Research on nanoprocess of non-equilibrium materials by in situ ultra-high voltage electron microscopy

Microscopy ◽  
2020 ◽  
Vol 69 (6) ◽  
pp. 331-339
Author(s):  
Hidehiro Yasuda ◽  
Kazuhisa Sato ◽  
Hirotaro Mori

Abstract Ultra-high voltage electron microscopy is useful for research utilizing high-penetration thickness of electron beam, in situ observation, or irradiation effects by the particle characteristics of electrons. In this review, the importance of non-equilibrium materials science research by a combination with irradiation effects and in situ observation is shown, and examples of some research are introduced. For example, crystal-amorphous-crystalline phase transition in intermetallic compounds, non-equilibrium phase transition in pure metallic nanoparticles and nucleation and growth process of electron irradiation-induced crystallization in amorphous nanoparticles will be discussed. Finally, we want to suggest the importance of exploring non-equilibrium materials science based on dynamic structures which has been unexplored.

Author(s):  
Gareth Thomas

The applications of high voltage electron microscopy in materials science stem principally from the well known advantages of improved penetration, resolution, and benefits derived from multiple diffraction effects (e.g. critical voltage).The principal disadvantages are the high costs, somewhat poorer resolution compared to the latest breed of 100 to 125 kV microscopes and for crystals it is necessary to operate at voltages below those which cause primary knockon damage, unless in situ studies of such damage are required.


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