scholarly journals Strain rate sensitivity of the tensile strength of two silicon carbides: experimental evidence and micromechanical modelling

Author(s):  
Jean-Luc Zinszner ◽  
Benjamin Erzar ◽  
Pascal Forquin

Ceramic materials are commonly used to design multi-layer armour systems thanks to their favourable physical and mechanical properties. However, during an impact event, fragmentation of the ceramic plate inevitably occurs due to its inherent brittleness under tensile loading. Consequently, an accurate model of the fragmentation process is necessary in order to achieve an optimum design for a desired armour configuration. In this work, shockless spalling tests have been performed on two silicon carbide grades at strain rates ranging from 10 3 to 10 4  s −1 using a high-pulsed power generator. These spalling tests characterize the tensile strength strain rate sensitivity of each ceramic grade. The microstructural properties of the ceramics appear to play an important role on the strain rate sensitivity and on the dynamic tensile strength. Moreover, this experimental configuration allows for recovering damaged, but unbroken specimens, giving unique insight on the fragmentation process initiated in the ceramics. All the collected data have been compared with corresponding results of numerical simulations performed using the Denoual–Forquin–Hild anisotropic damage model. Good agreement is observed between numerical simulations and experimental data in terms of free surface velocity, size and location of the damaged zones along with crack density in these damaged zones. This article is part of the themed issue ‘Experimental testing and modelling of brittle materials at high strain rates’.

Author(s):  
Muhammad Yasir Khalid ◽  
Zia Ullah Arif ◽  
Waqas Ahmed ◽  
Hassan Arshad

There has been an ever-going need for materials containing excellent mechanical properties, lower density, and improved fuel efficiency in the aerospace industry. To date, Fiber Metal Laminates (FMLs) are a prime choice for aerospace applications. The components of aircraft are subjected to various mechanical loadings under operating conditions; therefore, an in-depth understanding of material behavior under expected loading conditions is imperative for the meticulous design and manufacturing of these components. To evaluate the tensile behavior of the FMLs containing Aluminum 7075-T6 sheets as a metallic phase was the primary aim of this study. Furthermore, the manufactured composites were treated with the processes including surface de-greasing, mechanical abrasion, and anodizing. In order to perform mechanical characterization, uniaxial tensile tests were conducted at various strain rates 2×10−4 s−1, 5×10−4 s−1 and 8×10−4 s−1. The FMLs were fabricated through vacuum-assisted resin transfer molding (VARTM) process. The results revealed that FMLs based different combinations of the fiber and metal constituents exhibited a low degree of strain rate-sensitivity. In the case of CARALL, 1.7% increase in tensile strength was observed, and, its tensile strength was increased from 741 MPa to 754 MPa. Whereas, ARALL and GLARE laminates exhibited high degree of strain rate-sensitivity. When the strain rate is increased from 2×10−4 s−1, 5×10−4 s−1 and 8×10−4 s−1 the values are increased in the following patterns: 389 MPa, 411 MPa, and 475 MPa for GLARE laminates, and 253 MPa, 298 MPa 352 MPa for ARALL laminates. Thus, 39% and 22% increase in the tensile strengths were noted for ARALL and GLARE laminates, respectively.


2006 ◽  
Vol 503-504 ◽  
pp. 31-36 ◽  
Author(s):  
Johannes Mueller ◽  
Karsten Durst ◽  
Dorothea Amberger ◽  
Matthias Göken

The mechanical properties of ultrafine-grained metals processed by equal channel angular pressing is investigated by nanoindentations in comparison with measurements on nanocrystalline nickel with a grain size between 20 and 400 nm produced by pulsed electrodeposition. Besides hardness and Young’s modulus measurements, the nanoindentation method allows also controlled experiments on the strain rate sensitivity, which are discussed in detail in this paper. Nanoindentation measurements can be performed at indentation strain rates between 10-3 s-1 and 0.1 s-1. Nanocrystalline and ultrafine-grained fcc metals as Al and Ni show a significant strain rate sensitivity at room temperature in comparison with conventional grain sized materials. In ultrafine-grained bcc Fe the strain rate sensitivity does not change significantly after severe plastic deformation. Inelastic effects are found during repeated unloading-loading experiments in nanoindentations.


