Nitrogen Solubility Index

Author(s):  
AACC Technical
1990 ◽  
Vol 57 (2) ◽  
pp. 207-212
Author(s):  
Wolfgang Kneifel ◽  
Anne Beurel

SummaryThe nitrogen solubility index (NSI) method for the examination of caseinates was evaluated. It was found that widely scattering NSI values are mainly due to ineffective centrifugation and filtration of the caseinate dispersion. In order to avoid this, an improved combined centrifugation–filtration procedure was developed as an alternative to the original NSI method, using an Amicon micropartition system MPS-1 equipped with discs of filter paper. The micropartition devices can be centrifuged in a Gerber centrifuge of the type used for butyromctric fat determination. Several types of caseinates were evaluated with the new method and yielded a markedly smaller range of single values than were obtained with the NSI method.


1968 ◽  
Vol 5 (2) ◽  
pp. 65-71
Author(s):  
MINORU YOSHIDA ◽  
HIROSHI HOSHII ◽  
YOSHINAGA DOI ◽  
HIROSHI MORIMOTO

Author(s):  
L. A. Smirnov ◽  
I. I. Gorbachev ◽  
V. V. Popov ◽  
A. Yu. Pasynkov ◽  
A. S. Oryshchenko ◽  
...  

The CALPHAD method has been employed to compose thermodynamic description of the Fe–Cr–Mn–Ni–Si–C–N system. Using an algorithm based on finding a global minimum of Gibbs energy, the calculations of system phase composition were performed in the temperature range from 1750°C to hardening and in the range of compositions corresponding to 04Kh20N6G11M2AFB steel. Calculations showed that at temperatures above liquidus line, Cr and Mn increase nitrogen solubility in the melt, while Ni and Si reduce it. With an increase in the content of Cr, Mn, Ni, and Si in steel in the studied composition range, both liquidus and solidus temperature decrease. The degree of influence on these temperatures of Cr, Mn, Ni and Si within the steel grade is different and ranges from ~3 to ~14°C. Calculations taking into account the possibility of nitrogen transfer between steel and the atmosphere of air showed that the amount of fixed nitrogen in the alloy under study varies, depending on the composition of the steel and temperature, from ~0.3 to ~0.6 wt%. As the temperature decreases from liquidus to solidus, the amount of fixed nitrogen increases, with the exception of those steel compositions when ferrite and not austenite is released from the liquid phase.


1936 ◽  
Vol 113 (1) ◽  
pp. 273-278
Author(s):  
James A. Hawkins ◽  
Charles W. Shilling
Keyword(s):  

2021 ◽  
Vol 573 ◽  
pp. 120192
Author(s):  
Fabien Bernadou ◽  
Fabrice Gaillard ◽  
Evelyn Füri ◽  
Yves Marrocchi ◽  
Aneta Slodczyk

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