Experimental cell with a Fabry–Pérot resonator tuned in situ for magnetic resonance studies of matrix-isolated radicals at temperatures below 1 K

2020 ◽  
Vol 91 (6) ◽  
pp. 063901
Author(s):  
S. Sheludiakov ◽  
D. M. Lee ◽  
V. V. Khmelenko ◽  
J. Järvinen ◽  
J. Ahokas ◽  
...  
Keyword(s):  
Magnetic Resonance ◽  
Magnetic Resonance Studies ◽  
Experimental Cell ◽  
Fabry Perot

MoO(S2)(S2CNR2)2 Complexes (R = Me, Et, Pr, Bu): Improved Syntheses and Thermogravimetric and Nuclear Magnetic Resonance Studies

1991 ◽  
Vol 44 (3) ◽  
pp. 361 ◽  
Author(s):  
XF Yan ◽  
CG Young
Keyword(s):  
Mass Spectrometry ◽  
Nuclear Magnetic Resonance ◽  
Magnetic Resonance ◽  
Elemental Analysis ◽  
High Yield ◽  
Magnetic Resonance Studies ◽  
Thermogravimetric Analyses ◽  
Nuclear Magnetic

The reactions of MoO (S2CNR2)2 [R=Me, Et, Pr, Bu; formed in situ from the reactions of cis-MoO2(S2CNR2)2 and PR′3 (R′= Ph, Bu)] and propylene sulfide in 1,2-dichloroethane (for R = Me) or dichloromethane (others) constitute convenient, high-yield syntheses for the blue, seven-coordinate complexes MoO (S2)(S2CNR2)2 The complexes have been characterized by elemental analysis, infrared, electronic and 1H and 13C n.m.r. spectroscopy, and mass spectrometry. Thermogravimetric analyses indicate decomposition of the complexes to Mo2O2(μ-S)2(S2CNR2)2 at temperatures greater than 160°C.

The toroid cavity autoclave for high-pressure and variable-temperature in situ nuclear magnetic resonance studies

2002 ◽  
Vol 73 (3) ◽  
pp. 1259-1266 ◽  
Author(s):  
Heiko G. Niessen ◽  
Peter Trautner ◽  
Sabine Wiemann ◽  
Joachim Bargon ◽  
Klaus Woelk
Keyword(s):  
Nuclear Magnetic Resonance ◽  
High Pressure ◽  
Magnetic Resonance ◽  
Variable Temperature ◽  
Magnetic Resonance Studies ◽  
Nuclear Magnetic
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