2019 ◽  
Vol 2019 (1) ◽  
pp. 000480-000487
Author(s):  
Luke A. Wentlent ◽  
James Wilcox ◽  
Xuanyi Ding

Abstract As the electronics industry continues to evolve a concerted effort has developed to implement lower melting point solders. The ability to minimize the thermal exposure that an assembly is subjected to affords significant benefits with respect to both the reliability and the materials that can be used. One of the most popular low melt solder alloys currently being investigated by the industry is the Bi-Sn eutectic system, which has a melting point of 139°C. The BiSn system itself is not particularly novel as it was posited as a SAC alternative during the initial shift from Pb based solders. While a body of knowledge currently exists regarding this system, and the near eutectic variant BiSnAg, there are still concerns regarding its ductility, especially as a function of thermal exposure and strain rate. Bismuth is widely acknowledged as a brittle element and its presence in such quantities raises concerns of not just Cu6Sn5 embrittlement but also solder fragility in high strain rate types of environments. A challenge with regards to near term implementation is that most packages are not available with BiSn solder bumps. Therefore, it will be necessary to use components already balled with SAC 305 solder. This means that the resulting solder interconnect, reflowed below conventional SAC reflow temperatures, will form a type of mixed hybrid microstructure. This non-equilibrium microstructure will be composed of two regions, one Bi-rich region which is well past saturation and a second region which is Bi-deficient. It is of specific industrial interest then to not just investigate the BiSn solder system but also within the context of a realistic mixed interconnect. Recent work by several researchers has shown that this hybrid microstructure is unstable and quite active with respect to the movement and localized concentration of the Bismuth. The degree of mixing of these two regions has been shown to be highly dependent upon reflow temperature and the paste to ball volume ratio. Mixed SAC-BiSn solder joints were formed by placing SAC 305 spheres on BiSn paste deposits for a paste to ball volume ratio of .18. These samples were then reflowed at either 175°C or 200°C. SAC 305 control samples were also made using a conventional Pb-free reflow profile with a peak temperature of 247°C. A 22 mil Cu-OSP pad on a 1.0 mm thick FR4 substrate was used for all samples. A selection of the solder joints were then isothermally aged at 90°C for 200 hours. Using a joint level micromechanical tester, ball shear tests were conducted at a range of strain rates for samples in the as-reflowed and aged state. Using this information, the strain rate sensitivity of the interconnects was mapped and correlated with the observed failure modes. Investigations into the fracture mechanisms were conducted by examining the shear fracture surface with optical and scanning electron microscopy. Additionally, the evolution of the microstructure was characterized. Results showed a clear transition from ductile solder failure to a brittle separation failure at the higher strain rates.


Metals ◽  
2019 ◽  
Vol 9 (3) ◽  
pp. 344 ◽  
Author(s):  
Simon Sevsek ◽  
Christian Haase ◽  
Wolfgang Bleck

The strain-rate-dependent deformation behavior of an intercritically annealed X6MnAl12-3 medium-manganese steel was analyzed with respect to the mechanical properties, activation of deformation-induced martensitic phase transformation, and strain localization behavior. Intercritical annealing at 675 °C for 2 h led to an ultrafine-grained multi-phase microstructure with 45% of mostly equiaxed, recrystallized austenite and 55% ferrite or recovered, lamellar martensite. In-situ digital image correlation methods during tensile tests revealed strain localization behavior during the discontinuous elastic-plastic transition, which was due to the localization of strain in the softer austenite in the early stages of plastic deformation. The dependence of the macroscopic mechanical properties on the strain rate is due to the strain-rate sensitivity of the microscopic deformation behavior. On the one hand, the deformation-induced phase transformation of austenite to martensite showed a clear strain-rate dependency and was partially suppressed at very low and very high strain rates. On the other hand, the strain-rate-dependent relative strength of ferrite and martensite compared to austenite influenced the strain partitioning during plastic deformation, and subsequently, the work-hardening rate. As a result, the tested X6MnAl12-3 medium-manganese steel showed a negative strain-rate sensitivity at very low to medium strain rates and a positive strain-rate sensitivity at medium to high strain rates.


2019 ◽  
Vol 298 ◽  
pp. 43-51
Author(s):  
Jia Yong Si ◽  
Song Hao Liu ◽  
Long Chen

This research investigated the effect of hot extrusion on the flow behaviour of nickel-based superalloy FGH4096 by hot compression experiments in the temperature range from 1020 to 1110 °C and strain rates ranging from 0.1 to 0.001 s-1. The influence of the hot extrusion on the initial microstructures, work hardening rate, strain rate sensitivity, and activation energy of deformation were discussed. The results show that the extruded microstructure is constituted by the fine dynamic recrystallisation of grains. The true strain-true stress curves show that the as-HIPed and as-HEXed FGH4096 superalloy present double flow stress peaks and discontinuous flow softening. The as-HEXed FGH4096 is easily dynamically softened at high temperatures and high strain rates compared with as-HIPed microstructures. As for the work hardening rate, the as-HEXed FGH4096 exhibits higher θ values than that of as-HIPed. It is beneficial to the homogenous deformation and grain refinement during subsequent turbine disk forging. Comparing to as-HIPed FGH4096, the highest strain rate sensitivity value of as-HEXed is 0.306 at 1110 °C. The isothermal superplastic forging of a P/M turbine disk may be carried out at this temperature. The deformation activation energy value of the as-HIPed FGH4096 is lower which means that dislocation sliding and climbing can be easily initiated in the as-HIPed alloy.


