Band mapping of the weakly off-stoichiometric Heusler alloyNi49.7Mn29.1Ga21.2in the austenitic phase

2015 ◽  
Vol 91 (16) ◽  
Author(s):  
Y. Polyak ◽  
V. Drchal ◽  
J. Kudrnovský ◽  
O. Heczko ◽  
J. Honolka ◽  
...  
Keyword(s):  
Austenitic Phase ◽  
Band Mapping

scholarly journals Lath Martensite Microstructure Modeling: A High-Resolution Crystal Plasticity Simulation Study

Materials ◽  
2021 ◽  
Vol 14 (3) ◽  
pp. 691
Author(s):  
Francisco-José Gallardo-Basile ◽  
Yannick Naunheim ◽  
Franz Roters ◽  
Martin Diehl
Keyword(s):  
High Resolution ◽  
Mechanical Behavior ◽  
Crystal Plasticity ◽  
Lath Martensite ◽  
Three Dimensional ◽  
Building Blocks ◽  
Quantitative Agreement ◽  
Carbon Steels ◽  
Plastic Behavior ◽  
Austenitic Phase

Lath martensite is a complex hierarchical compound structure that forms during rapid cooling of carbon steels from the austenitic phase. At the smallest, i.e., ‘single crystal’ scale, individual, elongated domains, form the elemental microstructural building blocks: the name-giving laths. Several laths of nearly identical crystallographic orientation are grouped together to blocks, in which–depending on the exact material characteristics–clearly distinguishable subblocks might be observed. Several blocks with the same habit plane together form a packet of which typically three to four together finally make up the former parent austenitic grain. Here, a fully parametrized approach is presented which converts an austenitic polycrystal representation into martensitic microstructures incorporating all these details. Two-dimensional (2D) and three-dimensional (3D) Representative Volume Elements (RVEs) are generated based on prior austenite microstructure reconstructed from a 2D experimental martensitic microstructure. The RVEs are used for high-resolution crystal plasticity simulations with a fast spectral method-based solver and a phenomenological constitutive description. The comparison of the results obtained from the 2D experimental microstructure and the 2D RVEs reveals a high quantitative agreement. The stress and strain distributions and their characteristics change significantly if 3D microstructures are used. Further simulations are conducted to systematically investigate the influence of microstructural parameters, such as lath aspect ratio, lath volume, subblock thickness, orientation scatter, and prior austenitic grain shape on the global and local mechanical behavior. These microstructural features happen to change the local mechanical behavior, whereas the average stress–strain response is not significantly altered. Correlations between the microstructure and the plastic behavior are established.

scholarly journals Effect of weld metal composition on impact toughness properties of shielded metal arc welded ultra-high hard armor steel joints

2020 ◽  
Vol 29 (1) ◽  
pp. 186-194
Author(s):  
V. Balaguru ◽  
Visvalingam Balasubramanian ◽  
P. Sivakumar
Keyword(s):  
Impact Toughness ◽  
Weld Metal ◽  
Welded Joints ◽  
Weight Ratio ◽  
High Hardness ◽  
High Strength ◽  
Solidification Mode ◽  
Austenitic Phase ◽  
Ferrite Number ◽  
Steel Joints

AbstractNowadays, ultra-high hard armor (UHA) steels are employed in armor tracked vehicle (ATV) construction because of their high hardness, high strength to weight ratio, and excellent toughness. UHA steels are usually welded using austenitic stainless steel (ASS) welding consumables, to avoid hydrogen-induced cracking (HIC). The use of ASS consumables to weld the above steel was the only available remedy because of higher solubility of hydrogen in the austenitic phase. In this investigation, an attempt was made to investigate the effect of ASS consumables (with different Creq/Nieq ratio) on solidification mode, impact toughness and microstructural characteristics of shielded metal arc (SMA) welded UHA steel joints. The welded joints were characterised based on impact toughness properties, hardness, and microstructural features. As the ferrite number increases with an increase in Creq/Nieq ratio result in different solidification mode (A, FA, F). It is also found that ferrite number of weld metal has appreciable influence on impact toughness and has inversely proportional relationship with impact toughness of the welded joints.

Effects of Deformation Mode on Resistivity Curve Used for Estimating Martensite Induced in Stainless Steel

2010 ◽  
Vol 638-642 ◽  
pp. 2992-2997 ◽  
Author(s):  
Hidefumi Date
Keyword(s):  
Stainless Steel ◽  
Austenitic Stainless Steel ◽  
Linear Relation ◽  
Volume Fraction ◽  
Tensile Deformation ◽  
Deformation Mode ◽  
Transformation Process ◽  
Martensite Formation ◽  
Austenitic Phase ◽  
Ε Phase

The martensite induced in three types of austenitic stainless steel, which indicate the different stability of the austenitic phase (γ), were estimated by the resistivity measured during the tensile deformation or compressive deformation at the temperatures 77, 187 and 293 K. The resistivity curves were strongly dependent on the deformation mode. The volume fraction of the martensite (α’) was also affected by the deformation mode. The ε phase, which is the precursor of the martensite and is induced from the commencement of the deformation, decreased the resistivity. However, lots of defects generated by the deformation-induced martensite increased the resistivity. The experimental facts and the results shown by the modified parallelepiped model suggested a complicated transformation process depending on each deformation mode. The results shown by the model also suggested a linear relation between the resistivity and the martensite volume at the region of the martensite formation. The fact denoted that the resistivity is mostly not controlled by the austenite, ε phase and martensite, but by the defects induced due to the deformation-induced martensite.

