A 13C nuclear magnetic resonance study of glycals (1,5-Anhydro-hex-1-enitols)

1977 ◽  
Vol 30 (5) ◽  
pp. 1037 ◽  
Author(s):  
AIR Burfitt ◽  
RD Guthrie ◽  
RW Irvine
Keyword(s):  
Nuclear Magnetic Resonance ◽  
Magnetic Resonance ◽  
Chemical Shift ◽  
Nuclear Magnetic Resonance Study ◽  
Shift Reagent ◽  
Proton Chemical Shift ◽  
Lanthanide Shift Reagent ◽  
Magnetic Resonance Study ◽  
13C Nuclear Magnetic Resonance ◽  
Nuclear Magnetic

A series of D-allal and D-glucal derivatives were examined by 13C N.M.R. spectroscopy. Assignments of 13C resonances were established by standard chemical shift considerations, lanthanide shift reagent and proton chemical shift correlations. Configuration-induced chemical shift variations are reported between the glucal and allal systems.

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