scholarly journals Synthesis of rGO-Ni by microwave irradiation method

2020 ◽  
Author(s):  
I Made Joni ◽  
Mila Sri Hardiati ◽  
Ferry Faizal ◽  
Camellia Panatarani
Keyword(s):  
Microwave Irradiation ◽  
Microwave Irradiation Method

Cellulose-g-PAM Derived from Kenaf for Ethyl Orange Removal

2016 ◽  
Vol 818 ◽  
pp. 246-249 ◽  
Author(s):  
Siti Fatimah Mohamed Razak ◽  
Norzita Ngadi ◽  
Nurul Jannah Arsad
Keyword(s):  
Waste Water ◽  
Microwave Irradiation ◽  
Ftir Spectroscopy ◽  
Microwave Irradiation Method ◽  
Spectroscopy Analysis

A novel hybrid flocculant of acrylamide and cellulose was synthesized by using microwave irradiation method. Cellulose was extracted from kenaf by using TAPPI method. 57.4% of percentage grafting and efficiency has been obtained from the grafting process. There are additional peaks that appeared in FTIR spectroscopy analysis that show PAM was grafted into cellulose backbone. The flocculation behavior was studied by using ethyl orange wastewater. The result shows that hybrid flocculant (cellulose-g-PAM) has potential to be used as flocculant in treating dyes waste water.

Microwave synthesis of high rate nanostructured LiMnBO3 with excellent cyclic behavior for lithium ion batteries

RSC Advances ◽  
2014 ◽  
Vol 4 (60) ◽  
pp. 31851-31854 ◽  
Author(s):  
Kaliyappan Karthikeyan ◽  
Yun Sung Lee
Keyword(s):  
Microwave Irradiation ◽  
Lithium Ion Batteries ◽  
Microwave Synthesis ◽  
Lithium Ion ◽  
High Rate ◽  
Cyclic Behavior ◽  
Microwave Irradiation Method

LiMnBO3 nanobeads (LMB-NB) prepared using a urea assisted microwave irradiation method delivered 67 mA h g−1 capacity at 0.6 C rate between 1.25 and 4.8 V, showing 88% cyclability after 100 cycles.

MAGNETIC BEHAVIOR OF Ni-DOPED CuO NANOPARTICLES SYNTHESIZED BY MICROWAVE IRRADIATION METHOD

2019 ◽  
Vol 26 (05) ◽  
pp. 1850184 ◽  
Author(s):  
C. THANGAMANI ◽  
M. PONNAR ◽  
P. PRIYADHARSHINI ◽  
P. MONISHA ◽  
S. S. GOMATHI ◽  
...  
Keyword(s):  
Magnetic Properties ◽  
Microwave Irradiation ◽  
Copper Oxide ◽  
Lattice Constant ◽  
Copper Oxide Nanoparticles ◽  
Oxide Nanoparticles ◽  
Microwave Irradiation Method ◽  
Nickel Doping ◽  
X Ray ◽  
Ft Ir

Nickel-substituted copper oxide nanoparticles at various concentrations were synthesized by the microwave irradiation technique. The consequence of nickel doping on crystal structure, optical properties, and magnetic properties was examined by means of X-ray diffractometer, ultraviolet-visible spectrometer, Fourier transform infrared (FT-IR) spectrometer, transmission electron microscope, and vibrating sample magnetometer (VSM). X-ray diffraction analysis shows that the samples are monoclinic and their crystallite size varies from 25[Formula: see text]nm to 42[Formula: see text]nm, and lattice constant significantly increases with nickel concentration. Additional increase of nickel content (7%) decreases the lattice constant. TEM micrograph witnessed that the prepared nanoparticles were sphere-shaped and the particle distribution is in the range between 20 and 40[Formula: see text]nm. Bandgap measurement reveals that both undoped and nickel-doped copper oxides are direct bandgap semiconductor materials with bandgaps of 3.21 and 3.10[Formula: see text]eV, respectively, FT-IR spectra of the synthesized samples confirmed the nickel doping. VSM studies confirmed the ferromagnetic behavior of the synthesized samples at room temperature. The results revealed that the nickel-doped copper oxide nanoparticles synthesized via the microwave irradiation method exhibit better magnetic properties than the undoped copper oxide.

