scholarly journals Neutron and x-ray scattering study of phonon dispersion and diffuse scattering in (Na,Bi)TiO3−xBaTiO3 single crystals near the morphotropic phase boundary

2017 ◽  
Vol 96 (17) ◽  
Author(s):  
Chengtao Luo ◽  
Dipanshu Bansal ◽  
Jiefang Li ◽  
Dwight Viehland ◽  
Barry Winn ◽  
...  
Author(s):  
Ilya V. Roslyakov ◽  
Andrei P. Chumakov ◽  
Andrei A. Eliseev ◽  
Alexey P. Leontiev ◽  
Oleg V. Konovalov ◽  
...  

1997 ◽  
Vol 30 (1) ◽  
pp. 16-20 ◽  
Author(s):  
A. Gibaud ◽  
D. Harlow ◽  
J. B. Hastings ◽  
J. P. Hill ◽  
D. Chapman

The technique of high-energy monochromatic Laue X-ray scattering using image plates to record the diffraction patterns is presented. A tunable wiggler beamline is used as an X-ray source. It is shown that such experimental conditions present many advantages over conventional tube sources and photographic films. A study of diffuse scattering in the perovskite compound KMnF3 is presented to illustrate this in a qualitative way.


2011 ◽  
Vol 110 (5) ◽  
pp. 053508 ◽  
Author(s):  
D. Dompoint ◽  
A. Boulle ◽  
I. Galben-Sandulache ◽  
D. Chaussende ◽  
L. T. M. Hoa ◽  
...  

2010 ◽  
Vol 43 (4) ◽  
pp. 867-875 ◽  
Author(s):  
A. Boulle ◽  
D. Dompoint ◽  
I. Galben-Sandulache ◽  
D. Chaussende

The X-ray scattering of partially transformed 3C-SiC single crystals is considered in detail. Extended diffuse scattering streaks, originating from stacking faults (SFs) lying in the {111} planes, are clearly observed in the wide-range reciprocal-space maps. The intensity distribution along the diffuse streaks is simulated with a model including the contributions of the diffuse scattering originating from the SFs [based on the pioneering theoretical description given by Kabra, Pandey & Lele (1986).J. Mater. Sci.21, 1654–1666], the coherent scattering emanating from untransformed areas of the crystals and all θ-dependent terms that affect the scattered intensity (the layer structure factor, the irradiated volume and the polarization of the beam). The quantitative simulation of the diffuse streaks reveals that the transformation occurs through the glide of partial dislocations and allows one to derive the transformation level. It is shown that the 3C polytype is indeed unstable at high temperature. However, it is further shown that defect-free 3C-SiC single crystals remain stable at temperatures where 3C-SiC is known to be usually unstable (2173 K). The origin of this apparent stability is very likely of kinetic nature,i.e.the lack of crystalline defects inhibits the transformation.


1996 ◽  
Vol 6 (8) ◽  
pp. 1085-1094 ◽  
Author(s):  
A. Gibaud ◽  
J. Wang ◽  
M. Tolan ◽  
G. Vignaud ◽  
S. K. Sinha

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