Microwave-Assisted Extraction and the Antioxidant Activity of Water-Soluble Polysaccharide from Palmaria palmata: Extraction Process and Antioxidant Activity of Polysaccharide from Palmaria palmate

2011 ◽  
Author(s):  
Zhong-rui Li ◽  
Bin Wang ◽  
Qi-hong Zhang ◽  
Fang-fang Huang ◽  
Jia-hui Ma
Keyword(s):  
Antioxidant Activity ◽  
Extraction Process ◽  
Water Soluble ◽  
Palmaria Palmata ◽  
Microwave Assisted Extraction ◽  
Microwave Assisted ◽  
Assisted Extraction ◽  
Soluble Polysaccharide

scholarly journals Optimization Of Microwave-Assisted Extraction Of Flavonoids From Binahong (Anredera cordifolia) Leaves Using Respon Surface Methodology

2020 ◽  
Vol 7 (3) ◽  
pp. 10-19
Author(s):  
Zaldy Rusli ◽  
Bina Lohita Sari ◽  
Novi Fajar Utami ◽  
S Sabila
Keyword(s):  
Antioxidant Activity ◽  
Ethanol Concentration ◽  
Antioxidant Activities ◽  
Extraction Process ◽  
Extraction Time ◽  
Microwave Assisted Extraction ◽  
Optimum Conditions ◽  
Microwave Assisted ◽  
Assisted Extraction

Binahong (Anredera scandens (L.) Moq.) leaves are one of the plants that empirically can be used for wound healing and contain flavonoids which have antibacterial and antioxidant activities. Determination of the optimum conditions of the Binahong leaf extraction process needs to be done to ensure the extraction quality of the Binahong leaves associated with the given activity. Microwave Assisted Extraction (MAE) is an extraction that utilizes microwave radiation to heat the solvent quickly and efficiently. This study aims to determine the most effective binahong leaf extraction conditions that produce optimal levels of flavonoids and antioxidant activity. The extraction process was carried out using the Microwave assisted extraction (MAE) method. Determination of optimum conditions is done based on Response Surface Method (RSM) with variable ethanol concentration (70%, 80% and 90%), extraction time (4, 12 and 20 minutes) and power (450, 600, and 800 watts) using Box- Behnken Design (BBD) with Design Expert 7.0 software. The extract quality parameters measured were total flavonoid levels and antioxidant activity. The results showed the optimum conditions with the BBD method were obtained at an ethanol concentration of 81.49%, extraction time of 13.84 minutes, and power of 626.19 watts with flavonoid levels of 3.8561% and antioxidant activity (IC50) of 95.51834 ppm with active categories.

scholarly journals Optimization of Microwave-Assisted Extraction (MAE) Time and Material to Solvent Ratio of Gembili (Dioscorea esculenta) Water-Soluble Polysaccharides (WSP)

2021 ◽  
Vol 10 (1) ◽  
pp. 78-98
Author(s):  
Widya Dwi Rukmi Putri ◽  
◽  
Eko Isro Riyanto ◽  
Almaria Heliana ◽  
Ambo Wellang ◽  
...  
Keyword(s):  
Water Soluble ◽  
Extraction Time ◽  
Solvent Ratio ◽  
Microwave Assisted Extraction ◽  
Optimum Conditions ◽  
Design Expert ◽  
Microwave Assisted ◽  
Assisted Extraction ◽  
Soluble Polysaccharide ◽  
Central Composite

