the foil thickness permits the complete crystallographic characterization of interfaces. Finally, the program facilitates the discrimination of phases and includes the fit of the lattice parametersa,bandcfrom diffraction patterns. The new procedures are described in detail. Application examples are given for all functions.


2000 ◽  
Vol os-9 (4) ◽  
pp. 1558925000OS-90
Author(s):  
Ayad Oumera ◽  
Abdelfattah M. Seyam ◽  
William Oxenham

The one-dimensional characteristic of yarn has resulted in very little attention being given to the uniformity of carded web in the cross machine direction. The development of nonwovens has prompted researchers to reconsider the importance of cross machine uniformity in determining the total uniformity of the carded web. It is therefore important to develop manual and online techniques to quantify cross machine uniformity at both the input and output of the card. At the card input, uniformity is taken as representing both mass and openness characteristics of the feed matt. While at the card output, there are many available techniques that allow the on-line measurement of the mass uniformity of the carded web, determination of uniformity at the input level is more difficult. The approach that was taken was to use an off-line technique to find the mass and openness of the feed matt at different locations across the card. While traditionally mass as a property has been given a lot of importance, much less attention has been given to the concept of openness. This is due in part to the difficulty in quantifying openness. Openness is believed to have great significance in determining the overall quality of the carded web, especially with regard to the formation of neps. In order to make the concept of openness more clear, it was found necessary to develop a way of quantifying it. This was done by performing a compression test on the feed matt, and then fitting the compression data with an exponential curve. The coefficient of the exponent was used to represent openness. This approach was used to find the effect of the feed roller (pin type) on cross machine uniformity. It was found that the squeezing of the feed roller did not have an effect in redistributing the mass of the feed matt, but did have an effect in changing the openness of the feed matt. Because of the difficulty involved in the handling of the feed matt, a newly developed technique is suggested to characterize openness. While this method still relies on the compression characteristics of the feed matt, it is more appropriate because it is performed on-line. Preliminary results are reported. It was found that thickness measurement under carefully selected pressure value could be used to characterize openness precisely.


1989 ◽  
Vol 35 (1) ◽  
pp. 64-68 ◽  
Author(s):  
H Echizen ◽  
R Itoh ◽  
T Ishizaki

Abstract This assay method allows the simultaneous determination of adenosine and dopamine in 0.5 mL of human urine within approximately 35 min, by using isocratic, reversed-phase, high-performance liquid chromatography coupled with an on-line detector for ultraviolet absorbance and electrochemical activity. The analytes were rapidly separated on an affinity column packed with phenylboronate-bonded silica. Mean recoveries for adenosine, 2-chloroadenosine (internal standard), dopamine, and (+/-)-isoproterenol (also an internal standard) were 91%, 99%, 88%, and 104%, respectively. The calibration curves for adenosine and dopamine were linear (r = 0.999, P less than 0.01) over the respective concentration ranges of 0.10 to 2.00 mg/L and 0.05 to 1.00 mg/L. Analytical precisions, assessed by the within-day and the day-to-day CVs, were 4.5% and 6.5% for adenosine, and 5.1% and 6.6% for dopamine, respectively. The mean (+/- SD) concentrations of adenosine (1.27 +/- 0.73 mg/L) and dopamine concentrations (0.38 +/- 0.25 mg/L) measured in urine from 19 healthy subjects agreed well with those previously reported.


2012 ◽  
Vol 571 ◽  
pp. 304-307
Author(s):  
Mei Zhao ◽  
Yu Fang Sha ◽  
Fei Guo ◽  
Ming Quan Yang

In view of bigger error (0.24%) of conventional measuring method, this paper focuses on a bigger aperture aerial camera focus measuring system and discusses measuring principle and structure of the system. The image in this system is received by the collimator of long focus and area CCD (Charge Coupled Devices) camera. Using dynamic scanning and center of gravity method, the system measures effectively the location and size of the optimum image. The image resolution of CCD can be up to one tenth of the size of the photosensitive sensor and the precision of 0.1percent of focus measuring can be obtained. The problem of the larger error of conventional measuring method is salved fundamentally. The accurate, real-time and on-line measurement of the focus of aerial camera lens can be realized and the exact determination of the position of the surface can be determined.


Author(s):  
John F. Mansfield ◽  
Douglas C. Crawford

A method has been developed that allows on-line measurement of the thickness of crystalline materials in the analytical electron microscope. Two-beam convergent beam electron diffraction (CBED) patterns are digitized from a JEOL 2000FX electron microscope into an Apple Macintosh II microcomputer via a Gatan #673 CCD Video Camera and an Imaging Systems Technology Video 1000 frame-capture board. It is necessary to know the lattice parameters of the sample since measurements are made of the spacing of the diffraction discs in order to calibrate the pattern. The sample thickness is calculated from measurements of the spacings of the fringes that are seen in the diffraction discs. This technique was pioneered by Kelly et al, who used the two-beam dynamic theory of MacGillavry relate the deviation parameter (Si) of the ith fringe from the exact Bragg condition to the specimen thickness (t) with the equation:Where ξg, is the extinction distance for that reflection and ni is an integer.


Author(s):  
M.A. Gribelyuk ◽  
M. Rühle

A new method is suggested for the accurate determination of the incident beam direction K, crystal thickness t and the coordinates of the basic reciprocal lattice vectors V1 and V2 (Fig. 1) of the ZOLZ plans in pixels of the digitized 2-D CBED pattern. For a given structure model and some estimated values Vest and Kest of some point O in the CBED pattern a set of line scans AkBk is chosen so that all the scans are located within CBED disks.The points on line scans AkBk are conjugate to those on A0B0 since they are shifted by the reciprocal vector gk with respect to each other. As many conjugate scans are considered as CBED disks fall into the energy filtered region of the experimental pattern. Electron intensities of the transmitted beam I0 and diffracted beams Igk for all points on conjugate scans are found as a function of crystal thickness t on the basis of the full dynamical calculation.


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