Graphite intercalation compound (GIC) crystal monochromators for cold neutron instruments: Characterization of KC24 by time-of-flight neutron diffraction

2021 ◽  
Vol 92 (2) ◽  
pp. 023306
Author(s):  
Andrew J. C. Dennison ◽  
Anton Devishvili ◽  
Philipp Gutfreund ◽  
Robert Cubitt ◽  
Alexei Vorobiev ◽  
...  
Keyword(s):  
Neutron Diffraction ◽  
Cold Neutron ◽  
Time Of Flight ◽  
Intercalation Compound ◽  
Graphite Intercalation Compound ◽  
Graphite Intercalation

Preparation and Characterization of a Tetrabutylammonium Graphite Intercalation Compound

2011 ◽  
Vol 133 (32) ◽  
pp. 12436-12438 ◽  
Author(s):  
Weekit Sirisaksoontorn ◽  
Adeniyi A. Adenuga ◽  
Vincent T. Remcho ◽  
Michael M. Lerner
Keyword(s):  
Intercalation Compound ◽  
Graphite Intercalation Compound ◽  
Graphite Intercalation

Preparation and Characterization of the C2H5COOH-Graphite Intercalation Compound

2013 ◽  
Vol 734-737 ◽  
pp. 2181-2186 ◽  
Author(s):  
Ming Shan Zhou ◽  
Jian Cai Xia
Keyword(s):  
Raw Materials ◽  
Intercalation Compound ◽  
Chemical Oxidation ◽  
Graphite Intercalation Compound ◽  
Structure And Properties ◽  
Mass Ratio ◽  
Natural Graphite ◽  
Graphite Intercalation ◽  
Composition Structure

The graphite intercalation compound with easy low temperature exfoliated and high exfoliated volume was prepared by chemical oxidation method using natural graphite flakes, C2H5COOH, FeCl3 and CrO3 as raw materials, according to the mass ratio of 1:2.8:0.3:0.2. The expansion volume of graSubscript textphite intercalation compounds was 320 mL•g-1 at 300°C and achieved biggest 580 mL•g-1 at 700°C. The composition, structure and properties of the graphite intercalation compound were characterized and analyzed by SEM, FTIR, XRD, TG, DSC, VSM techniques. Results showed that the intercalant of graphite sandwich were C2H5COO- and FeCl3.

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