Abstract Gembili (Dioscorea esculenta) is a tuber-producing plant containing 14.63% inulin, a Water-Soluble Polysaccharide (WSP). This study aims to determine the optimum point of material to solvent ratio and Microwave-Assisted Extraction (MAE) time needed to extract gembili WSP, and determine the WSP's characteristics produced. The optimization process uses the Response Surface Methodology-Central Composite Design (RSM-CCD) with Design Expert 7.0 software. The material to solvent ratio's minimum and maximum points are 1:25 g/L and 1:45 g/L, while the minimum and maximum points of extraction time are 20 minutes and 40 minutes. This study observed 13 experimental combinations and responses from gembili WSP yield, WSP powder inulin levels, and WSP solubility. The results showed that the optimum conditions of material to solvent were at a 1:33.81 g/mL ratio, and the extraction time was 29.26 minutes. This optimum condition resulted in 32.42% WSP yield, 40.8% inulin content in WSP powder, 26.98% WSP solubility, 12.24% WSP water content, and 49.3 cp WSP viscosity. These results indicate that extraction using a microwave can increase WSP's rich inulin yield from gembili tubers. Keywords: gembili, inulin, microwave, optimization, Water-Soluble Polysaccharides

Microwave-Assisted Extraction for Maximizing the Yield of Phenolic Compounds and Antioxidant Capacity from Cacao Pod Husk (Theobroma Cacao L.)

2020 ◽  
Vol 16 ◽  
Author(s):  
Van Tang Nguyen ◽  
Thi Dieu Pham ◽  
Long Binh Vu ◽  
Van Hoa Nguyen ◽  
Ngoc Le Tran
Keyword(s):  
Antioxidant Activity ◽  
Phenolic Compounds ◽  
Antioxidant Capacity ◽  
Extraction Efficiency ◽  
Water Soluble ◽  
Total Phenolic ◽  
Microwave Assisted Extraction ◽  
Microwave Assisted ◽  
Assisted Extraction ◽  
Phytochemical Compounds

Background: Extraction is an important step to obtain phytochemical compounds from natural materials. Among different extraction techniques, microwave-assisted extraction (MAE) is an advanced method with high extraction efficiency and low energy consumption. Objective: The aim of this study was to optimize the MAE parameters for obtaining the highest levels of phenolic compounds and antioxidant activity from cacao pod husk (CPH). Methods: The dried CPH was prepared using microwave drying method. The CPH extract was prepared using microwave-assisted extraction method. The powdered CPH extract was prepared using vacuum evaporation and freeze drying methods. Phytochemical compounds and antioxidant capacity of CPH extracts were analyzed using spectrophotometric methods. Results: The optimal MAE parameters were 600 W microwave power, 5 s/min irradiation time, 30 min extraction time, and 50 mL/g solvent to sample ratio. Under these MAE parameters, total phenolic content (TPC), phenolic extraction efficiency (PEE), saponin content (SC), and DPPH radical scavenging capacity (DRSC) were achieved from the CPH to be 10.97 mg GAE/g dried sample, 76.82%, 70.10 mg EE/g dried sample, and 141.18 mg DPPH/g dried sample, respectively, which were not significantly different from the predicted values (10.38 mg GAE/g dried sample, 72.68%, 70.09 mg EE/g dried sample, and 121.49 mg DPPH/g dried sample, respectively). The residual moisture, water activity, density, water soluble index and pH of powdered CPH extract were 9.72%, 0.38, 0.17 g/ml, 84.93% and 7.68, respectively. TPC, total flavonoid content (TFC) and SC of powdered CPH extract were 15.75 mg GAE/g dried sample, 27.03 mg CE/g dried sample and 133.67 mg EE/g dried sample, respectively. DRSC and ferric reducing antioxidant power (FRAP) of powdered CPH extract were 227.79 mg DPPH/g dried sample and 14.12 mg Fe(II)/g dried sample, respectively. Conclusion: The findings from this study reveal that the powdered extract obtained from the CPH at the optimal MAE parameters is a rich source of phytochemicals possessing great antioxidant activity. Therefore, it is a potential candidate to apply in the functional foods.