3,4-Dihydropyrimidin-2(1H)-One Analogues: Microwave irradiated Synthesis with Antimicrobial and Antituberculosis Study

2019 ◽  
Vol 6 (1) ◽  
pp. 61-70
Author(s):  
Navin Patel ◽  
Sabir Pathan ◽  
Hetal I. Soni
Keyword(s):  
Microwave Irradiation ◽  
Biginelli Reaction ◽  
Antitubercular Activity ◽  
Antimicrobial Activities ◽  
Chemical Diversity ◽  
Spectral Studies ◽  
Dilution Method ◽  
Bacterial Strains ◽  
Microwave Irradiation Method

Background: For rapid and sustainable synthesis, microwave irradiation method is serviceable. This present study deals with the preparation of oxadiazole and pyridine bearing 1,2,3,4- tetrahydro pyrimidine derivatives by microwave irradiation. Objective: The present study aims to carry out rapid synthesis of chloro-acetamides of oxadiazoles of Biginelli product and amino cyano derivative of pyridine by microwave-assisted heating. Our efforts are focused on the introduction of chemical diversity in the molecular framework in order to synthesize pharmacologically interesting compounds. Methods:: Microwave irradiation was used for the synthesis of 2-((3-cyano-4-(3,4-dichloro phenyl)- 6-(4-hydroxy-3-methoxyphenyl) pyridin-2-yl) amino)-N-(5-(substituted) -(6-methyl-2-oxo -1,2,3,4- tetrahydro pyrimidin-5-yl)-1,3,4-oxadiazol-2-yl)acetamide by using Biginelli reaction. New structural analogues were confirmed by spectral studies followed by their screening for in vitro antibacterial activity against Staphylococcus aureus, Staphylococcus Pyogenus, Escherichia coli and Pseudomonas aeruginosa bacterial strains and for antifungal activity against Candida albicans, Aspergillus niger and Aspergillus clavatus by micro-broth dilution method. In vitro antimycobacterial activity determined out against (Mycobacterium tuberculosis) H37Rv strain using Lowenstein-Jensen medium. Results: As compared to the conventional method, microwave irradiation method is advantageous for the synthesis of 1,2,3,4-tetrahydropyrimidin derivatives. Potent antimicrobial activities and antitubercular activity were found for some of the compounds. Conclusion: Microwave irradiation method provided an effective way to discover a novel class of antimicrobial and antituberculosis agents. 1,2,3,4-tetrahydropyrimidin derivatives showed improved antimicrobial and good antituberculosis activity.

scholarly journals Enhanced electrochemical performance of α-MoO3/graphene nanocomposites prepared by an in situ microwave irradiation technique for energy storage applications

RSC Advances ◽  
2020 ◽  
Vol 10 (38) ◽  
pp. 22836-22847
Author(s):  
P. Nagaraju ◽  
M. Arivanandhan ◽  
A. Alsalme ◽  
A. Alghamdi ◽  
R. Jayavel
Keyword(s):  
Energy Storage ◽  
Microwave Irradiation ◽  
Electrochemical Performance ◽  
Graphene Sheets ◽  
Microwave Irradiation Method ◽  
Graphene Nanocomposites ◽  
One Step ◽  
Energy Storage Applications ◽  
Enhanced Electrochemical Performance

Nanoparticles of α-molybdenum oxide (α-MoO3) are directly grown on graphene sheets using a surfactant-free facile one step ultrafast in situ microwave irradiation method.

Microwave synthesis of new biologically important 1,4-dihydropyridines containing benzothiazole moiety

2010 ◽  
Vol 75 (3) ◽  
pp. 275-287 ◽  
Author(s):  
Mithlesh ◽  
Pawan K. Pareek ◽  
Hemraj Chippa ◽  
Ravikant ◽  
Krishan G. Ojha
Keyword(s):  
Microwave Irradiation ◽  
Aromatic Aldehyde ◽  
Microwave Synthesis ◽  
Solid Support ◽  
Solvent Free ◽  
Microwave Irradiation Method ◽  
Antifungal Activities ◽  
Antibacterial And Antifungal Activities ◽  
Antibacterial And Antifungal ◽  
Active Methylene

2,3,5,6-Tetrasubstituted-4-aryl-1-(6-ethoxybenzothiazol-2-yl)-1,4-dihydropyridines were synthesized by the reaction of 2-amino-6-ethoxybenzothiazole, an aromatic aldehyde and an active methylene compound in methanol by conventional or microwave irradiation method (solvent-free or with solid support). All compounds were tested for antibacterial and antifungal activities and the results were compared with standard drugs. Their acaricidal and antifeedant activities were also tested.

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