In Situ Measurement of Poisson’s Ratio of Steel Plates During Thermal Processes Using Resonant Modes

2021 ◽  
Author(s):  
Clemens Grünsteidl ◽  
Christian Kerschbaummayr ◽  
Edgar Scherleitner ◽  
Bernhard Reitinger ◽  
Georg Watzl ◽  
...  
Keyword(s):  
Poisson’S Ratio ◽  
Dual Phase Steel ◽  
Steel Plates ◽  
Poisson's Ratio ◽  
Austenitic Phase ◽  
Resonant Modes ◽  
Longitudinal Sound Velocity ◽  
Contact Free

Abstract We demonstrate the determination of the Poisson’s ratio of steel plates during thermal processing based on contact free laser ultrasound measurements. Our method utilizes resonant elastic waves sustained by the plate, provides high amplitudes, and requires only a moderate detection bandwidth. For the analysis, the thickness of the samples does not need to be known. The trend of the measured Poisson’s ratio reveals a phase transformation in dual-phase steel samples. While previous approaches based on the measurement of the longitudinal sound velocity cannot distinguish between the ferritic and austenitic phase above 770°C, the shown method can. If the thickness of the samples is known, the method also provides both sound velocities of the material. The gained complementary information could be used to analyze phase composition of steel from low temperatures up to its melting point.

Diffusion and its Application in NiMnGa Alloys

2018 ◽  
Vol 19 ◽  
pp. 80-95 ◽  
Author(s):  
Le Zhou ◽  
Yong Ho Sohn
Keyword(s):  
Crystal Structure ◽  
Martensitic Transformation ◽  
Phase Diagrams ◽  
Diffusion Coefficients ◽  
Diffusion Couples ◽  
Arrhenius Behavior ◽  
Ferromagnetic Shape Memory Alloys ◽  
Two Phase ◽  
Austenitic Phase ◽  
Practical Applications

Heusler NiMnGa alloys are often categorized as ferromagnetic shape memory alloys or magnetocaloric materials, which are important for both practical applications and fundamental research. The NiMnGa alloys undergo a series of diffusion and diffusionless transformation from high temperature to low temperature. Among these transformation, martensitic transformation from austenitic phase to martensitic phase is critical in determining the properties of the alloys. Although martensitic transformation is considered diffusionless, diffusion also has important applications in the research of NiMnGa alloysDiffusion couples along with equilibrium alloys have been used to determine the ternary phase diagrams in NiMnGa alloys. Phase diagrams are important in selecting NiMnGa alloys, in particular two-phase NiMnGa alloys for practical applications. Furthermore, the diffusion couples effectively assist in the determination of compositions that exhibit martensitic transformation temperature near room temperature. Diffusion coefficients have been assessed for NiMnGa alloys. Tracer diffusivity of Ni, Mn and Ga was reported in a wide temperature range and followed Arrhenius behavior. Two different activation energies were obtained, corresponding to B2 and L21 crystal structure, respectively. Interdiffusion coefficients for NiMnGa alloys with B2 crystal structure are measured, which showed that Ni diffuses the fastest, followed by Mn then Ga. The diffusion coefficients provide useful information for fabricating NiMnGa alloys through diffusional process.A combinatorial approach involving diffusion couples and advance characterization has been developed to investigate the mechanical properties, microstructure and crystallography of NiMnGa alloys rapidly and systematically over a large compositional range. The composition-dependent modulus and hardness for NiMnGa alloys was extracted from the diffusion couples with the help of nanoindentation. Martensitic phases with non-modulated and various modulated crystal structures, and austenitic phase were identified in the interdiffusion zones by transmission electron microscopy. The results demonstrate the capability of using diffusion couples to speed up the discovery of new NiMnGa alloys or other similar alloys showing martensitic transformation.

scholarly journals Structural Characterisation and Mechanical FE Analysis of Conventional and M-Wire Ni-Ti Alloys Used in Endodontic Rotary Instruments

2014 ◽  
Vol 2014 ◽  
pp. 1-8 ◽  
Author(s):  
Diogo Montalvão ◽  
Francisca Sena Alçada ◽  
Francisco Manuel Braz Fernandes ◽  
Sancho de Vilaverde-Correia
Keyword(s):  
Body Temperature ◽  
Mechanical Response ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
Austenitic Phase ◽  
X Ray ◽  
Structural Characterisation ◽  
Working Temperature ◽  
Ti Alloys ◽  
Rotary Instruments

The purpose of this study is to understand how the M-Wire alloy conditions the mechanical flexibility of endodontic rotary files at body temperature.Two different rotary instruments, a Profile GT 20/.06 and a Profile GT Series X 20/.06, were selected due to their geometrical similarity and their different constituent alloy. GT series X files are made from M-Wire, a Ni-Ti alloy allegedly having higher flexibility at body temperature. Both files were analysed by X-Ray Diffraction and Differential Scanning Calorimetry to investigate phase transformations and the effects of working temperature on these different alloys. Mechanical behaviour was assessed by means of static bending and torsional Finite Element simulations, taking into account the nonlinear superelastic behaviour of Ni-Ti materials. It was found that GT files present austenitic phase at body temperature, whereas GT series X present R-phase at temperatures under 40°C with a potential for larger flexibility. For the same load conditions, simulations showed that the slight geometrical differences between the two files do not introduce great disagreement in the instruments’ mechanical response. It was confirmed that M-Wire increases the instrument’s flexibility, mainly due to the presence of R-phase at body temperature.

Valence band and core-level photoemission of Au/Ge(001): Band mapping and bonding sites

2014 ◽  
Vol 90 (12) ◽  
Author(s):  
S. Meyer ◽  
L. Dudy ◽  
J. Schäfer ◽  
C. Blumenstein ◽  
P. Höpfner ◽  
...  
Keyword(s):  
Valence Band ◽  
Core Level ◽  
Band Mapping
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