Orthogonal test in optimizing microwave-assisted extraction process of magnolin from Magnoliae Flos

2010 ◽  
Vol 30 (5) ◽  
pp. 567-568
Author(s):  
Xiao-li LI ◽  
Ming-yuan ZHANG ◽  
Wei-quan ZHAO ◽  
Man Li ◽  
Hai-ying TENG ◽  
...  
Keyword(s):  
Extraction Process ◽  
Orthogonal Test ◽  
Microwave Assisted Extraction ◽  
Microwave Assisted ◽  
Assisted Extraction

scholarly journals Microwave Assisted Extraction and Pressurized Liquid Extraction of Sulfated Polysaccharides from Fucus virsoides and Cystoseira barbata

Foods ◽  
2021 ◽  
Vol 10 (7) ◽  
pp. 1481
Author(s):  
Ana Dobrinčić ◽  
Sandra Pedisić ◽  
Zoran Zorić ◽  
Mladenka Jurin ◽  
Marin Roje ◽  
...  
Keyword(s):  
Antioxidant Activity ◽  
Chemical Composition ◽  
Liquid Extraction ◽  
Pressurized Liquid Extraction ◽  
Sulfate Group ◽  
Sulfated Polysaccharides ◽  
Microwave Assisted Extraction ◽  
Microwave Assisted ◽  
Assisted Extraction ◽  
Cystoseira Barbata

Sulfated polysaccharide fucoidan isolated from brown algae shows a wide range of biological activities that are significantly dependent on its chemical composition, which is closely related to the applied technique and extraction parameters. Therefore, the objective of this study was to evaluate the influence of microwave assisted extraction (MAE) and pressurized liquid extraction (PLE) parameters (solvent, temperature, time, and number of cycles) on the Fucus virsoides and Cystoseira barbata polysaccharide yield (%PS) and chemical composition (total sugar, fucose, and sulfate group). The optimal MAE parameters that resulted in the highest polysaccharide extraction from F. virsoides and C. barbata were 0.1 M H2SO4 for 10 min at 80 °C, while the optimal PLE parameters were 0.1 M H2SO4, for two cycles of 15 min at 140 °C. Furthermore, the %PS, chemical structure, molecular properties, and antioxidant activity of the F. virsoides and C. barbata polysaccharide extracts obtained with MAE, PLE, and conventional extraction (CE) performed under previously determinate optimal conditions were compared. PLE resulted in a significantly higher %PS from F. virsoides, while for C. barbata, a similar yield was achieved with CE and PLE, as well as CE and MAE, for both algae. Furthermore, the polysaccharides obtained using PLE had the highest polydispersity index, fucose, and sulfate group content, and the lowest uronic acid content; however their antioxidant activity was lower.

scholarly journals Microwave-Assisted Extraction and Ultrasound-Assisted Extraction of Bioactive Compounds from Grape Pomace

2020 ◽  
Vol 16 (1-2) ◽  
Author(s):  
Cassiano Brown da Rocha ◽  
Caciano Pelayo Zapata Noreña
Keyword(s):  
Antioxidant Activity ◽  
Phenolic Compounds ◽  
Bioactive Compounds ◽  
Grape Pomace ◽  
Total Phenolic ◽  
Microwave Assisted Extraction ◽  
Ultrasound Assisted Extraction ◽  
Microwave Assisted ◽  
Assisted Extraction ◽  
Ultrasound Assisted

AbstractThe grape pomace is a by-product from the industrial processing of grape juice, which can be used as a source of bioactive compounds. The aim of this study was to separate the phenolic compounds from grape pomace using an acidic aqueous solution with 2 % citric acid as a solvent, using both ultrasound-assisted extraction, with powers of 250, 350 and 450 W and times of 5, 10 and 15 min, and microwave-assisted extraction using powers of 600, 800 and 1,000 W and times of 5, 7 and 10 min. The results showed that for both methods of extraction, the contents of total phenolic compounds and antioxidant activity by ABTS and DPPH increased with time, and microwave at 1,000 W for 10 min corresponded to the best extraction condition. However, the contents of phenolic compounds and antioxidant activity were lower than exhaustive extraction using acidified methanol solution.

Sign in / Sign up

Export Citation Format

Share Document