In-situ, non-destructive identification of chemical elements by means of portable EDXRF spectrometer

1999 ◽  
Vol 46 (6) ◽  
pp. 2011-2016 ◽  
Author(s):  
C. Fiorini ◽  
A. Longoni
Keyword(s):  
Chemical Elements ◽  
Non Destructive

scholarly journals Laser-excited elastic guided waves reveal the complex mechanics of nanoporous silicon

2021 ◽  
Vol 12 (1) ◽  
Author(s):  
Marc Thelen ◽  
Nicolas Bochud ◽  
Manuel Brinker ◽  
Claire Prada ◽  
Patrick Huber
Keyword(s):  
Guided Waves ◽  
Laser Ultrasonics ◽  
Bulk Silicon ◽  
Nanoporous Silicon ◽  
Stiffness Reduction ◽  
Mechanical Characterisation ◽  
Isotropic Elasticity ◽  
On Chip ◽  
Non Destructive

AbstractNanoporosity in silicon leads to completely new functionalities of this mainstream semiconductor. A difficult to assess mechanics has however significantly limited its application in fields ranging from nanofluidics and biosensorics to drug delivery, energy storage and photonics. Here, we present a study on laser-excited elastic guided waves detected contactless and non-destructively in dry and liquid-infused single-crystalline porous silicon. These experiments reveal that the self-organised formation of 100 billions of parallel nanopores per square centimetre cross section results in a nearly isotropic elasticity perpendicular to the pore axes and an 80% effective stiffness reduction, altogether leading to significant deviations from the cubic anisotropy observed in bulk silicon. Our thorough assessment of the wafer-scale mechanics of nanoporous silicon provides the base for predictive applications in robust on-chip devices and evidences that recent breakthroughs in laser ultrasonics open up entirely new frontiers for in-situ, non-destructive mechanical characterisation of dry and liquid-functionalised porous materials.

In-Situ Characterization of Growth and Intermixing at a Heteroepitaxial Interface: Fe on Au(001)

1993 ◽  
Vol 318 ◽  
Author(s):  
Q. Jiang ◽  
A. Chan ◽  
Y.-L. He ◽  
G.-C. Wang
Keyword(s):  
Elevated Temperatures ◽  
Chemical Elements ◽  
Background Intensity ◽  
In Situ Characterization ◽  
Initial Stage ◽  
Monolayer Growth ◽  
Low Energy Electron ◽  
Energy Dependent

ABSTRACTThe growth and chemical intermixing of submonolayer and a few monolayer thick Fe films on a Au(001) surface was studied by High Resolution Low Energy Electron Diffraction (HRLEED) technique. Through the analysis of the energy dependent angular profiles as a function of time, we obtained the distribution of islands and distribution of spacings during submonolayer growth. The interference of electron waves from different chemical elements in terraces at different heights in the surface contributes to the background intensity and broadening in the angular profiles of diffraction beams. A subsurface Fe capped by Au islands as a result of atomic place exchange was observed at the initial stage of monolayer growth. From the energy dependent angular profiles as a function of temperature, we determine the quantitative change of inhomogeneity length (∼20 Å) at the interface of ultrathin films at elevated temperatures due to intermixing.

scholarly journals In-Situ Evaluation of the Protectivity of Coatings Applied to Metal Cultural Artefacts Using Non-Destructive Electrochemical Measurements

2021 ◽  
Vol 2 (1) ◽  
pp. 120-132
Author(s):  
Douglas J. Mills ◽  
Katarzyna Schaefer ◽  
Tomasz Wityk
Keyword(s):  
Baltic Sea ◽  
Electrochemical Noise ◽  
Organic Coating ◽  
Noise Measurement ◽  
The Baltic Sea ◽  
Coating Type ◽  
The Baltic ◽  
Non Destructive ◽  
Electrolytic Resistance

Electrochemical Noise Measurement (ENM) and DC electrolytic resistance measurement (ERM) can be used to assess the level of protectiveness provided by an organic coating (paint or varnish) to the underlying metal. These techniques also have applicability to the thinner, transparent type of coatings used to protect archaeological artefacts. Two studies are presented here demonstrating how ERM and ENM techniques can be applied in artefact preservation. The similarity of the techniques, both of which are a measure of resistance, means results can be considered to be analogous. The first study investigated the use of ERM to determine the protection levels provided by typical coatings in order to develop a database of coating type and application for objects, for specific environments. The second study used ENM to evaluate coatings which had been applied to historic artefacts recovered from shipwrecks in the Baltic Sea and displayed inside the museum or kept in the museum store area. The studies showed the usefulness of both techniques for determining the level of protection of a coating and how a better performing coating can be specified if a pre-existing coating on an artefact has been found to be unsuitable.

OCT-Einschweißtiefenüberwachung bei Unterdruck/OCT-based weld penetration monitoring at reduced ambient pressure – Influence of reduced ambient pressure on the OCT signal quality in laser deep penetration welding

2021 ◽  
Vol 111 (11-12) ◽  
pp. 863-868
Author(s):  
Thorsten Mattulat ◽  
Ronald Pordzik ◽  
Peer Woizeschke
Keyword(s):  
Penetration Depth ◽  
Ambient Pressure ◽  
Laser Beam Welding ◽  
In Situ Monitoring ◽  
Deep Penetration ◽  
Weld Penetration ◽  
Laser Deep Penetration Welding ◽  
Deep Penetration Welding ◽  
Non Destructive

Die optische Kohärenztomographie (OCT) erlaubt die zerstörungsfreie In-situ-Überwachung der Einschweißtiefe beim Laserstrahlschweißen. Für dieses Verfahren wird hier der Einfluss von verringerten Umgebungsdrücken auf die Messqualität untersucht. Es wird gezeigt, dass sich bei niedrigerem Umgebungsdruck deutlich größere Signalanteile aus dem Bereich des Bodens der Dampfkapillare zurückerhalten lassen. Auf diese Weise steigen die effektive Messfrequenz und die Erkennbarkeit von Änderungen der Einschweißtiefe.   Optical coherence tomography (OCT) enables non-destructive in-situ monitoring of the weld penetration depth during laser beam welding. For this technology, the influence of reduced ambient pressures on the measurement quality is investigated. It is shown that significantly larger signal components are obtained from the bottom of the vapor capillary at lower ambient pressure increasing the applicable measurement frequency and the detectability of changes in the weld penetration depth.

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