2018 ◽  
Vol 115 (5) ◽  
pp. 507
Author(s):  
Onur Çavusoglu ◽  
Hakan Gürün ◽  
Serkan Toros ◽  
Ahmet Güral

In this study, strain hardening and strain rate sensitivity behavior of commercial DP1000 dual phase steel have been examined in detail at temperatures of 25 °C, 100 °C, 200 °C and 300 °C, at strain rates of 0.0016 s−1 and 0.16 s−1. As the strain rate has increased, the yield strength has increased but no significant change in tensile strength and strain hardening coefficient has been observed. As the temperature has increased, the yield and tensile strength has decreased in between 25 and 200 °C but it has showed an increase at 300 °C. The strain hardening coefficient has increased in parallel with temperature increase. It has been seen that the strain rate sensitivity has not been affected by temperature. No significant difference in the hardening rate has appeared in between 25 and 200 °C, but the highest value has been calculated at 300 °C. It has been determined that the fracture behavior has occurred earlier and load carrying capacity on necking has reduced with the increase of strain rate and not significantly affected by temperature.


1980 ◽  
Vol 15 (4) ◽  
pp. 201-207 ◽  
Author(s):  
M S J Hashmi

Experimental results on a mild steel are reported from ballistics tests which gave rise to strain rates of up to 105 s−1. A finite-difference numerical technique which incorporates material inertia, elastic-strain hardening and strain-rate sensitivity is used to establish the strain-rate sensitivity constants p and D in the equation, σ4 = σ1 (1+(∊/D)1/ p). The rate sensitivity established in this study is compared with those reported by other researchers.


2015 ◽  
Vol 2015 ◽  
pp. 1-6 ◽  
Author(s):  
Ramzi Othman

In several industrial applications, metallic structures are facing impact loads. Therefore, there is an important need for developing constitutive equations which take into account the strain rate sensitivity of their mechanical properties. The Johnson-Cook equation was widely used to model the strain rate sensitivity of metals. However, it implies that the yield and flow stresses are linearly increasing in terms of the logarithm of strain rate. This is only true up to a threshold strain rate. In this work, a three-constant constitutive equation, assuming an apparent activation volume which decreases as the strain rate increases, is applied here for some metals. It is shown that this equation fits well the experimental yield and flow stresses for a very wide range of strain rates, including quasi-static, high, and very high strain rates (from 10−5to 5 × 104 s−1). This is the first time that a constitutive equation is showed to be able to fit the yield stress over a so large strain rate range while using only three material constants.


Understanding the rate dependencies of the tensile strength of reinforcing fibres is a key for the understanding of the rate dependencies of the properties of the corresponding composite materials. Hence, in this study it is attempted to clarify the mechanical responses of aramid and carbon fibres at different rates of strain in the light of our previous observations of strain rate dependence of the corresponding hybrid composites under both static and fatigue flexural conditions. In addition, it is attempted to correlate the rate sensitivity with the degree of structural order in the fibres. The study is carried out with low-, medium- and high-modulus pitch based carbon fibres and with Kevlar 29, 49 and 149 para-aramid fibres, whose strengths were tested at strain rates ranging between 0.004 to 2.0% s -1 . It is shown that the strength results of the two fibre families follow the Weibull distribution at all strain rates studied. In the case of the carbon fibres two different régimes are observed for the scale parameter as a function of strain rate. At low strain rates the scale parameter increases slowly with the rate, whereas a strong decrease is observed at higher strain rates. This trend becomes more evident as the crystallinity of the fibre increases. The low strain rate behaviour is governed by the power law breakdown rule model, whereas the high strain rate behaviour is accounted for by the rate of growth of a sharp inter-crystallite flaw. In the case of the aramid fibres the scale parameter is insensitive to the strain rate, which supposedly results from a situation where fracture in these fibres does not necessarily involve an activation volume controlled mechanism.


1998 ◽  
Vol 552 ◽  
Author(s):  
J. Sun ◽  
J. S. Wu ◽  
G. X. Hu ◽  
Y. H. He ◽  
B. Y. Huang

ABSTRACTIn this work, superplastic behaviours in Ti-33A1–3Cr-0.5Mo (wt%) γ-TiAl alloys with two different initial microstructures of near gamma (NG) and duplex (DM) structure were investigated with respect to the effect of testing temperatures and strain rates. At 1050°C and a strain rate of 8×10–5 S–1, a maximum elongation of 570% was observed for NG-TiAl and a maximum elongation of 467% for DM-TiAl. The relations of flow stress and strain rate sensitivity vs. strain rates at different temperatures were also determined by incremental strain rate tests. The results showed that the value of strain rate sensitivity is higher and the flow stress is lower for NG than those for DM at the same condition. The microstructural evolution during superplastic deformation was examined and correlated to the mechanical properties for these two alloys. The influence of microstructure on the superplastic behaviours of γ-TiAl alloys, and possible superplastic deformation mechanisms were finally discussed.


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