Comparative analysis of dry ashing and wet digestion methods for determination of Pb metal in tobacco leaves

2020 ◽  
Author(s):  
Mai Anugrahwati ◽  
Ardi Falahudin ◽  
Argo Khoirul Anas
Keyword(s):  
Comparative Analysis ◽  
Tobacco Leaves ◽  
Wet Digestion ◽  
Dry Ashing ◽  
Digestion Methods

Adaptation of a Dry Ashing Procedure for Determination of Selenium by Fluorimetry in High-Fat Foods

1995 ◽  
Vol 78 (2) ◽  
pp. 477-479 ◽  
Author(s):  
Jacques R Bellanger
Keyword(s):  
Magnesium Nitrate ◽  
High Fat ◽  
Fluorimetric Determination ◽  
Digestion Method ◽  
Wet Digestion ◽  
Dry Ashing ◽  
Selenium Determination ◽  
Wet Ashing ◽  
Total Procedure

Abstract The wet ashing–dry ashing procedure for destruction of organic matter in high-fat foods for subsequent fluorimetric determination of selenium was investigated. Samples were decomposed by predigestion with nitric acid and dry-ashed with magnesium nitrate and hydrochloric acid. Selenium was recovered quantitatively through the total procedure. Detection limit was about 4 ppb. Accuracy was tested by analysis of several reference materials and by comparison with the wet-digestion method. The present method can be used conveniently for selenium determination in high-fat foods.

Comparative Research of Two Pretreatment Methods on Determination of Trace Manganese in Panax Pseudo-Ginseng Var. Notoginseng by Atomic Absorption Spectroscopy

2012 ◽  
Vol 554-556 ◽  
pp. 2064-2067
Author(s):  
Jin Yang ◽  
Wei Liu ◽  
Bao Sheng Wang ◽  
Qing Hua Li ◽  
Ping Yi ◽  
...  
Keyword(s):  
Atomic Absorption ◽  
Absorption Spectroscopy ◽  
Atomic Absorption Spectroscopy ◽  
Recovery Rate ◽  
Comparative Research ◽  
Manganese Content ◽  
Wet Digestion ◽  
Dry Ashing ◽  
Better Than

In this research the atomic absorption spectroscopy method (the correlation coefficient was 0.9995) was employed for determination of the content of heavy metal-manganese in panax pseudo-ginseng var. notoginseng, which was chosen as the sample. The optimum conditions of two pretreatments were researched independently. In the dry ashing, the optimized temperature and time are 600°C and 4~6 hours respectively, and the manganese content determined is 53.16 ug/g and the recovery rate of manganese added in sample is 98.64%. In the wet digestion, The HNO3-H2O2 digestion system is the best one, and the content was 52.95ug/g and the recovery rate is 97.30%. So the two pretreatment methods of the sample are accurate enough on manganese content determination. But the dry ashing is better than the wet digestion relatively.

Minerals in Feeds by Atomic Absorption Spectrophotometry

1967 ◽  
Vol 50 (1) ◽  
pp. 45-50 ◽  
Author(s):  
Mary Heckman
Keyword(s):  
Sample Preparation ◽  
Atomic Absorption ◽  
Atomic Absorption Spectrophotometry ◽  
Absorption Spectrophotometry ◽  
Wet Digestion ◽  
Dry Ashing ◽  
Mineral Mixture ◽  
Calcium Magnesium ◽  
Calcium And Magnesium

Abstract Seventeen laboratories collaborated in the study of analysis of feeds for calcium, magnesium, zinc, manganese, iron, and copper by atomic absorption spectrophotometry. Six feeds and one mineral mixture were analyzed; both dry ashing and wet digestion were used to prepare samples. Three feeds were in the form of solutions to eliminate sample preparation as a variable. Strontium and lanthanum were added to the feed to eliminate phosphorus interference and results were compared. Results indicate that the method is suitable for calcium and magnesium. Further work is needed on the determination of zinc, manganese, iron, and copper.

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