scholarly journals Fingerprint Analysis ofDesmodium TriquetrumL.Based on Ultra Performance Liquid Chromatography with Photodiode Array Detector Combined with Chemometrics Methods

2016 ◽  
Vol 54 (5) ◽  
pp. 706-712 ◽  
Author(s):  
Meiling Zhang ◽  
Cui Zhao ◽  
Xianrui Liang ◽  
Yin Ying ◽  
Bing Han ◽  
...  
Molecules ◽  
2019 ◽  
Vol 24 (4) ◽  
pp. 718 ◽  
Author(s):  
Fernanda Rezende ◽  
Marcelo Ferreira ◽  
Mads Clausen ◽  
Magdalena Rossi ◽  
Claudia Furlan

Tibouchina pulchra (Cham.) Cogn. is a plant native to Brazil whose genus and family (Melastomataceae) are poorly studied with regards to its metabolite profile. Phenolic pigments of pink flowers were studied by ultra-performance liquid chromatography with a photodiode array detector and electrospray ionization quadrupole time-of-flight mass spectrometry. Therein, twenty-three flavonoids were identified with eight flavonols isolated by preparative high-performance liquid chromatography and analysed by one- and two-dimensional nuclear magnetic resonance. Kaempferol derivatives were the main flavonols, encompassing almost half of the detected compounds with different substitution patterns, such as glucoside, pentosides, galloyl-glucoside, p-coumaroyl-glucoside, and glucuronide. Concerning the anthocyanins, petunidin p-coumaroyl-hexoside acetylpentoside and malvidin p-coumaroyl-hexoside acetylpentoside were identified and agreed with previous reports on acylated anthocyanins from Melastomataceae. A new kaempferol glucoside was identified as kaempferol-(2′′-O-methyl)-4′-O-α-d-glucopyranoside. Moreover, twelve compounds were described for the first time in the genus with five being new to the family, contributing to the chemical characterisation of these taxa.


2014 ◽  
Vol 6 (15) ◽  
pp. 5872-5878 ◽  
Author(s):  
Yi Yang ◽  
Jing Zhang ◽  
Bing Shao

An analytical method was developed for the simultaneous determination of 14 dyes in jelly and gummy candy using ultra performance liquid chromatography with a photodiode array detector.


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