Static density response function studied by inelastic x-ray scattering: Friedel oscillations in solid and liquid Li

2020 ◽  
Vol 102 (5) ◽  
Author(s):  
Toru Hagiya ◽  
Kazuhiro Matsuda ◽  
Nozomu Hiraoka ◽  
Yukio Kajihara ◽  
Koji Kimura ◽  
...  
Keyword(s):  
Response Function ◽  
X Ray ◽  
Friedel Oscillations ◽  
X Ray Scattering ◽  
Density Response Function ◽  
Density Response ◽  
Ray Scattering

Friedel oscillations and charge density wave pinning in quasi-one dimensional conductors: Thermal effects

2002 ◽  
Vol 12 (9) ◽  
pp. 9-14
Author(s):  
J.-P. Pouget ◽  
S. Ravy ◽  
S. Rouziere ◽  
S. Brazovskii
Keyword(s):  
Charge Density ◽  
Interference Effect ◽  
Charge Density Wave ◽  
Density Wave ◽  
Thermal Dependence ◽  
One Dimensional ◽  
X Ray ◽  
Friedel Oscillations ◽  
X Ray Scattering ◽  
Ray Scattering

An original interference effect observed in one-dimensional (1D) disordered conductors between X-ray scattering due to the disorder and the charge density wave (CDW)- periodic lattice modulation (PLD) allows to study the pinning of the modulation at local scale. We apply this effect to determine the phase of the CDW at the pinning centres and to show that the response of the CDW to the impurity potential leads to the formation of Friedel oscillations (FO). We report experimental determination and quantitative interpretation of the thermal evolution of both features. The thermal dependence of the interference effect allows one to determine the pinning energy of the 2kF-CDW in the V-and W-doped blue bronzes. We show in particular that in these compounds the regular CDW is pinned to the dopant dressed by its FO. In the organic charge transfer salts irradiation leads to an enhancement of the 2kF and 4kF X-ray scattering that we show, by its thermal dependence, to be due to the formation of FO.

scholarly journals Dynamical response function in sodium studied by inelastic x-ray scattering spectroscopy

2011 ◽  
Vol 84 (7) ◽  
Author(s):  
Simo Huotari ◽  
Marco Cazzaniga ◽  
Hans-Christian Weissker ◽  
Tuomas Pylkkänen ◽  
Harald Müller ◽  
...  
Keyword(s):  
Response Function ◽  
Dynamical Response ◽  
X Ray ◽  
X Ray Scattering ◽  
Ray Scattering

Microtubule nucleation sequence studied by time-resolved x-ray scattering and electron microscopy

1983 ◽  
Vol 41 ◽  
pp. 766-767
Author(s):  
Eva-Maria Mandelkow ◽  
Eckhard Mandelkow ◽  
Joan Bordas
Keyword(s):  
Electron Microscopy ◽  
Dynamic Equilibrium ◽  
Time Resolved ◽  
X Ray ◽  
Additional Information ◽  
X Ray Scattering ◽  
Low Concentrations ◽  
Microtubule Growth ◽  
Ray Patterns ◽  
Ray Scattering

When a solution of microtubule protein is changed from non-polymerising to polymerising conditions (e.g. by temperature jump or mixing with GTP) there is a series of structural transitions preceding microtubule growth. These have been detected by time-resolved X-ray scattering using synchrotron radiation, and they may be classified into pre-nucleation and nucleation events. X-ray patterns are good indicators for the average behavior of the particles in solution, but they are difficult to interpret unless additional information on their structure is available. We therefore studied the assembly process by electron microscopy under conditions approaching those of the X-ray experiment. There are two difficulties in the EM approach: One is that the particles important for assembly are usually small and not very regular and therefore tend to be overlooked. Secondly EM specimens require low concentrations which favor disassembly of the particles one wants to observe since there is a dynamic equilibrium between polymers and subunits.

Time-Resolved Cryo-Electron Microscopy of Oscillating Microtubules

1990 ◽  
Vol 48 (1) ◽  
pp. 502-503
Author(s):  
Eva-Maria Mandelkow ◽  
Ron Milligan
Keyword(s):  
Electron Microscopy ◽  
Dynamic Instability ◽  
Entire Solution ◽  
Reaction Scheme ◽  
Time Resolved ◽  
X Ray ◽  
X Ray Scattering ◽  
A Chain ◽  
Ray Scattering

Microtubules form part of the cytoskeleton of eukaryotic cells. They are hollow libers of about 25 nm diameter made up of 13 protofilaments, each of which consists of a chain of heterodimers of α-and β-tubulin. Microtubules can be assembled in vitro at 37°C in the presence of GTP which is hydrolyzed during the reaction, and they are disassembled at 4°C. In contrast to most other polymers microtubules show the behavior of “dynamic instability”, i.e. they can switch between phases of growth and phases of shrinkage, even at an overall steady state [1]. In certain conditions an entire solution can be synchronized, leading to autonomous oscillations in the degree of assembly which can be observed by X-ray scattering (Fig. 1), light scattering, or electron microscopy [2-5]. In addition such solutions are capable of generating spontaneous spatial patterns [6].In an earlier study we have analyzed the structure of microtubules and their cold-induced disassembly by cryo-EM [7]. One result was that disassembly takes place by loss of protofilament fragments (tubulin oligomers) which fray apart at the microtubule ends. We also looked at microtubule oscillations by time-resolved X-ray scattering and proposed a reaction scheme [4] which involves a cyclic interconversion of tubulin, microtubules, and oligomers (Fig. 2). The present study was undertaken to answer two questions: (a) What is the nature of the oscillations as seen by time-resolved cryo-EM? (b) Do microtubules disassemble by fraying protofilament fragments during oscillations at 37°C?

X-ray scattering by 1D molecular Guinier-Preston zones in ordered smectic phases

1992 ◽  
Vol 2 (6) ◽  
pp. 899-913 ◽  
Author(s):  
Patrick Davidson ◽  
Elisabeth Dubois-Violette ◽  
Anne-Marie Levelut ◽  
Brigitte Pansu
Keyword(s):  
X Ray ◽  
X Ray Scattering ◽  
Smectic Phases ◽  
Ray Scattering

An X-ray Scattering Study of Laterally Modulated Structures: Investigation of Coherence and Resolution Effects with a Grating

1996 ◽  
Vol 6 (8) ◽  
pp. 1085-1094 ◽  
Author(s):  
A. Gibaud ◽  
J. Wang ◽  
M. Tolan ◽  
G. Vignaud ◽  
S. K. Sinha
Keyword(s):  
X Ray ◽  
X Ray Scattering ◽  
Modulated Structures ◽  
Scattering Study ◽  
Ray Scattering

Pixel detectors: New detectors for X-ray scattering

2002 ◽  
Vol 12 (6) ◽  
pp. 385-390 ◽  
Author(s):  
J.-F. Bérar ◽  
L. Blanquart ◽  
N. Boudet ◽  
P. Breugnon ◽  
B. Caillot ◽  
...  
Keyword(s):  
X Ray ◽  
X Ray Scattering ◽  
Pixel Detectors ◽  
Ray Scattering
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