Crystal structure ofHgBa2Ca2Cu3O8+δat high pressure (to 8.5 GPa) determined by powder neutron diffraction

1995 ◽  
Vol 52 (21) ◽  
pp. 15551-15557 ◽  
Author(s):  
A. R. Armstrong ◽  
W. I. F. David ◽  
I. Gameson ◽  
P. P. Edwards ◽  
J. J. Capponi ◽  
...  
Keyword(s):  
Crystal Structure ◽  
High Pressure ◽  
Neutron Diffraction ◽  
Powder Neutron Diffraction

Temperature dependence of the crystal structure of α-AgSCN by powder neutron diffraction

2007 ◽  
Vol 40 (6) ◽  
pp. 1039-1043 ◽  
Author(s):  
Darrick J. Williams ◽  
L. L. Daemen ◽  
S. C. Vogel ◽  
Th. Proffen
Keyword(s):  
Crystal Structure ◽  
High Pressure ◽  
Neutron Diffraction ◽  
Structural Changes ◽  
Rietveld Method ◽  
Tetrahedral Coordination ◽  
Bond Lengths ◽  
Powder Neutron Diffraction ◽  
Different Temperatures ◽  
Neutron Powder Diffractometer

A structural study of α-AgSCN was carried out using the neutron powder diffractometer HIPPO (high-pressure preferred orientation powder) at ten different temperatures between 25 and 275 K. The structure of α-AgSCN was refined using the Rietveld method and the symmetry elements for the material were found to be: space group No. 15,C2/c,a= 8.7210 (8) Å,b= 7.9318 (8) Å,c= 12.3329 (5) Å, β = 138.750 (3)°, volume = 562.497 (9) Å3andZ= 8. The Ag+cation has tetrahedral coordination and is surrounded by three –SCN thiocyanate ligands and one isothiocyanate –NCS ligand down to 25 K, with no structural changes. The bond lengths at 275 K are Ag—S1 = 2.749 (10), Ag—S2 = 2.995 (11), Ag—S3 = 2.411 (11), Ag—N = 2.150 (5), S—C = 1.783 (11) and C—N = 1.1447 (35) Å. The bond lengths at 25 K are Ag—S1 = 2.782 (5), Ag—S2 = 2.941 (5), Ag—S3 = 2.431 (5), Ag—N = 2.1526 (26), S—C = 1.749 (5) and C—N = 1.140 (2) Å.

Crystal structure determination by powder neutron diffraction at the spallation neutron source, ISIS

Nature ◽  
1986 ◽  
Vol 320 (6057) ◽  
pp. 46-48 ◽  
Author(s):  
A. K. Cheetham ◽  
W. I. F. David ◽  
M. M. Eddy ◽  
R. J. B. Jakeman ◽  
M. W. Johnson ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Neutron Diffraction ◽  
Neutron Source ◽  
Structure Determination ◽  
Crystal Structure Determination ◽  
Spallation Neutron Source ◽  
Powder Neutron Diffraction

Neutron diffraction study of the crystal structure of TlInSe2 at high pressure

2019 ◽  
Vol 33 (15) ◽  
pp. 1950149 ◽  
Author(s):  
N. T. Mamedov ◽  
S. H. Jabarov ◽  
D. P. Kozlenko ◽  
N. A. Ismayilova ◽  
M. Yu. Seyidov ◽  
...  
Keyword(s):  
Crystal Structure ◽  
High Pressure ◽  
Neutron Diffraction ◽  
Tetragonal Phase ◽  
Unit Cell Volume ◽  
Diffraction Method ◽  
Lattice Parameter ◽  
Neutron Diffraction Study ◽  
Pressure Derivative ◽  
Neutron Diffraction Method

We have investigated the crystal structure of strongly anisotropic semiconductor TlInSe2 by neutron diffraction method under high pressure upto P = 3.3 GPa. It was shown that the tetragonal phase of TlInSe2 crystal (the space group I4/mcm) is stable in the whole investigated range of pressure. The lattice parameters dependence of the pressure and the unit cell volume are obtained, the linear coefficients of compressibility and the bulk moduli are calculated. At the low pressure, obtained value of compressibility for the lattice parameter a is k[Formula: see text] = 14.23 × 10[Formula: see text] GPa[Formula: see text] and for c is k[Formula: see text] = 5.93 × 10[Formula: see text] GPa[Formula: see text]. Obtained values for bulk modulus B0 and its pressure derivative B[Formula: see text] in tetragonal phase are 30(7) GPa and 4(1), respectively.

Problems of studying the crystal structure of Ce1−xLax11B6 solid solutions by high-resolution powder neutron diffraction

1991 ◽  
Vol 24 (2) ◽  
pp. 142-145 ◽  
Author(s):  
V. A. Trunov ◽  
A. L. Malyshev ◽  
D. Yu. Chernyshov ◽  
A. I. Kurbakov ◽  
M. M. Korsukova ◽  
...  
Keyword(s):  
Crystal Structure ◽  
High Resolution ◽  
Neutron Diffraction ◽  
Solid Solutions ◽  
Powder Neutron Diffraction

The Structure of High Pressure Ca(OD)2II from Powder Neutron Diffraction: Relationship to the ZrO2and EuI2Structures

1997 ◽  
Vol 132 (2) ◽  
pp. 267-273 ◽  
Author(s):  
Kurt Leinenweber ◽  
Dan E. Partin ◽  
Udo Schuelke ◽  
Michael O'Keeffe ◽  
Robert B. Von Dreele
Keyword(s):  
High Pressure ◽  
Neutron Diffraction ◽  
Powder Neutron Diffraction

Pressure dependence of crystal structure of Cu2O by TOF powder neutron diffraction

2014 ◽  
Vol 262 ◽  
pp. 622-624
Author(s):  
Yoshihisa Ishikawa ◽  
Takashi Sakuma ◽  
Haruyuki Takahashi ◽  
Sergey A. Danilkin
Keyword(s):  
Crystal Structure ◽  
Neutron Diffraction ◽  
Pressure Dependence ◽  
Powder Neutron Diffraction

scholarly journals A High Pressure Experiment of Powder Neutron Diffraction on the HRPD at JRR-3

2008 ◽  
Vol 18 (2) ◽  
pp. 170-172 ◽  
Author(s):  
Kazuki KOMATSU ◽  
Hiroshi ARIMA ◽  
Hiroyuki KAGI ◽  
Takuo OKUCHI ◽  
Shigeo SASAKI ◽  
...  
Keyword(s):  
High Pressure ◽  
Neutron Diffraction ◽  
Powder Neutron Diffraction ◽  
Pressure Experiment ◽  
High Pressure Experiment
Sign in / Sign up

Export Citation Format

Share Document